CN214106952U - Tributyl phosphate three-phase stirring reaction kettle - Google Patents

Tributyl phosphate three-phase stirring reaction kettle Download PDF

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Publication number
CN214106952U
CN214106952U CN202023009002.7U CN202023009002U CN214106952U CN 214106952 U CN214106952 U CN 214106952U CN 202023009002 U CN202023009002 U CN 202023009002U CN 214106952 U CN214106952 U CN 214106952U
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box
work box
heat preservation
heating
tributyl phosphate
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CN202023009002.7U
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Chinese (zh)
Inventor
何飞
郑维维
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Jiangsu Poly Pharmaceutical Co ltd
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Jiangsu Poly Pharmaceutical Co ltd
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Abstract

The utility model discloses a tributyl phosphate three-phase stirring reation kettle, including work box and supporting leg, the work box is installed on the top of supporting leg, the internally mounted of heating box has the miscellaneous net of straining, the heater strip is all installed to the both sides on heating box top, the feed opening is installed to one side of work box bottom end, one side of work box inside is provided with insulation construction. The utility model discloses a carry out certain installation earlier with the incubator and handle, then open the admission valve and make its air current begin to flow after, after its air current gets into the inside of incubator, make it carry out certain miscellaneous processing of straining through straining miscellaneous net earlier, the air current after the processing rises gradually and carries out certain intensification processing under the effect of heater strip, the inside of work box is introduced to the air current after will intensifing under the water conservancy diversion of honeycomb duct, thereby fine improvement the temperature of its inside work, so as to improve holistic reaction efficiency.

Description

Tributyl phosphate three-phase stirring reaction kettle
Technical Field
The utility model relates to an adapting unit technical field specifically is a tributyl phosphate three-phase stirring reation kettle.
Background
With the continuous development of society and the continuous improvement of economic level, the chemical level of people is also gradually improved, wherein tributyl phosphate is an organic compound, is a colorless and odorous liquid, mainly acts as a solvent, and is often required to be processed and reacted by a reaction kettle in the process of processing various things;
however, the conventional reaction kettle still has problems in use, such as low working efficiency in use, and poor reaction capability in working engineering.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a tributyl phosphate three-phase stirring reation kettle to solve the problem that proposes work efficiency low among the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: a tributyl phosphate three-phase stirring reaction kettle comprises a working box and supporting legs, wherein the working box is installed at the top end of the supporting legs, feed inlets are installed on two sides of the top end of the working box, heating structures are arranged on two sides of the working box respectively, each heating structure comprises a heating box, heating wires, a sundry filtering net, an air inlet valve and a guide pipe, the heating box is installed on one side of the working box, the air inlet valves are installed at the bottom end of the heating box, the guide pipe is connected to the top end of the heating box, the sundry filtering net is installed inside the heating box, the heating wires are installed on two sides of the top end of the heating box respectively, a driving motor is installed at the middle position of the top end of the working box, a driving shaft is installed at the bottom end of the driving motor, stirring blades are fixed on two sides of the driving shaft respectively, a wall scraping structure is arranged on one side of each stirring blade, and a discharging port is installed on one side of the bottom end of the working box, and a heat insulation structure is arranged on one side of the interior of the working box.
Preferably, the draft tube extends to the inside of the working box, and the heating wires are symmetrically distributed in the inside of the heating box about a vertical central axis of the heating box.
Preferably, scrape the wall structure and include connecting plate, mounting panel and scrape the wall blade, the one side at the stirring leaf is installed to the connecting plate, the mounting panel is installed to one side of connecting plate, and one side of mounting panel is installed and is scraped the wall blade.
Preferably, the outer side wall of the wall scraping blade is serrated, and the mounting plate is embedded in the connecting plate.
Preferably, insulation construction includes heat preservation chamber, reservation chamber, heat preservation cotton and heating element, the heat preservation chamber is installed in one side of work box inside, the intermediate position department of heat preservation intracavity portion is filled there is the heat preservation cotton, the cotton both sides of heat preservation all are provided with the reservation chamber, and the internally mounted in reservation chamber has heating element.
Preferably, the heating components are arranged in the reserved cavity at equal intervals, and the reserved cavity is symmetrically distributed about the vertical central axis of the heat preservation cavity.
Compared with the prior art, the beneficial effects of the utility model are that: the tributyl phosphate three-phase stirring reaction kettle not only improves the working efficiency of the reaction kettle, but also improves the heat preservation capability and the wall scraping cleaning capability of the device;
(1) the temperature raising box is firstly subjected to certain installation treatment, then the air inlet valve is opened, the air flow starts to flow, after the air flow enters the interior of the temperature raising box, the air flow is firstly subjected to certain impurity filtering treatment through the impurity filtering net, the treated air flow gradually rises under the action of the heating wire for certain temperature raising treatment, and the heated air flow is introduced into the interior of the working box under the flow guidance of the flow guide pipe, so that the working temperature in the working box is well improved, and the integral reaction efficiency is improved;
(2) the heat preservation cavity is firstly installed, then the heat preservation cotton in the heat preservation cavity is filled, so that certain heat preservation capacity is improved, and after the reserved cavity is installed, a heating assembly is installed in the reserved cavity, so that certain heating capacity is provided, the heat in the reserved cavity is not easy to dissipate, and the whole heat preservation capacity is improved;
(3) after the connecting plate is installed, the driving motor is opened to drive the driving shaft to rotate, the stirring blades are driven to move synchronously in the rotating process, the connecting plate is driven to rotate synchronously, and the wall scraping blade is fixedly installed on the inner side wall of the working box in the rotating process to scrape the wall to a certain extent, so that the integral wall scraping capacity is improved.
Drawings
Fig. 1 is a schematic front view of a cross-sectional structure of the present invention;
fig. 2 is a schematic rear view of the present invention;
fig. 3 is an enlarged partial sectional view of the utility model at a in fig. 1;
fig. 4 is a schematic side view of the thermal insulation structure of the present invention.
In the figure: 1. a work box; 2. a feed inlet; 3. a drive motor; 4. a drive shaft; 5. a temperature rising structure; 501. a temperature raising box; 502. heating wires; 503. filtering the impurity net; 504. an intake valve; 505. a flow guide pipe; 6. a wall scraping structure; 601. a connecting plate; 602. mounting a plate; 603. a wall scraping blade; 7. stirring blades; 8. supporting legs; 9. a feeding port; 10. a heat preservation structure; 1001. a heat preservation cavity; 1002. reserving a cavity; 1003. heat preservation cotton; 1004. and a heating assembly.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-4, the present invention provides an embodiment: the utility model provides a tributyl phosphate three-phase stirring reation kettle, includes work box 1 and supporting leg 8, its characterized in that: the top end of the supporting leg 8 is provided with a working box 1, both sides of the top end of the working box 1 are provided with feed inlets 2, both sides of the working box 1 are provided with heating structures 5, each heating structure 5 comprises a heating box 501, a heating wire 502, a sundry filtering net 503, an air inlet valve 504 and a guide pipe 505, the heating box 501 is arranged on one side of the working box 1, the bottom end of the heating box 501 is provided with the air inlet valve 504, the top end of the heating box 501 is connected with the guide pipe 505, the sundry filtering net 503 is arranged in the heating box 501, and both sides of the top end of the heating box 501 are provided with the heating wires 502;
the draft tube 505 extends to the inside of the working box 1, and the heating wires 502 are symmetrically distributed in the heating box 501 about the vertical central axis of the heating box 501;
firstly, certain installation treatment is carried out on the heating box 501, then the air inlet valve 504 is opened to enable the air flow to start flowing, after the air flow enters the interior of the heating box 501, the air flow is firstly subjected to certain impurity filtering treatment through the impurity filtering net 503, the treated air flow gradually rises to carry out certain heating treatment under the action of the heating wire 502, and the heated air flow is guided into the interior of the working box 1 under the flow guidance of the guide pipe 505;
a driving motor 3 is installed in the middle of the top end of the working box 1, a driving shaft 4 is installed at the bottom end of the driving motor 3, stirring blades 7 are fixed on two sides of the driving shaft 4, and a wall scraping structure 6 is arranged on one side of each stirring blade 7;
the wall scraping structure 6 comprises a connecting plate 601, a mounting plate 602 and a wall scraping blade 603, wherein the connecting plate 601 is mounted on one side of the stirring blade 7, the mounting plate 602 is mounted on one side of the connecting plate 601, the wall scraping blade 603 is mounted on one side of the mounting plate 602, the outer side wall of the wall scraping blade 603 is in a sawtooth shape, and the mounting plate 602 is embedded in the connecting plate 601;
mounting the connecting plate 601, opening the driving motor 3 to drive the driving shaft 4 to start rotating, driving the stirring blades 7 to synchronously move in the rotating process, and driving the connecting plate 601 to synchronously rotate;
a feed opening 9 is installed on one side of the bottom end of the working box 1, a heat insulation structure 10 is arranged on one side inside the working box 1, the heat insulation structure 10 comprises a heat insulation cavity 1001, a reserved cavity 1002, heat insulation cotton 1003 and a heating assembly 1004, the heat insulation cavity 1001 is installed on one side inside the working box 1, the heat insulation cotton 1003 is filled in the middle position inside the heat insulation cavity 1001, the reserved cavity 1002 is arranged on each of two sides of the heat insulation cotton 1003, and the heating assembly 1004 is installed inside the reserved cavity 1002;
the heating components 1004 are arranged in the reserved cavity 1002 at equal intervals, and the reserved cavity 1002 is symmetrically distributed about the vertical central axis of the heat preservation cavity 1001;
after reaction is carried out inside, the heat preservation cavity 1001 is installed firstly, then certain heat preservation capacity is improved after heat preservation cotton 1003 in the cavity is filled, and after the reserved cavity 1002 is installed, certain temperature rise capacity is provided after the heating component 1004 is installed in the reserved cavity, so that the heat in the cavity is kept not easy to dissipate.
The working principle is as follows: firstly, after the whole device is externally connected with a power supply, the device starts to normally work, then raw materials are led into the working box 1 from the feeding hole 2, then the heating box 501 is subjected to certain installation treatment firstly, then the air inlet valve 504 is opened to enable the air flow to start flowing, after the air flow enters the inside of the heating box 501, the air flow is subjected to certain impurity filtering treatment through the impurity filtering net 503, the treated air flow gradually rises under the action of the heating wire 502 to carry out certain temperature rise treatment, and the heated air flow is led into the inside of the working box 1 under the flow guidance of the flow guide pipe 505;
then, in the reaction process, the connecting plate 601 is installed, the driving motor 3 is turned on to drive the driving shaft 4 to start rotating, the stirring blades 7 are driven to synchronously move in the rotating process, and the connecting plate 601 is driven to synchronously rotate, and as the wall scraping blades 603 are fixedly installed in the rotating process, certain wall scraping treatment is performed on the inner side wall of the working box 1;
finally, after the reaction is carried out inside, the heat preservation cavity 1001 is firstly installed, then the heat preservation cotton 1003 in the cavity is filled to improve certain heat preservation capacity, and after the reserved cavity 1002 is installed, the heating assembly 1004 is installed in the reserved cavity to provide certain heating capacity, so that the heat in the cavity is not easy to dissipate, certain reaction efficiency is guaranteed, and finally the processed raw materials are subjected to blanking treatment from the blanking port 9.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Claims (6)

1. The utility model provides a tributyl phosphate three-phase stirring reation kettle, includes work box (1) and supporting leg (8), its characterized in that: work box (1) is installed on the top of supporting leg (8), feed inlet (2) are all installed to the both sides on work box (1) top, the both sides of work box (1) all are provided with intensification structure (5), intensification structure (5) are including warming box (501), heater strip (502), miscellaneous net of straining (503), admission valve (504) and honeycomb duct (505), one side at work box (1) is installed in warming box (501), admission valve (504) are installed to the bottom of warming box (501), the top of warming box (501) is connected with honeycomb duct (505), the internally mounted of warming box (501) has miscellaneous net of straining (503), heater strip (502) are all installed to the both sides on warming box (501) top, driving motor (3) are installed to the intermediate position department on work box (1) top, and driving motor (3)'s bottom installs drive shaft (4), the both sides of drive shaft (4) all are fixed with stirring leaf (7), one side of stirring leaf (7) all is provided with scrapes wall structure (6), feed opening (9) are installed to one side of work box (1) bottom, the inside one side of work box (1) is provided with insulation construction (10).
2. The tributyl phosphate three-phase stirring reaction kettle according to claim 1, characterized in that: the draft tube (505) extends to the inside of the working box (1), and the heating wires (502) are symmetrically distributed in the heating box (501) about the vertical central axis of the heating box (501).
3. The tributyl phosphate three-phase stirring reaction kettle according to claim 1, characterized in that: scrape wall structure (6) including connecting plate (601), mounting panel (602) and scrape wall blade (603), install the one side at stirring leaf (7) connecting plate (601), mounting panel (602) are installed to one side of connecting plate (601), and one side of mounting panel (602) is installed and is scraped wall blade (603).
4. The tributyl phosphate three-phase stirring reaction kettle according to claim 3, characterized in that: the outer side wall of the wall scraping blade (603) is in a sawtooth shape, and the mounting plate (602) is embedded in the connecting plate (601).
5. The tributyl phosphate three-phase stirring reaction kettle according to claim 1, characterized in that: insulation construction (10) include heat preservation chamber (1001), reserve chamber (1002), heat preservation cotton (1003) and heating element (1004), install in the inside one side of work box (1) heat preservation chamber (1001), the inside intermediate position department in heat preservation chamber (1001) is filled there is heat preservation cotton (1003), the both sides of heat preservation cotton (1003) all are provided with reserve chamber (1002), and the internally mounted who reserves chamber (1002) has heating element (1004).
6. The tributyl phosphate three-phase stirring reaction kettle according to claim 5, characterized in that: the heating components (1004) are arranged in the reserved cavity (1002) at equal intervals, and the reserved cavity (1002) is symmetrically distributed about the vertical middle axis of the heat preservation cavity (1001).
CN202023009002.7U 2020-12-14 2020-12-14 Tributyl phosphate three-phase stirring reaction kettle Active CN214106952U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202023009002.7U CN214106952U (en) 2020-12-14 2020-12-14 Tributyl phosphate three-phase stirring reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202023009002.7U CN214106952U (en) 2020-12-14 2020-12-14 Tributyl phosphate three-phase stirring reaction kettle

Publications (1)

Publication Number Publication Date
CN214106952U true CN214106952U (en) 2021-09-03

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115518408A (en) * 2022-11-08 2022-12-27 山东坤宝新材料集团股份有限公司 Scraper catcher for anhydrous aluminum trichloride production and method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115518408A (en) * 2022-11-08 2022-12-27 山东坤宝新材料集团股份有限公司 Scraper catcher for anhydrous aluminum trichloride production and method
CN115518408B (en) * 2022-11-08 2024-04-26 山东坤宝新材料集团股份有限公司 Scraper catcher and method for anhydrous aluminum trichloride production

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