CN214210473U

CN214210473U - Industrial-grade graphene oxide production device

Info

Publication number: CN214210473U
Application number: CN202022056601.8U
Authority: CN
Inventors: 不公告发明人
Original assignee: Changzhou Lanyue New Material Technology Co ltd
Current assignee: Changzhou Lanyue New Material Technology Co ltd
Priority date: 2020-09-18
Filing date: 2020-09-18
Publication date: 2021-09-17
Anticipated expiration: 2030-09-18

Abstract

The utility model discloses an industrial grade oxidation graphite alkene apparatus for producing, including the mount, still include: the protective kettle is fixedly arranged at the top end of the fixing frame; the fixed seat is fixedly arranged in the middle of the top end of the protection kettle; the motor is fixedly arranged at the top end of the fixed seat along the vertical direction, and the output end of the bottom end of the motor extends into the inner cavity of the protective kettle; the cover plate can be hinged to the middle part of the front side of the top end of the protective kettle in an opening and closing manner; and the swinging mechanism is arranged at the top end of the inner cavity of the protection kettle. This industrial grade oxidation graphite alkene apparatus for producing accelerates the oxidation reaction of graphite alkene, makes reaction solution and graphite alkene contact abundant contact, reduces the oxidation graphite alkene required time, improves the production efficiency of enterprise, can do suitable adjustment to reaction rate according to the graphite alkene of different weight simultaneously, and the use scene is nimble abundant, and safety protection nature is stronger.

Description

Industrial-grade graphene oxide production device

Technical Field

The utility model relates to a graphite alkene production technical field specifically is an industrial grade oxidation graphite alkene apparatus for producing.

Background

Graphene is a carbon simple substance formed by orderly arranging carbon atoms according to hexagonal lattices, a two-dimensional space infinitely-extending base plane formed by hybridizing the carbon atoms according to sp2 is a material with a 2D structure and is proved to be the thinnest and the hardest substance found in the world, the graphene is a basic unit for constructing other-dimension carbonaceous materials, can be changed into zero-dimension fullerene, is curled into a one-dimension carbon nano tube, can also be superposed into three-dimensional graphite, is oxidized graphene, is an oxide of the graphene as the name suggests, introduces active oxygen-containing groups onto the graphene, and obtains a modified graphene sheet after treatment, so that the active reaction sites of the graphene are increased, the oxidized graphene is easier to carry out surface modification, functional means are enriched, and the compatibility of the modified oxidized graphene with solvents, polymers and the like can be effectively improved, the material has wider application in the field of organic and inorganic composite materials;

at present, the society is extensive to graphite alkene material demand, and traditional industrial grade oxidation graphite alkene production efficiency is lower, all needs to optimize in the continuation and the continuity of graphite alkene production process, and secondly in the oxidation reaction process to graphite alkene, reaction solution and graphite alkene contact reaction are not enough, lead to the oxidation graphite alkene yield of production lower, need prolong reaction time, influence production efficiency, the safety protection nature is relatively poor.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide an industrial grade oxidation graphite alkene apparatus for producing to have in the production process that provides among the solution prior art and treat optimization, graphite alkene and the insufficient and lower problem of production efficiency of solution reaction on continuation and the continuity.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides an industrial grade oxidation graphite alkene apparatus for producing, includes the mount, still includes:

the protective kettle is fixedly arranged at the top end of the fixing frame;

the fixed seat is fixedly arranged in the middle of the top end of the protection kettle;

the motor is fixedly arranged at the top end of the fixed seat along the vertical direction, and the output end of the bottom end of the motor extends into the inner cavity of the protective kettle;

the cover plate can be hinged to the middle part of the front side of the top end of the protective kettle in an opening and closing manner;

the swinging mechanism is arranged at the top end of the inner cavity of the protective kettle;

the feeding pipe penetrates through the middle position of the front side of the protective kettle along the front-back direction;

the electromagnetic flow meter is fixedly arranged on the outer side of the outer wall of the feeding pipe and is attached to the middle of the front side of the protective kettle;

and the liquid discharge pipe is fixedly connected to the middle part of the bottom end of the protection kettle.

Preferably, the swing mechanism includes: a rotating rod, the rotating rod along the upper and lower direction and through the shaft coupling lock in the output of motor: the two limiting rods are fixedly arranged on the upper side and the lower side of the top end of the inner cavity of the protective kettle respectively along the left-right direction; the first rotating disc can move up and down and is clamped outside the outer wall of the top end of the rotating rod; the screw handle can be rotationally clamped at the middle position of the left side of the top end of the protective kettle around the axis of the screw handle; the top end of the pulley is in threaded connection with the bottom end of the wrench, and the bottom end of the pulley is clamped in the middle of the first rotary disc; the middle part of the second rotary disc is sleeved and connected with the middle part of the bottom end of the rotary rod in a rotating mode through a pin shaft; the upper end and the lower end of the connecting rod are respectively connected to the inner side edge positions of the first rotating disc and the second rotating disc in a rotating mode through pin shafts; the two lifting rods can be respectively clamped in the middle parts of the left side and the right side of the limiting rod in a vertically movable manner; the limiting fixture blocks are fixedly arranged on the inner sides of the lifting rods respectively in the left and right directions, and the inner sides of the limiting fixture blocks extend and are attached to the inner sides of the middle parts of the outer walls of the second turnplates.

Preferably, the outer walls of the two sides of the front side of the rotating rod, which is in contact with the second rotating disc, are both planes.

Preferably, the inner side of the limiting clamping block is spherical.

Preferably, the inner cavity of the protection kettle is further provided with: the two connecting seats are respectively and rotatably connected to the bottom ends of the lifting rods through pin shafts; the reaction kettle is fixedly connected to the inner sides of the two fixing seats; the electromagnetic valve is fixedly arranged in the middle of the bottom end of the reaction kettle; one end of the liquid leakage pipe is fixedly connected to the left side of the bottom end of the inner cavity of the protective kettle, and the other end of the liquid leakage pipe is connected to the upper part of the middle part of the liquid discharge pipe; the corrugated pipe is fixedly connected between the electromagnetic valve and the liquid discharge pipe; stirring fan blade, a plurality of stirring fan blade is the slope form and follows circumference fixed connection in the bottom outer wall outside of rotary rod, and is located in reation kettle's the inner chamber.

Preferably, a certain gap is left between the edge of the stirring fan blade and the inner wall of the reaction kettle.

Compared with the prior art, the beneficial effects of the utility model are that: this industrial grade oxidation graphite alkene apparatus for producing, through the inlet pipe, electromagnetic flowmeter, reation kettle, the duration and the continuity in graphite alkene production process have been optimized to the mutually supporting between solenoid valve and the fluid-discharge tube, improve industrial grade oxidation graphite alkene's production efficiency, secondly can rock and stir simultaneously graphite alkene in the reation kettle and solution through the mutually supporting between swing mechanism and the stirring flabellum, with higher speed oxidation reaction of graphite alkene, make reaction solution and graphite alkene contact abundant contact, reduce oxidation graphite alkene required time, improve enterprise production efficiency, simultaneously can be according to the graphite alkene of different weight do suitable adjustment to reaction rate, the use scene is nimble abundant, safety protection nature is stronger.

Drawings

Fig. 1 is a schematic structural view of the present invention;

FIG. 2 is a schematic sectional view of the front view of the present invention;

fig. 3 is a schematic view of a three-dimensional structure of the middle swing mechanism of the present invention.

In the figure: 1. the mount, 2, the protection cauldron, 3, the fixing base, 4, the motor, 5, the apron, 6, swing mechanism, 7, the inlet pipe, 8, electromagnetic flowmeter, 9, the connecting seat, 10, reation kettle, 11, the solenoid valve, 12, the weeping pipe, 13, the bellows, 14, the fluid-discharge tube, 15, stirring fan blade, 61, the rotary rod, 62, the gag lever post, 63, first carousel, 64, twist the hand, 65, the pulley, 66, the connecting rod, 67, the second carousel, 68, the lifter, 69, spacing fixture block.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-3, the present invention provides a technical solution: the utility model provides an industrial grade oxidation graphite alkene apparatus for producing, includes mount 1, still includes: the device comprises a protective kettle 2, a fixed seat 3, a motor 4, a cover plate 5, a swing mechanism 6, a feeding pipe 7, an electromagnetic flowmeter 8 and an electromagnetic flowmeter 8, wherein the protective kettle 2 is fixedly arranged at the top end of a fixed frame 1 to prevent corrosive solution in the protective kettle from splashing out, and has a certain protective and anticorrosive effect; the fixed seat 3 is fixedly arranged in the middle of the top end of the protective kettle 2 and plays a role in fixing the motor 4; the motor 4 is fixedly arranged at the top end of the fixed seat 3 along the up-down direction, and the output end at the bottom end of the motor extends into the inner cavity of the protective kettle 2 to provide main power energy for the device; the cover plate 5 can be hinged to the middle part of the front side of the top end of the protective kettle 2 in an opening and closing manner; the swing mechanism 6 is arranged at the top end of the inner cavity of the protective kettle 2; the feeding pipe 7 penetrates through the middle position of the front side of the protective kettle 2 along the front-back direction; the electromagnetic flowmeter 8 is fixedly arranged on the outer side of the outer wall of the feeding pipe 7 and is attached to the middle of the front side of the protective kettle 2, so that the volume of the solution entering the protective kettle can be counted conveniently; and the liquid discharge pipe 14 is fixedly connected to the middle part of the bottom end of the protective kettle 2 and used for discharging the reacted graphene oxide.

Preferably, the swing mechanism 6 further includes: rotary rod 61, gag lever post 62, first carousel 63, twist hand 64, pulley 65, connecting rod 66, second carousel 67, lifter 68 and spacing fixture block 69, rotary rod 61 is along upper and lower direction and through the output of shaft coupling locking in motor 4: the two limiting rods 62 are respectively and fixedly arranged at the upper side and the lower side of the top end of the inner cavity of the protective kettle 2 along the left-right direction; the first rotating disc 63 can move up and down and is clamped outside the outer wall of the top end of the rotating rod 61; the screw handle 64 can be clamped at the middle position of the left side of the top end of the protective kettle 2 in a rotating way around the axis of the screw handle; the top end of the pulley 65 is screwed with the bottom end of the wrench 64, and the bottom end of the pulley 65 is clamped in the middle of the first rotating disc 63; the middle part of the second rotating disc 67 is sleeved and connected with the middle part of the bottom end of the rotating rod 61 through a pin shaft; the upper end and the lower end of the connecting rod 66 are respectively connected to the inner side edge positions of the first rotating disc 63 and the second rotating disc 67 through pin shafts in a rotating manner; the two lifting rods 68 can be respectively clamped in the middle parts of the left side and the right side of the limiting rod 62 in a vertically movable manner; the limiting fixture block 69 is respectively and fixedly arranged on the inner side of the lifting rod 68 along the left-right direction, the inner side of the limiting fixture block 69 extends and is attached to the inner side of the middle part of the outer wall of the second turntable 67, the reaction kettle 10 can be swung through the swinging mechanism 6, and the swinging amplitude can be adjusted.

Preferably, the outer walls of the rotating rod 61 contacting the second rotating disk 67 are flat, so that the second rotating disk 67 can be turned.

Preferably, the inner side of the stopper 69 is formed in a spherical shape so that the elevating rod 68 can be driven even when the second turntable 67 is in a tilted state.

As a preferable scheme, further, the inner cavity of the protective kettle 2 is further provided with: the device comprises connecting seats 9, a reaction kettle 10, an electromagnetic valve 11, a liquid leakage pipe 12, a corrugated pipe 13 and stirring fan blades 15, wherein the two connecting seats 9 are respectively connected to the bottom ends of lifting rods 68 in a rotating manner through pin shafts; the reaction kettle 10 is fixedly connected to the inner sides of the two fixed seats 3; the electromagnetic valve 11 is fixedly arranged at the middle position of the bottom end of the reaction kettle 10, so that a worker can conveniently control and discharge the solution in the reaction kettle 10; one end of the liquid leakage pipe 12 is fixedly connected to the left side of the bottom end of the inner cavity of the protective kettle 2, and the other end of the liquid leakage pipe is connected to the upper part of the middle part of the liquid discharge pipe 14, so that the solution splashed into the protective kettle 2 can be discharged; the bellows 13 is fixedly connected between the electromagnetic valve 11 and the liquid discharge pipe 14, has certain flexibility, and can swing along with the swing of the reaction kettle 10; a plurality of stirring fan blade 15 is the slope form and along circumference fixed connection in the bottom outer wall outside of rotary rod 61, and is arranged in reation kettle 10's inner chamber, stirs solution.

As a preferable scheme, a certain gap is left between the edge of the stirring fan 15 and the inner wall of the reaction kettle 10, so as to prevent the reaction kettle 10 from colliding with the stirring fan 15 in the swinging process.

All the electric device models of the scheme can meet the use requirement of the scheme, and can be purchased in the market.

The detailed connection means is a technique known in the art, and the following mainly describes the working principle and process, and the specific operation is as follows.

In the actual use process of the device, graphene and reaction solution can be added into the reaction kettle 10 through the liquid inlet pipe and the cover plate 5, so as to achieve the oxidation condition of the graphene, then the reaction kettle 10 swings left and right through the swing mechanism 6, firstly, the motor 4 is started, as the rotating rod 61 is locked at the output end at the bottom end of the motor 4 through the coupler, the inner side of the middle part of the rotating rod 61 is sleeved and rotationally connected with the middle part of the bottom end of the rotating rod 61 through the pin shaft, in the movement process, the first rotating disc 63 and the second rotating disc 67 are driven to rotate, and as the top end of the pulley 65 is screwed with the screw handle 64 and is simultaneously clamped at the middle part of the inner side of the outer wall of the first rotating disc 63; the upper and lower ends of the connecting rod 66 are respectively connected to the edge position between the first turntable 63 and the second turntable 67 through the pin shaft, when the operator rotates the handle 64, the pulley 65 and the first turntable 63 are driven to move up and down, and the connecting rod 66 drives one side of the second turntable 67 to turn over upwards, at this time, the second turntable 67 is in an inclined and rotating state, in the rotating process of the second turntable 67, the two lifting rods 68 are driven to do a mutually staggered lifting motion under the clamping action of the two limiting clamping blocks 69, so as to achieve the purpose of swinging the reaction kettle 10 left and right, and under the stirring action of the stirring fan blades 15, the solution and the graphene are fully stirred, and in the reaction process, if the solution rolls and splashes out of the reaction kettle 10, the solution can fall into the inner cavity of the protective kettle 2 and is sent into the liquid discharge pipe 14 through the liquid leakage pipe 12, treat that whole reactions are accomplished the back, see off inside mixed solution through bellows 13 and fluid-discharge tube 14 through control solenoid valve 11, the device can be applicable to multiple oxidation graphite alkene production scene, and nimble adjustment reation kettle 10's swing angle accelerates the oxidation reaction of graphite alkene, makes reaction solution and graphite alkene contact abundant contact, reduces the required time of oxidation graphite alkene, improves the production efficiency of enterprise.

In the description of the present invention, it is to be understood that the terms "bottom", "one end", "top", "middle", "other end", "upper", "one side", "top", "inner", "front", "both ends" and the like indicate orientations or positional relationships based on those shown in the drawings, which are merely for convenience of description and simplicity of description, and do not indicate or imply that the device or element so referred to must have a particular orientation, be constructed in a particular orientation, and be operated; also, unless expressly stated or limited otherwise, the terms "disposed," "mounted," "connected," "fixedly mounted," and the like are to be construed broadly and can, for example, be fixedly connected, detachably connected, or integral to one another; can be mechanically or electrically connected; they may be directly connected or indirectly connected through an intermediate medium, and may be connected through the inside of two elements or in an interaction relationship between two elements, unless otherwise specifically defined, and the specific meaning of the above terms in the present invention will be understood by those skilled in the art according to specific situations.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides an industrial grade oxidation graphite alkene apparatus for producing, includes mount (1), its characterized in that still includes:

the protective kettle (2), the protective kettle (2) is fixedly arranged at the top end of the fixed frame (1);

the fixed seat (3) is fixedly arranged in the middle of the top end of the protective kettle (2);

the motor (4) is fixedly arranged at the top end of the fixed seat (3) along the vertical direction, and the output end of the bottom end of the motor (4) extends into the inner cavity of the protective kettle (2);

the cover plate (5) is hinged to the middle part of the front side of the top end of the protective kettle (2) in an openable and closable manner;

the swing mechanism (6) is arranged at the top end of the inner cavity of the protective kettle (2);

the feeding pipe (7) penetrates through the middle position of the front side of the protective kettle (2) along the front-back direction;

the electromagnetic flow meter (8) is fixedly arranged on the outer side of the outer wall of the feeding pipe (7) and is attached to the middle of the front side of the protective kettle (2);

and the liquid discharge pipe (14), wherein the liquid discharge pipe (14) is fixedly connected to the middle part of the bottom end of the protective kettle (2).

2. The industrial-grade graphene oxide production device according to claim 1, wherein: the swing mechanism (6) comprises:

rotary rod (61), rotary rod (61) along upper and lower direction and through the shaft coupling lock in the output of motor (4):

the two limiting rods (62) are fixedly arranged on the upper side and the lower side of the top end of the inner cavity of the protective kettle (2) along the left-right direction respectively;

the first rotating disc (63) can move in the vertical direction and is clamped outside the outer wall of the top end of the rotating rod (61);

the screwing handle (64) can rotate around the axis of the screwing handle (64) and is clamped in the middle position of the left side of the top end of the protective kettle (2);

the top end of the pulley (65) is in threaded connection with the bottom end of the twisting handle (64), and the bottom end of the pulley (65) is clamped in the middle of the first rotating disc (63);

the middle part of the second rotating disc (67) is sleeved and connected with the middle part of the bottom end of the rotating rod (61) in a rotating mode through a pin shaft;

the upper end and the lower end of the connecting rod (66) are respectively connected to the inner side edge positions of the first rotating disc (63) and the second rotating disc (67) in a rotating mode through pin shafts;

the two lifting rods (68) can move up and down respectively and are clamped in the middle parts of the left side and the right side of the limiting rod (62);

the limiting clamping blocks (69) are fixedly arranged on the inner sides of the lifting rods (68) in the left-right direction respectively, and the inner sides of the limiting clamping blocks (69) extend and are attached to the inner sides of the middle of the outer wall of the second rotating disc (67).

3. The industrial-grade graphene oxide production device according to claim 2, wherein: the outer walls of the two sides of the front side, which is contacted with the second rotating disc (67), of the rotating rod (61) are planes.

4. The industrial-grade graphene oxide production device according to claim 2, wherein: the inner side of the limiting clamping block (69) is spherical.

5. The industrial-grade graphene oxide production device according to claim 2, wherein: still be provided with in the inner chamber of protection cauldron (2):

the two connecting seats (9) are respectively connected to the bottom ends of the lifting rods (68) in a rotating mode through pin shafts;

the reaction kettle (10), the reaction kettle (10) is fixedly connected to the inner sides of the two fixing seats (3);

the electromagnetic valve (11), the electromagnetic valve (11) is fixedly arranged at the middle position of the bottom end of the reaction kettle (10);

one end of the liquid leakage pipe (12) is fixedly connected to the left side of the bottom end of the inner cavity of the protective kettle (2), and the other end of the liquid leakage pipe (12) is connected to the upper part of the middle part of the liquid discharge pipe (14);

the corrugated pipe (13), the fixed connection of the said corrugated pipe (13) is between said electromagnetic valve (11) and said drain pipe (14);

stirring fan blade (15), a plurality of stirring fan blade (15) are the slope form and along circumference fixed connection in the bottom outer wall outside of rotary rod (61), and are located in the inner chamber of reation kettle (10).

6. The industrial-grade graphene oxide production device according to claim 5, wherein: and a certain gap is reserved between the edge of the stirring fan blade (15) and the inner wall of the reaction kettle (10).