CN214242219U

CN214242219U - Sealed strorage device of limonene preparation raw materials

Info

Publication number: CN214242219U
Application number: CN202023214904.4U
Authority: CN
Inventors: 王成坤; 郝建锋
Original assignee: Emei Mountain In Sichuan Pharmaceutical Co ltd
Current assignee: Emei Mountain In Sichuan Pharmaceutical Co ltd
Priority date: 2020-12-28
Filing date: 2020-12-28
Publication date: 2021-09-21
Anticipated expiration: 2030-12-28

Abstract

The utility model relates to a pharmacy technical field just discloses a sealed strorage device of limonene preparation raw materials, including holding vessel, retort, waste liquid jar, holding vessel outer wall right side through connection has the biography material pipe, retort outer wall right side through connection has the outlet pipe, holding vessel outer wall right side middle part through connection has the discharging pipe, retort top surface through connection has the inlet pipe. This kind of sealed strorage device of limonene preparation raw materials, it has conical hopper to connect through the fixed cover in retort top, conical hopper inner wall surface runs through and has seted up the through-hole, the problem that thoughtlessly there are other impurity in the limonene raw materials leads to pharmacy purity not high in the production process is solved, there is the hydraulic means of moulding material through holding vessel top fixed mounting, activity metal pole tail end fixed mounting has the pressure platform, the in-process of having avoided exporting is thoughtlessly had the air to get into the oxidation raw materials, the storage of high-purity limonene and the convenience of taking out have been improved.

Description

Sealed strorage device of limonene preparation raw materials

Technical Field

The utility model relates to a pharmacy technical field specifically is a sealed strorage device of limonene preparation raw materials.

Background

Limonene, named limonene and monoterpene compound, is a natural functional monoterpene, is widely used as an essence and spice additive in food, is colorless oily liquid with fragrance similar to that of lemon, has good effects of relieving cough, eliminating phlegm and inhibiting bacteria, can be clinically used for cholagogue, dissolving stone, promoting secretion of digestive juice and eliminating intestinal pneumatosis, is orange red, orange yellow or colorless clear liquid with specific fragrance, is miscible in ethanol and most of nonvolatile oil, is slightly soluble in glycerol, and is insoluble in water and propylene glycol.

The field of limonene applied in modern life is more and more, however, the process of preparing limonene on a large scale is complex, limonene raw materials obtained through distillation of crude materials added with catalysts are often mixed with other impurities, limonene bodies are active and easy to oxidize by air, and during the process of extracting and storing fine limonene, sealing devices are needed to be used, and therefore a sealed storage device for limonene preparing raw materials is provided.

SUMMERY OF THE UTILITY MODEL

Technical problem to be solved

Not enough to prior art, the utility model provides a sealed strorage device of limonene preparation raw materials possesses the convenience of storage and taking out and is high, and the extraction purity of raw materials is high, and the problem of mentioning in the background art has been solved to advantages such as the leakproofness is stronger.

(II) technical scheme

For the convenience that realizes above-mentioned storage and take out is high, the extraction purity of raw materials is high, the stronger purpose of leakproofness, the utility model provides a following technical scheme: the utility model provides a sealed strorage device of limonene preparation raw materials, includes holding vessel, retort, waste liquid jar, holding vessel outer wall right side through connection has the material pipe of biography, retort outer wall right side through connection has the outlet pipe, holding vessel outer wall right side middle part through connection has the discharging pipe, retort top surface through connection has the inlet pipe, discharging pipe left end demountable installation has the solenoid valve, holding vessel top fixed mounting has hydraulic means, hydraulic means bottom surface fixed mounting has movable metal pole, movable metal pole tail end fixed mounting has the platform that pressurizes, the fixed conical funnel that has cup jointed in retort top, the through-hole has been seted up in conical funnel inner wall surface through.

Preferably, the storage tank, the distillation tank and the waste liquid tank are identical in shape and size and are horizontally arranged at equal intervals, the material conveying pipe is Z-shaped, the left end of the material conveying pipe is connected with the storage tank in a penetrating mode, and the right end of the material conveying pipe is connected with the distillation tank in a penetrating mode.

Preferably, the left end of the water outlet pipe is vertically and penetratingly connected with the bottom of the conical funnel, the height value of the water outlet pipe is larger than that of the material conveying pipe and that of the water outlet pipe, and the diameter values of the material conveying pipe, the material conveying pipe and the water outlet pipe are equal.

Preferably, the hydraulic means's material is moulding material, just the hydraulic means is inside to be filled with inert gas, the diameter value of pressurization platform with holding vessel inner wall diameter value equals, the length value of activity metal rod equals the discharging pipe outer wall with the distance value between the holding vessel top surface.

Preferably, the top size of the conical funnel is matched with the top surface size of the distillation tank, the length value of the bottom end of the conical funnel is half of the length value of the distillation tank, and a catalyst is placed at the bottom of the distillation tank.

Preferably, the quantity of through-hole is a plurality of, divides two rows to be circumference equidistant range and is in conical funnel inner wall, and every the through-hole all runs through perpendicularly conical funnel.

(III) advantageous effects

Compared with the prior art, the utility model discloses possess following beneficial effect:

1. this kind of sealed strorage device of limonene preparation raw materials, it has conical hopper to fix through the retort top and has connect, conical hopper inner wall surface runs through and has seted up the through-hole, the catalyst has been placed through the retort bottom, some other impurity and moisture after the distillation are condensed to conical hopper, in discharging the waste liquid tank with the waste liquid through the outlet pipe, can be continuous during this period add the coarse fodder distill, the purity of this limonene coarse fodder has been improved, the problem that thoughtlessly there are other impurity in the limonene raw materials in the production process and lead to pharmacy purity not high has been solved.

2. This kind of sealed strorage device of limonene preparation raw materials, there is the hydraulic means of moulding material through holding vessel top fixed mounting, and the inside inert gas that is filled with of hydraulic means, hydraulic means bottom surface fixed mounting has movable metal pole, activity metal pole tail end fixed mounting has the platform that pressurizes, press down moulding hydraulic means and make inside inert gas that is filled with extrude the holding vessel in, the platform that pressurizes can be quick passes through the discharging pipe output with the higher limonene raw materials of purity, the output of limonene raw materials in can effectual control discharging pipe through the solenoid valve, the in-process of having avoided exporting has thoughtlessly been thoughtlessly had air admission oxidation raw materials, the storage of high-purity limonene and the convenience of taking out have been improved.

Drawings

FIG. 1 is a schematic view of the whole structure of the present invention;

FIG. 2 is a schematic diagram of a part of the components of the structure of FIG. 1 of the present invention;

fig. 3 is a schematic diagram of a part of the components of the structure diagram 2 of the present invention.

In the figure: 1. a storage tank; 2. a distillation tank; 3. a waste liquid tank; 4. a material conveying pipe; 5. a water outlet pipe; 6. a discharge pipe; 7. a feed pipe; 8. an electromagnetic valve; 9. a hydraulic device; 10. a pressurizing table; 11. a movable metal rod; 12. a conical funnel; 13. and a through hole.

Detailed Description

The technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, rather than all embodiments, and all other embodiments obtained by a person of ordinary skill in the art without creative work belong to the protection scope of the present invention based on the embodiments of the present invention.

Examples

Referring to fig. 1-3, a sealed storage device for raw materials for limonene preparation comprises a storage tank 1, a distillation tank 2, a waste liquid tank 3, the storage tank 1, the distillation tank 2 and the waste liquid tank 3 are identical in shape and size and are horizontally arranged at equal intervals, a catalyst is placed at the bottom of the distillation tank 2, a material transfer pipe 4 is connected to the right side of the outer wall of the storage tank 1 in a penetrating manner, the material transfer pipe 4 is Z-shaped, the left end of the material transfer pipe 4 is connected to the storage tank 1 in a penetrating manner, the right end of the material transfer pipe 4 is connected to the distillation tank 2 in a penetrating manner, a water outlet pipe 5 is connected to the right side of the outer wall of the distillation tank 2 in a penetrating manner, the left end of the water outlet pipe 5 is vertically connected to the bottom of a conical funnel 12 in a penetrating manner, a discharge pipe 6 is connected to the middle of the right side of the outer wall of the storage tank 1 in a penetrating manner, the height value of the discharge pipe 6 is greater than the height values of the material transfer pipe 4 and the water outlet pipe 5, the diameter values of the three are equal, a feeding pipe 7 is connected to the top surface of the distillation tank 2 in a penetrating manner, the left end of the discharge pipe 6 is detachably provided with an electromagnetic valve 8, the top of the storage tank 1 is fixedly provided with a hydraulic device 9, the hydraulic device 9 is made of a shaping material, inert gas is filled in the hydraulic device 9, the bottom surface of the hydraulic device 9 is fixedly provided with a movable metal rod 11, the length value of the movable metal rod 11 is equal to the distance value between the outer wall of the discharge pipe 6 and the top surface of the storage tank 1, the tail end of the movable metal rod 11 is fixedly provided with a pressurizing table 10, the diameter value of the pressurizing table 10 is equal to the diameter value of the inner wall of the storage tank 1, the inert gas filled in the storage tank 1 is extruded by pressing the shaping hydraulic device 9, the limonene raw material with higher purity can be rapidly output through the discharge pipe 6 through the pressurizing table 10, the output of the limonene raw material in the discharge pipe 6 can be effectively controlled through the electromagnetic valve 8, and the phenomenon that air, the fixed conical hopper 12 that has cup jointed in 2 tops of retort, conical hopper 12's top size and 2 top surface size looks adaptations of retort, and conical hopper 12's bottom length value is half of retort 2's length value, conical hopper 12 inner wall surface runs through and has seted up through-hole 13, the quantity of through-hole 13 is a plurality of, divide two rows to be circumference equidistant range at conical hopper 12 inner wall, and every through-hole 13 all runs through conical hopper 12 perpendicularly, the catalyst has been placed through retort 2 bottom, some other impurity and moisture after the distillation are condensed to conical hopper 12 in, discharge waste liquid tank 3 with the waste liquid through outlet pipe 5, can constantly add the coarse fodder during this period and distill, the purity of this limonene coarse fodder has been improved.

The working principle is as follows: firstly, put into a quantitative catalyst with retort 2 bottom, connect into the device that carries the limonene raw materials with inlet pipe 7 and carry the coarse fodder, the catalyst has been placed through retort 2 bottom, then, some other impurity and moisture after the distillation are condensed to conical hopper 12 in, discharge the waste liquid to waste liquid jar 3 through outlet pipe 5 in, the coarse fodder of adding that can be continuous during this period distills, finally, press moulding hydraulic means 9 and make inside inert gas that is filled with extrude storage tank 1 in, through adding the output of table 10 can be quick with the higher limonene raw materials of purity through discharging pipe 6, solenoid valve 8 can the output of the limonene raw materials in the effectual control discharging pipe 6, avoided the in-process at the output to mix the air admission oxidation raw materials.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a sealed strorage device of limonene preparation raw materials, includes holding vessel (1), retort (2), waste liquid jar (3), its characterized in that: storage tank (1) outer wall right side through connection has material transmission pipe (4), retort (2) outer wall right side through connection has outlet pipe (5), storage tank (1) outer wall right side middle part through connection has discharging pipe (6), retort (2) top surface through connection has inlet pipe (7), discharging pipe (6) left end demountable installation has solenoid valve (8), storage tank (1) top fixed mounting has hydraulic means (9), hydraulic means (9) bottom surface fixed mounting has movable metal pole (11), movable metal pole (11) tail end fixed mounting has pressurization platform (10), the fixed cover of retort (2) top has cup jointed toper funnel (12), toper funnel (12) inner wall surface runs through and has seted up through-hole (13).

2. The sealed storage device for limonene preparation raw materials according to claim 1, wherein: the storage tank (1), the distillation retort (2) the shape and size of the waste liquid tank (3) are the same, and are arranged horizontally at equal intervals, the material conveying pipe (4) is Z-shaped, the left end of the material conveying pipe (4) is in through connection with the storage tank (1), and the right end of the material conveying pipe is in through connection with the distillation retort (2).

3. The sealed storage device for limonene preparation raw materials according to claim 1, wherein: the left end of the water outlet pipe (5) is vertically and penetratingly connected with the bottom of the conical funnel (12), the height value of the water outlet pipe (6) is larger than that of the material conveying pipe (4) and the water outlet pipe (5), and the diameter values of the three are equal.

4. The sealed storage device for limonene preparation raw materials according to claim 1, wherein: the material of hydraulic means (9) is the plasticity material, just hydraulic means (9) is inside to be filled with inert gas, the diameter value of pressurization platform (10) with holding vessel (1) inner wall diameter value equals, the length value of activity metal pole (11) equals discharging pipe (6) outer wall with distance value between holding vessel (1) top surface.

5. The sealed storage device for limonene preparation raw materials according to claim 1, wherein: the top size of conical funnel (12) with retort (2) top surface size looks adaptation, just the bottom length value of conical funnel (12) is half of the length value of retort (2), the catalyst has been placed to retort (2) bottom.

6. The sealed storage device for limonene preparation raw materials according to claim 1, wherein: the quantity of through-hole (13) is a plurality of, divides two rows to be the circumference and arranges equally spaced cone funnel (12) inner wall, and every through-hole (13) all runs through perpendicularly cone funnel (12).