CN214319405U - Natural methyl laurate purification device - Google Patents

Abstract

The utility model is suitable for a purification device technical field provides a natural methyl laurate purification device, the top of purification bucket has seted up the feed inlet, and fixedly connected with screen cloth on the inner wall of feed inlet, be provided with electric heating coil on the inner wall of purification bucket, still seted up the inlet on the lateral wall of purification bucket, and one side that purification bucket is close to the inlet still is provided with the mixing solution bucket, the mixing solution bucket with the intercommunication has first connecting pipe between the inlet, sets up the feed inlet at the top of purification device, and sets up the screen cloth in the feed inlet, after the staff pours methyl laurate on the screen cloth, through the vibrations of vibrator to the screen cloth, can be with methyl laurate from a plurality of via holes of seting up on the screen cloth in the purification bucket, through the vibrations of vibrator, can effectually guarantee that methyl laurate can not cause the jam to the via hole, affecting the normal feeding of the working personnel.

Description

Natural methyl laurate purification device

Technical Field

The utility model belongs to the technical field of the purification device, especially, relate to a natural methyl laurate purification device.

Background

Methyl laurate, also known as beta-methyl phenylacrylate, has cocoa flavor, is mainly used in daily use chemicals and food industry, is a common fixative or edible flavor, and is also an important organic synthetic raw material, and the current synthetic methods of the methyl laurate include an inorganic acid (such as hydrochloric acid and sulfuric acid) catalytic esterification method, an organic acid catalytic esterification method, a heterogeneous catalytic esterification method and a high-pressure microwave synthesis method.

At present, most of purification devices are formed by respectively connecting a plurality of evaporation bottles, but in the using process, the evaporation bottles are required to be heated by hands, so that the inconvenience in use is caused, the evaporation bottles are heated by oil lamps, the heating is uneven, and the purification effect is poor; in addition, the manual operation is adopted, so that the labor intensity is high, and the daily operation is not facilitated.

SUMMERY OF THE UTILITY MODEL

The utility model provides a natural methyl laurate purification device aims at solving current purification device operation inconvenient, the poor problem of heating effect.

The utility model discloses a realize like this, a natural methyl laurate purification device, including the purification bucket.

The purification device is characterized in that a feed inlet is formed in the top of the purification barrel, a screen is fixedly connected to the inner wall of the feed inlet, an electric heating coil is arranged on the inner wall of the purification barrel, a liquid inlet is formed in the side wall of the purification barrel, a mixed liquid barrel is arranged on one side, close to the liquid inlet, of the purification barrel, a first connecting pipe is communicated between the mixed liquid barrel and the liquid inlet, a gas outlet is formed in the other side wall of the purification barrel, a collecting box is arranged on one side, close to the gas outlet, of the purification barrel, a second connecting pipe is communicated between the collecting box and the gas outlet, and a condenser is fixedly connected to the second connecting pipe.

Preferably, the two ends of the first connecting pipe and the second connecting pipe are sleeved with sealing rings.

Preferably, a pressure pump is further fixedly connected to the first connecting pipe.

Preferably, a plurality of through holes are formed in the screen, and the lower surface of the screen is fixedly connected with a vibrator.

Preferably, still include the stirring subassembly, the stirring subassembly includes the motor, motor fixed connection in the bottom of purification bucket, its output runs through the diapire of purification bucket and extends to the inside of purification bucket, and through shaft coupling fixedly connected with connecting rod, follow its vertical direction interval on the outer wall of connecting rod, encircle and be provided with the multiunit (mixing) shaft, and every adjacent two sets of the mutual staggered distribution of (mixing) shaft.

Preferably, still encircle on the inner wall of purification bucket and be provided with a plurality of reposition of redundant personnel pieces, and every the reposition of redundant personnel piece is close to the lateral wall of connecting rod all extends to the opposite direction of the direction of motion of connecting rod.

Compared with the prior art, the beneficial effects of the utility model are that: the utility model discloses a natural methyl laurate purification device:

1. the feed inlet is seted up at the top of purification device, and sets up the screen cloth in the feed inlet, after the staff pours methyl laurate on the screen cloth, through the vibrations of vibrator to the screen cloth, can be with in methyl laurate from a plurality of via holes of seting up on the screen cloth pours the purification bucket into, through the vibrations of vibrator, can effectually guarantee that methyl laurate can not lead to the fact the jam to the via hole, influence the normal material loading of staff.

2. Set up the condenser on the second connecting pipe, can carry out quick cooling to the gas that produces in the purification process to become liquid after with gas cooling, then flow into to the collection box in, supply the subsequent use of staff.

3. The stirring subassembly that sets up can flow into in the methyl laurate and the mixed liquid bucket in to the purification bucket and mix the liquid and carry out abundant stirring for its and electric heating coil give off the heat intensive mixing, accelerated reaction efficiency, improved purification speed, made things convenient for staff's daily work.

4. Through the rotation of motor output, can drive the connecting rod and rotate, the connecting rod can drive the multiunit (mixing) shaft and carry out the circumference around the connecting rod and rotate when rotating to carry out the intensive mixing and mix with mixed liquid to the methyl laurate in the purification bucket, avoided the methyl laurate deposit in purification barrel head portion, influence reaction efficiency.

5. The staff sets up a plurality ofly to the shunting piece that the connecting rod rotation direction opposite extended on purification bucket inner wall to carry out the separation to the mixed liquid that is close to purification bucket inner wall and shunt, disturb its flow direction originally, make its abundant and methyl laurate mix, improved the reaction efficiency who mixes liquid and methyl laurate, improved the practicality of this device.

Drawings

Fig. 1 is a schematic structural view of the present invention;

FIG. 2 is a front sectional view of the purification barrel of the present invention;

FIG. 3 is a schematic structural diagram of the screen of the present invention;

FIG. 4 is a top cross-sectional view of the purification barrel of the present invention;

in the figure: the device comprises a purification barrel 1 part, a feed inlet 2 part, a screen 3 part, a via hole 31 part, a liquid inlet 4 part, a mixed liquid barrel 5 part, a first connecting pipe 6 part, a gas outlet 7 part, a collecting box 8 part, a second connecting pipe 9 part, a condenser 10 part, a seal ring 11 part, a pressure pump 12 part, a vibrator 13 part, a stirring assembly 14 part, a motor 141 part, a coupler 142 part, a connecting rod 143 part, a stirring shaft 144 part, an electric heating coil 15 part and a shunting block 16 part.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more clearly understood, the present invention is further described in detail below with reference to the accompanying drawings and embodiments, it is to be understood that the specific embodiments described herein are only used for explaining the present invention, and are not used for limiting the present invention.

Referring to fig. 1-4, the present invention provides a device for purifying natural methyl laurate, which comprises a purifying barrel 1.

Feed inlet 2 has been seted up at the top of purification bucket 1, and fixedly connected with screen cloth 3 on the inner wall of feed inlet 2, be provided with electric heating coil 15 on the inner wall of purification bucket 1, inlet 4 has still been seted up on the lateral wall of purification bucket 1, and one side that purification bucket 1 is close to inlet 4 still is provided with mixing liquid bucket 5, the intercommunication has first connecting pipe 6 between mixing liquid bucket 5 and the inlet 4, gas outlet 7 has still been seted up on another lateral wall of purification bucket 1, and one side that purification bucket 1 is close to gas outlet 7 still is provided with collecting box 8, the intercommunication has second connecting pipe 9 between collecting box 8 and the gas outlet 7, fixedly connected with condenser 10 on the second connecting pipe 9.

In this embodiment, the worker sets the mixing liquid barrel 5 and the collecting tank 8 at two sides of the purifying barrel 1 with the feed inlet 2, respectively, and communicates the first connecting pipe 6 between the liquid inlets 4 formed on the side walls of the mixing liquid barrel 5 and the purifying barrel 1, so as to ensure that the ethanol and the ether in the mixing liquid barrel 5 can enter the purifying barrel 1 from the liquid inlets 4 along the first connecting pipe 6, and then communicates the second connecting pipe 9 between the gas outlets 7 formed on the side walls of the collecting tank 1 and the purifying barrel 1, so as to ensure that the purified gas of the methyl laurate can be discharged into the second connecting pipe 9 along the gas outlet 7 by the purifying barrel 1, further, in this embodiment, the worker also sets a condenser 10 on the second connecting pipe 9, and can cool the purified gas in the second connecting pipe 9 through the condenser 10, and further discharge the cooled liquid into the collecting tank 8, supply subsequent use of staff, in this embodiment, the staff pours methyl laurate into purification bucket 1 from feed inlet 2 in, and the screen cloth 3 that sets up in the feed inlet 2 can disperse methyl laurate to avoided methyl laurate to block up the screen cloth, provided the assurance for the normal operating of this device when having guaranteed that the staff normally feeds.

Referring to fig. 1, further, the two ends of the first connecting pipe 6 and the second connecting pipe 9 are sleeved with sealing rings 11.

In this embodiment, the sealing washer 11 that sets up can be effectual guarantees to mix liquid and purification gas and can not reveal in the junction of first connecting pipe 6 and second connecting pipe 9 in transportation process, has guaranteed the normal work of this device, simultaneously, has also reduced staff's maintenance work load, further improvement the practicality of this device.

Referring to fig. 1, a pressure pump 12 is further fixedly connected to the first connecting pipe 6.

In this embodiment, the force (forcing) pump 12 that sets up can exert pressure to mixed liquid to be convenient for mixed liquid in the mixed liquid bucket 5 can be stable quick enter into purification bucket 1 inside from inlet 4, accelerated with the reaction efficiency of methyl laurate, also avoided appearing the phenomenon emergence of mixed liquid supply insufficiency simultaneously.

Referring to fig. 2-3, further, the screen 3 is provided with a plurality of through holes 31, and the lower surface of the screen 3 is fixedly connected with the vibrator 13.

In this embodiment, the vibrator 13 that sets up is installed in the below of screen cloth 3, when the staff poured methyl laurate into on screen cloth 3, through the vibrations of vibrator 13, drives screen cloth 3 and shakes to it enters into the inside of purification bucket 1 to set up via hole 31 in the abundant screen cloth 3 of following of methyl laurate on screen cloth 3, has accelerated methyl laurate's falling speed, avoids appearing the condition emergence of blockking up screen cloth 3.

Referring to fig. 2, further, the stirring assembly 14 further includes a motor 141, the motor 141 is fixedly connected to the bottom of the purifying barrel 1, an output end of the motor 141 penetrates through the bottom wall of the purifying barrel 1 and extends into the purifying barrel 1, a connecting rod 143 is fixedly connected to the connecting rod 143 through a coupling 142, a plurality of groups of stirring shafts 144 are circumferentially arranged on an outer wall of the connecting rod 143 along a vertical direction thereof at intervals, and each two adjacent groups of stirring shafts 144 are distributed in a staggered manner.

In this embodiment, after the staff pours mixed liquid and methyl laurate into in the purification bucket 1, carry external power source in to motor 141, the warm rotation of controller output, its output rotates through shaft coupling 142 electric connecting rod 143 at purification bucket 1, connecting rod 143 is when rotating, the rotation takes place for electronic multiunit (mixing) shaft 144 of installing on its outer wall, thereby can carry out abundant stirring to mixed liquid and methyl laurate, the reaction efficiency of the two is improved, the purification has been accelerated, guaranteed that this device can satisfy staff's normal work demand.

Referring to fig. 4, further, a plurality of diversion blocks 16 are disposed around the inner wall of the purifying barrel 1, and a side wall of each diversion block 16 near the connecting rod 143 extends in a direction opposite to the moving direction of the connecting rod 143.

In this embodiment, the effect of a plurality of shunting block 16 that set up lies in, and the staff sets up a plurality ofly to connecting rod 143 rotation direction opposite extension's shunting block 16 on the inner wall of purification bucket 1 to carry out the separation to the mixed liquid that is close to purification bucket 1 inner wall and shunt, disturb its original flow direction, make it fully mix with methyl laurate, improved the reaction efficiency of mixed liquid and methyl laurate, improved the practicality of this device.

The utility model discloses a theory of operation and use flow: after the utility model is installed, the worker pours the methyl laurate into the screen mesh 3 in the feed inlet 2, then, after the vibrator 13 is connected with the external power supply, the vibrator drives the screen mesh 3 to shake in the vertical direction, the methyl laurate on the screen mesh 3 conveniently enters the purification barrel 1 along a plurality of through holes 31, then, the work pumps the ethanol and the diethyl ether in the mixed liquid barrel 5 into the purification barrel 1 through the pressure pump 12, and connects the electric heating coil 15 in the purification barrel 1 with the external power supply, so that the temperature of the electric heating coil reaches the temperature required by the reaction, then, the worker connects the external power supply with the motor 141, controls the output end to rotate, drives the multi-group stirring shaft 144 to rotate around the connecting rod 143 when the output end rotates, the mixed liquid and the methyl laurate are stirred, the mixing degree of the mixed liquid and the methyl laurate is improved, the shunt block 16 arranged on the inner wall of the purification barrel 1 can cooperate with the stirring shaft 144 to fully mix the mixed liquid and the methyl laurate, the gas produced after purification reaches the condenser 10 along the second connecting pipe 9, and the condenser 10 cools the gas and then reaches the collecting box 8 along the second connecting pipe 9 for subsequent use of workers.

The above description is only exemplary of the present invention and should not be taken as limiting the scope of the present invention, as any modifications, equivalents, improvements and the like made within the spirit and principles of the present invention are intended to be included within the scope of the present invention.

Claims (6)

1. A natural methyl laurate purification device, which is characterized in that: comprises a purifying barrel (1),

a feed inlet (2) is arranged at the top of the purification barrel (1), a screen (3) is fixedly connected on the inner wall of the feed inlet (2), an electric heating coil (15) is arranged on the inner wall of the purification barrel (1), a liquid inlet (4) is also arranged on the side wall of the purification barrel (1), and a mixed liquid barrel (5) is also arranged on one side of the purification barrel (1) close to the liquid inlet (4), a first connecting pipe (6) is communicated between the mixed liquid barrel (5) and the liquid inlet (4), the other side wall of the purification barrel (1) is also provided with an air outlet (7), and a collecting box (8) is also arranged on one side of the purification barrel (1) close to the air outlet (7), a second connecting pipe (9) is communicated between the collecting box (8) and the air outlet (7), and a condenser (10) is fixedly connected to the second connecting pipe (9).

2. The purification device of natural methyl laurate according to claim 1, wherein: and sealing rings (11) are sleeved at two ends of the first connecting pipe (6) and the second connecting pipe (9).

3. The apparatus for purifying natural methyl laurate according to claim 2, wherein: the first connecting pipe (6) is also fixedly connected with a pressure pump (12).

4. The purification device of natural methyl laurate according to claim 1, wherein: a plurality of through holes (31) are formed in the screen (3), and a vibrator (13) is fixedly connected to the lower surface of the screen (3).

5. The purification device of natural methyl laurate according to claim 1, wherein: still include stirring subassembly (14), stirring subassembly (14) include motor (141), motor (141) fixed connection in the bottom of purification bucket (1), its output runs through the diapire of purification bucket (1) and extend to the inside of purification bucket (1), and through shaft coupling (142) fixedly connected with connecting rod (143), along its vertical direction interval, encircle on the outer wall of connecting rod (143) and be provided with multiunit (144), and every adjacent two sets of (144) crisscross distribution each other.

6. The apparatus of claim 5, wherein the apparatus comprises: the inner wall of the purification barrel (1) is further provided with a plurality of shunting blocks (16) in a surrounding mode, and each shunting block (16) is close to the side wall of the connecting rod (143) and extends towards the direction opposite to the moving direction of the connecting rod (143).

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