CN214344450U - Europium oxide purification is with concentrated jar in vacuum - Google Patents

Abstract

The utility model relates to a vacuum concentration jar technical field just discloses an europium oxide purification uses vacuum concentration jar, including a jar body and upper seal lid, the equal fixedly connected with supporting leg in both sides of jar body bottom, the equal fixedly connected with ear seat in both sides on the both sides on jar body top and upper seal lid top, just jar body and upper seal lid pass through bolt looks fixed connection, one side fixedly connected with inlet pipe at upper seal lid top, the fixed cover of middle part fixedly connected with at upper seal lid top. This europium oxide purification is with vacuum concentration jar, through the setting of screw rod, the rotation of puddler can drive the screw rod rotation of looks fixed connection with it, and the rotation of screw rod makes the thread bush of looks threaded connection with it can remove along the screw rod, and the thread bush drives the stirring leaf of looks fixed connection with it and reciprocates, and the reciprocating of stirring leaf makes the internal liquid of jar can be heated evenly, has improved the concentrated efficiency of liquid.

Description

Europium oxide purification is with concentrated jar in vacuum

Technical Field

The utility model relates to a vacuum concentration jar technical field specifically is a vacuum concentration jar is used in europium oxide purification.

Background

The material science shows the status and the function of traditional Chinese medicine in the high-tech field which is rapidly developed at present, the wide application of rare earth elements draws attention of people, in a plurality of high-tech fields, the purity required by the application of the rare earth elements is increasingly ultra-high purified, and europium is taken as one of the rare earth elements and is applied to the research of high-definition fluorescent materials, laser, superconducting materials and the like due to the special electronic layer structure and the performance of the europium.

Europium oxide needs to use the vacuum concentration jar in the purification process, the jar body top of the presently used vacuum concentration jar is equipped with blowing pipe and vacuum outlet duct, vacuum outlet duct hookup vacuum pump, the last vacuum discharge port that has seted up of blowing pipe, during the use, throw europium oxide raw materials solution into the jar body from the inlet pipe, then start the vacuum pump, take out the internal air of jar, be vacuum environment, to jar body heating, evaporation, concentrated material, after the concentration is accomplished, open the drain hole of vacuum discharge port and jar body bottom, negative pressure cancellation in the jar body makes the automatic drain hole of following of concentrated material discharge, but in practical application, when the blowing, the material is easy with vacuum discharge port jam, slowed down the speed that negative pressure cancelled in the jar body, influenced the automatic smooth discharge of material, reduced production efficiency.

SUMMERY OF THE UTILITY MODEL

To current europium oxide purification with the not enough of vacuum concentration jar, the utility model provides a europium oxide purification is with vacuum concentration jar possesses the advantage that can prevent that the vacuum discharge port from blockking up etc. has solved the problem of proposing among the above-mentioned background art.

The utility model provides a following technical scheme: a vacuum concentration tank for purifying europium oxide comprises a tank body and an upper sealing cover, wherein supporting legs are fixedly connected to two sides of the bottom of the tank body, lug seats are fixedly connected to two sides of the top of the tank body and two sides of the top of the upper sealing cover, the tank body and the upper sealing cover are fixedly connected through bolts, an inlet pipe is fixedly connected to one side of the top of the upper sealing cover, a fixing sleeve is fixedly connected to the middle of the top of the upper sealing cover, a motor is fixedly sleeved in an inner cavity of the fixing sleeve, a stirring rod is fixedly connected to the tail end of an output shaft of the motor, the other end of the stirring rod penetrates through the top of the upper sealing cover and extends to the inner cavity of the tank body, the stirring rod is movably connected with the top of the upper sealing cover, a vacuum discharge pipe is fixedly connected to the other side of the top of the upper sealing cover, and an exhaust pipe is fixedly connected to the other side of the top of the upper sealing cover, the other end of exhaust tube and the air inlet looks fixed connection of vacuum pump, one side fixedly connected with baffle at sealed lid inner chamber top on, the lateral wall of baffle and the inner wall looks fixed connection of sealed lid on, the other end of vacuum delivery pipe and exhaust tube all is located the inboard of baffle, the lateral wall of the jar body is bilayer, one side fixedly connected with steam admission pipe of jar body bottom, the opposite side fixedly connected with steam discharge pipe on jar body top, the middle part of jar body bottom is equipped with the bin outlet, and the inner chamber swing joint of bin outlet has the electromagnetism door, the equal fixedly connected with comdenstion water receiving flask in both sides of jar body bottom, the top of comdenstion water receiving flask extends to the inner chamber of jar body lateral wall.

Preferably, the middle part of the bottom of the condensed water collecting bottle is provided with a water outlet, an inner cavity of the water outlet is clamped with a sealing plug, two sides of the bottom of the condensed water collecting bottle are fixedly connected with springs, and the other ends of the springs are fixedly connected with the sealing plug.

Preferably, a plurality of screw rods of bottom fixedly connected with of puddler, and the screw thread opposite direction that the surface of two adjacent screw rods was equipped with, the outer lane threaded connection of screw rod has the thread bush, and the even fixedly connected with stirring leaf in surface of thread bush, the inner chamber fixedly connected with electric heat silk screen of stirring leaf, the material of stirring leaf is the metal.

Preferably, one side fixedly connected with dead lever of puddler bottom, the other end fixedly connected with scraper blade of dead lever, the other end of scraper blade contacts with the inner wall of the jar body.

Preferably, the baffle includes the backup pad, the top of backup pad and the inner wall looks fixed connection of last sealed lid, the equal swing joint in both sides of backup pad bottom has the dwang, and the other end of dwang runs through the lateral wall of last sealed lid and extends to the outside of sealed lid, one the outside fixedly connected with baffle one at dwang middle part, another the outside fixedly connected with baffle two at dwang middle part, vacuum discharge pipe is located the inboard of baffle one, the exhaust tube is located the inboard of baffle two, two motors of outside fixedly connected with on last sealed lid top, the output shaft end of motor is fixedly connected with the other end of dwang.

With the current europium oxide purification vacuum concentration jar contrast, the utility model discloses possess following beneficial effect:

1. this europium oxide purification is with vacuum concentration jar, setting through the spring, the function of automatic drainage can be realized to the comdenstion water receiving flask, comdenstion water in the comdenstion water receiving flask is when the comdenstion water is gradual increase, the comdenstion water can extrude the sealing plug downwards, the sealing plug can be gradually with the inner chamber separation of outlet, when having the clearance between the inner chamber of sealing plug and outlet, unnecessary comdenstion water can be discharged in the comdenstion water receiving flask, water in the comdenstion water receiving flask reduces, water is less than the thrust of spring to the sealing plug to the extrusion force of sealing plug, the sealing plug again with outlet looks joint under the effect of the resilience force of spring, the comdenstion water can continue to be collected to the comdenstion water receiving flask, use the in-process of this comdenstion water receiving flask, do not need the staff to empty the comdenstion water, staff's the amount of labour has been reduced.

2. This europium oxide purification is with vacuum concentration jar, through the setting of screw rod, the rotation of puddler can drive the screw rod rotation of looks fixed connection with it, and the rotation of screw rod makes the thread bush of looks threaded connection with it can remove along the screw rod, and the thread bush drives the stirring leaf of looks fixed connection with it and reciprocates, and the reciprocating of stirring leaf makes the internal liquid of jar can be heated evenly, has improved the concentrated efficiency of liquid.

Drawings

FIG. 1 is a front view of the structure of the present invention;

FIG. 2 is an internal schematic view of the structure of FIG. 1 of the present invention;

fig. 3 is a schematic view of the top of the structure baffle of the present invention.

In the figure: 1. a tank body; 2. an upper sealing cover; 3. supporting legs; 4. a feed pipe; 5. a motor; 6. a vacuum exhaust pipe; 7. an air exhaust pipe; 8. a stirring rod; 9. stirring blades; 10. fixing the rod; 11. a squeegee; 12. a baffle plate; 121. a first baffle plate; 122. a second baffle plate; 123. a support plate; 124. rotating the rod; 125. a motor; 13. an electromagnetic gate; 14. a steam inlet pipe; 15. a condensed water collecting bottle; 16. a spring; 17. a sealing plug; 18. a steam discharge pipe; 19. a screw.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-3, a vacuum concentration tank for purifying europium oxide comprises a tank body 1 and an upper sealing cover 2, wherein two sides of the bottom of the tank body 1 are fixedly connected with supporting legs 3, two sides of the top of the tank body 1 and two sides of the top of the upper sealing cover 2 are fixedly connected with lug seats, the tank body 1 and the upper sealing cover 2 are fixedly connected through bolts, the upper sealing cover 2 and the tank body 1 are conveniently fixed or separated through the connection mode of the tank body 1 and the upper sealing cover 2, one side of the top of the upper sealing cover 2 is fixedly connected with a feeding pipe 4, europium oxide raw material solution to be purified can be injected into the tank body 1 for purification through the feeding pipe 4, a fixing sleeve is fixedly connected to the middle part of the top of the upper sealing cover 2, a motor 5 is fixedly sleeved in an inner cavity of the fixing sleeve, and the rotation of the motor 5 can drive a stirring rod 8 fixedly connected with the fixing sleeve to rotate through the setting of the motor 5, the tail end of an output shaft of the motor 5 is fixedly connected with a stirring rod 8, the other end of the stirring rod 8 penetrates through the top of the upper sealing cover 2 and extends to the inner cavity of the tank body 1, the stirring rod 8 is movably connected with the top of the upper sealing cover 2, the other side of the top of the upper sealing cover 2 is fixedly connected with a vacuum discharge pipe 6, the other side of the top of the upper sealing cover 2 is fixedly connected with an exhaust pipe 7, the other end of the exhaust pipe 7 is fixedly connected with an air inlet of a vacuum pump, one side of the top of the inner cavity of the upper sealing cover 2 is fixedly connected with a baffle plate 12, the baffle plate 12 can play a role in intercepting solution in the tank body 1, the solution in the tank body 1 is prevented from splashing into the inner cavity of the vacuum discharge pipe 6 or the exhaust pipe 7 to influence the work of the vacuum discharge pipe 6 and the exhaust pipe 7, the side wall of the baffle plate 12 is fixedly connected with the inner wall of the upper sealing cover 2, and the other ends of the vacuum discharge pipe 6 and the exhaust pipe 7 are positioned on the inner side of the baffle plate 12, the side wall of the tank body 1 is double-layer, one side of the bottom end of the tank body 1 is fixedly connected with a steam inlet pipe 14, steam is injected into an inner cavity of the side wall of the tank body 1 through the steam inlet pipe 14 and flows in the inner cavity of the side wall of the tank body 1, the steam generates heat exchange with liquid in the inner cavity of the tank body 1 in the process of moving in the inner cavity of the side wall of the tank body 1, the liquid is heated, evaporation of redundant moisture in the liquid is facilitated, solution in the tank body 1 is concentrated, europium oxide is purified conveniently, gas after the heat exchange is discharged from a steam discharge pipe 18, the other side of the top end of the tank body 1 is fixedly connected with a steam discharge pipe 18, the middle part of the bottom of the tank body 1 is provided with a discharge port, the inner cavity of the discharge port is movably connected with an electromagnetic door 13, opening or closing of the discharge port is conveniently controlled through the arrangement of the electromagnetic door 13, and the discharge port is in an open state, the concentrated liquid in the tank body 1 is conveniently discharged, when the bin outlet is in closed state, the use of this concentrated jar of being convenient for, the equal fixedly connected with comdenstion water receiving flask 15 in both sides of jar body 1 bottom, the top of comdenstion water receiving flask 15 extends to the inner chamber of jar body 1 lateral wall, can collect the comdenstion water of jar body 1 lateral wall inner chamber through comdenstion water receiving flask 15.

Wherein, the middle part of the bottom of the condensed water collecting bottle 15 is provided with a water outlet, and the inner cavity of the water outlet is clamped with a sealing plug 17, two sides of the bottom of the condensed water collecting bottle 15 are fixedly connected with springs 16, the other end of the spring 16 is fixedly connected with the sealing plug 17, the shape of the sealing plug 17 is a round platform, through the arrangement of the spring 16, the condensed water collecting bottle 15 can realize the function of automatic drainage, when the condensed water in the condensed water collecting bottle 15 gradually increases, the condensed water can downwards extrude the sealing plug 17, the sealing plug 17 can be gradually separated from the inner cavity of the water outlet, when a gap is formed between the sealing plug 17 and the inner cavity of the water outlet, the redundant condensed water in the condensed water collecting bottle 15 can be discharged, the water in the condensed water collecting bottle 15 is reduced, the extrusion force of the water to the sealing plug 17 is smaller than the thrust of the spring 16 to the sealing plug 17, the sealing plug 17 is clamped with the water outlet again under the resilience force of the spring 16, the comdenstion water collecting bottle 15 can continue to collect the comdenstion water, uses this comdenstion water collecting bottle 15's in-process, does not need the staff to empty the comdenstion water, has reduced staff's the amount of labour.

Wherein, a plurality of screw rods 19 of bottom fixedly connected with of puddler 8, and the screw thread opposite direction that two adjacent screw rods 19's surface was equipped with, the outer lane threaded connection of screw rod 19 has the thread bush, and the even fixedly connected with stirring leaf 9 in surface of thread bush, the inner chamber fixedly connected with electric heat silk screen of stirring leaf 9, the material of stirring leaf 9 is the metal, through the setting of screw rod 19, the rotation of puddler 8 can drive the screw rod 19 rotation of looks fixed connection with it, the rotation of screw rod 19 makes the thread bush of looks threaded connection with it can remove along screw rod 19, the thread bush drives the stirring leaf 9 of looks fixed connection with it and reciprocates, reciprocate of stirring leaf 9, make the liquid in the jar body 1 can be heated evenly, the concentration efficiency of liquid has been improved.

Wherein, one side fixedly connected with dead lever 10 of puddler 8 bottom, the other end fixedly connected with scraper blade 11 of dead lever 10, the other end of scraper blade 11 contacts with the inner wall of the jar body 1, through the setting of dead lever 10 and scraper blade 11, the rotation of puddler 8 drives mutually fixed connection's dead lever 10 and rotates with it, dead lever 10 drives mutually fixed connection's scraper blade 11 and rotates with it, scraper blade 11 can scrape the solution of adhesion on the internal wall of jar, prevent that solution from producing the burnt paste, influence the concentration of solution.

Wherein, the baffle 12 comprises a supporting plate 123, the top of the supporting plate 123 is fixedly connected with the inner wall of the upper sealing cover 2, both sides of the bottom of the supporting plate 123 are movably connected with a rotating rod 124, and the other end of the rotating rod 124 penetrates through the side wall of the upper sealing cover 2 and extends to the outer side of the upper sealing cover 2, the outer side of the middle part of one rotating rod 124 is fixedly connected with a baffle I121, the outer side of the middle part of the other rotating rod 124 is fixedly connected with a baffle II 122, the vacuum discharge pipe 6 is positioned at the inner side of the baffle I121, the exhaust pipe 7 is positioned at the inner side of the baffle II 122, the outer side of the top end of the upper sealing cover 2 is fixedly connected with two motors 125, the tail end of the output shaft of the motor 125 is fixedly connected with the other end of the rotating rod 124, through the arrangement of the motors 125, the rotation of the motor 125 can drive the rotating rod 124 fixedly connected therewith to rotate, the rotating rod 124 can drive the baffle I121 or the baffle II 122 fixedly connected therewith to rotate, when the first baffle 121 deflects, the inner cavity of the concentration tank is communicated with the vacuum discharge pipe 6, external gas can enter the concentration tank, the pressure intensity in the concentration tank is improved, liquid in the concentration tank is convenient to discharge, when the second baffle 122 deflects, the inner cavity of the exhaust pipe 7 is communicated with the inner cavity of the concentration tank, and the vacuum pump can exhaust the gas in the concentration tank through the exhaust pipe 7 to form vacuum in the concentration tank, so that the concentration of the solution is convenient.

The working principle is as follows: when the device is used, a worker injects a proper amount of europium oxide solution to be concentrated into the concentration tank through the feeding pipe 4, the motor 125 is started, the rotation of the motor 125 drives the rotating rod 124 fixedly connected with the motor to rotate, the rotating rod 124 can drive the baffle plate two 122 fixedly connected with the rotating rod 124 to rotate, the inner cavity of the exhaust pipe 7 is communicated with the inner cavity of the concentration tank, the vacuum pump is started, the vacuum pump exhausts gas in the concentration tank through the exhaust pipe 7 to form vacuum in the concentration tank, after the vacuum is formed in the concentration tank, the motor 125 rotates reversely, the vacuum pump stops working, the inner cavity of the concentration tank is in a sealed state, the worker injects steam into the steam inlet pipe 14, the steam enters the inner cavity of the side wall of the tank body 1 along the steam inlet pipe 14, the steam flows in the inner cavity of the side wall of the tank body 1, and the steam generates heat exchange with liquid in the inner cavity of the tank body 1 in the process of moving in the inner cavity of the side wall of the tank body 1, liquid is heated, evaporation of redundant moisture in the liquid is facilitated, concentration of solution in the tank body 1 is achieved, purification of europium oxide is facilitated, gas after heat exchange is discharged from a steam discharge pipe 18, in the process of introducing steam, a worker starts a motor 5 and an electric heating wire net, heat emitted by the electric heating wire net during working can heat a stirring blade 9, the stirring blade 9 heats liquid around the stirring blade, the motor 5 rotates to drive a stirring rod 8 fixedly connected with the stirring rod to rotate, the stirring rod 8 rotates to drive a screw rod 19 and a fixed rod 10 fixedly connected with the screw rod to rotate, the screw rod 19 rotates to enable a threaded sleeve in threaded connection with the screw rod to move along the screw rod 19, the threaded sleeve drives the stirring blade 9 fixedly connected with the threaded sleeve to move up and down, the stirring blade 9 moves up and down, the liquid in the tank body 1 can be heated uniformly, concentration efficiency of the liquid is improved, the fixed rod 10 drives a scraper 11 fixedly connected with the threaded sleeve to rotate, the scraper 11 can scrape off the solution adhered to the inner wall of the tank body 1, and prevent the solution from generating scorching and influencing the concentration of the solution.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (5)

1. The utility model provides a europium oxide purifies uses vacuum concentration jar, includes jar body (1) and last sealed lid (2), its characterized in that: the utility model discloses a novel energy-saving tank, including a tank body (1), a jar body (1), a top, a bottom, supporting legs (3), a top, a middle part, a fixed cover, a motor (5), a stirring rod (8), a top, a vacuum discharge pipe (6), a top, a bottom and a top cover (2), wherein the supporting legs (3) are fixedly connected to both sides of the bottom of the tank body (1), the ear seats are fixedly connected to both sides of the top of the tank body (1) and both sides of the top of the upper cover (2), the tank body (1) and the upper cover (2) are fixedly connected through bolts, the feeding pipe (4) is fixedly connected to one side of the top of the upper cover (2), the fixed cover is fixedly connected to the middle part of the top of the upper cover (2), the motor (5) is fixedly connected to the inner cavity of the fixed cover, the stirring rod (8) is fixedly connected to the tail end of the output shaft of the motor (5), the stirring rod (8) penetrates through the top of the upper cover (2) and extends to the inner cavity of the tank body (1), the other side of the top of the upper sealing cover (2) is fixedly connected with an exhaust pipe (7), the other end of the exhaust pipe (7) is fixedly connected with an air inlet of a vacuum pump, one side of the top of the inner cavity of the upper sealing cover (2) is fixedly connected with a baffle (12), the side wall of the baffle (12) is fixedly connected with the inner wall of the upper sealing cover (2), the other ends of the vacuum discharge pipe (6) and the exhaust pipe (7) are both positioned at the inner side of the baffle (12), the side wall of the tank body (1) is double-layer, one side of the bottom of the tank body (1) is fixedly connected with a steam inlet pipe (14), the other side of the top of the tank body (1) is fixedly connected with a steam discharge pipe (18), the middle part of the bottom of the tank body (1) is provided with a discharge hole, the inner cavity of the discharge hole is movably connected with an electromagnetic door (13), and both sides of the bottom of the tank body (1) are both fixedly connected with a condensed water collecting bottle (15), the top of the condensed water collecting bottle (15) extends into the inner cavity of the side wall of the tank body (1).

2. The vacuum concentration tank for europium oxide purification of claim 1, wherein: the middle part of comdenstion water receiving flask (15) bottom is equipped with the outlet, and the inner chamber joint of outlet has sealing plug (17), the equal fixedly connected with spring (16) in both sides of comdenstion water receiving flask (15) bottom, the other end and the looks fixed connection of sealing plug (17) of spring (16).

3. The vacuum concentration tank for europium oxide purification of claim 1, wherein: the utility model discloses a stirring rod, including puddler, bottom fixedly connected with a plurality of screw rods (19) of puddler (8), and the screw thread opposite direction that the surface of two adjacent screw rods (19) was equipped with, the outer lane threaded connection of screw rod (19) has the thread bush, and the even fixedly connected with stirring leaf in surface (9) of thread bush, the inner chamber fixedly connected with electric heat silk screen of stirring leaf (9), the material of stirring leaf (9) is the metal.

4. The vacuum concentration tank for europium oxide purification of claim 1, wherein: one side fixedly connected with dead lever (10) of puddler (8) bottom, the other end fixedly connected with scraper blade (11) of dead lever (10), the other end of scraper blade (11) contacts with the inner wall of jar body (1).

5. The vacuum concentration tank for europium oxide purification of claim 1, wherein: the baffle (12) comprises a supporting plate (123), the top of the supporting plate (123) is fixedly connected with the inner wall of the upper sealing cover (2), two sides of the bottom of the supporting plate (123) are movably connected with rotating rods (124), the other end of the rotating rod (124) penetrates through the side wall of the upper sealing cover (2) and extends to the outer side of the upper sealing cover (2), the outer side of the middle part of one rotating rod (124) is fixedly connected with a first baffle plate (121), the outer side of the middle part of the other rotating rod (124) is fixedly connected with a second baffle plate (122), the vacuum discharge pipe (6) is positioned on the inner side of the first baffle plate (121), the exhaust pipe (7) is positioned on the inner side of the second baffle plate (122), the outer side of the top end of the upper sealing cover (2) is fixedly connected with two motors (125), the tail end of an output shaft of the motor (125) is fixedly connected with the other end of the rotating rod (124).

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