CN214106001U - Pyrimidine compound temperature-adjustable positive pressure filtering device - Google Patents

Pyrimidine compound temperature-adjustable positive pressure filtering device Download PDF

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Publication number
CN214106001U
CN214106001U CN202022096300.8U CN202022096300U CN214106001U CN 214106001 U CN214106001 U CN 214106001U CN 202022096300 U CN202022096300 U CN 202022096300U CN 214106001 U CN214106001 U CN 214106001U
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China
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filter
positive pressure
tank body
heat preservation
temperature
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CN202022096300.8U
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Chinese (zh)
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宗玺
于文渊
胡海燕
吉民
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Jiangsu Dongnan Nano Material Co ltd
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Jiangsu Dongnan Nano Material Co ltd
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Abstract

The utility model discloses a positive pressure filtering device capable of adjusting temperature for pyrimidine compounds, which comprises a compressed gas container, a positive pressure filter and a high-low temperature circulator, wherein the gas outlet of the compressed gas container is connected with the filtering inlet at the top of the positive pressure filter through a pipeline, the positive pressure filter comprises a filter tank body, a filter membrane or filter paper and a filter bottom, and the inner wall or the outer wall of the filter tank body is provided with a heat-insulating jacket; the filter tank body is connected with the bottom of the filter through a flange, and a gasket for sealing is arranged between the filter tank body and the bottom of the filter; the upper part of the bottom of the filter is provided with a support frame, the filter membrane or the filter paper is positioned on the support frame, and a filter outlet is arranged below the bottom of the filter. The device can accurately control the temperature inside the filter tank body through the high-low temperature circulator and the heat-preservation jacket in the positive pressure filtering process, so that the whole filtering process is kept in a rated constant temperature state, and the device is particularly suitable for substances which are sensitive to temperature, such as pyrimidine compounds and the like.

Description

Pyrimidine compound temperature-adjustable positive pressure filtering device
Technical Field
The utility model belongs to the filtration equipment field, concretely relates to malleation filter equipment of but pyrimidine class compound temperature regulation.
Background
The filtration is an operation of separating solid and other substances from liquid (or gas) by making the liquid (or gas) in suspension (or solid particle-containing heating gas) permeate through the medium and making the solid particles and other substances be retained by the filter medium under the action of a driving force or other external forces. Filtration is typically carried out in various filtration devices.
During or after the chemical reaction, it is usually necessary to post-treat it with a filtration device. However, the existing filtering device is usually operated at normal temperature, and when liquid needing hot filtration is filtered, because the filtering device treats the normal temperature state, the compound is easy to generate crystallization phenomenon in the filtering process, thereby not only affecting the yield of the product, but also affecting the filtering effect. When some low-temperature or extremely low-temperature liquids are filtered, the filtering device still treats the normal temperature state, so that the compounds are extremely easy to damage in the filtering process, and the product quality is influenced.
Disclosure of Invention
The utility model aims at overcoming the above-mentioned problem, provide a malleation filter equipment of adjustable temperature of pyrimidine class compound.
The technical scheme of the utility model is that:
a positive pressure filtering device capable of adjusting temperature for pyrimidine compounds comprises a compressed gas container, a positive pressure filter and a high-low temperature circulating machine, wherein a gas outlet of the compressed gas container is connected with a filtering inlet at the top of the positive pressure filter through a pipeline, the positive pressure filter comprises a filter tank body, a filter membrane or filter paper and a filter bottom, a heat-insulating jacket is arranged on the inner wall or the outer wall of the filter tank body, a heat-insulating medium inlet and a heat-insulating medium outlet which are communicated with the inside of the heat-insulating jacket are respectively arranged below and above the filter tank body, and a circulating medium inlet and a circulating medium outlet of the high-low temperature circulating machine are respectively connected with the heat-insulating medium inlet and the heat-insulating medium outlet through pipelines; the filter tank body is connected with the bottom of the filter through a flange, and a gasket for sealing is arranged between the filter tank body and the bottom of the filter; the upper part of the bottom of the filter is provided with a support frame, the filter membrane or the filter paper is positioned on the support frame, and a filter outlet is arranged below the bottom of the filter.
In one scheme, an upper flange is arranged at the lower edge of a filter tank body, a lower flange is arranged at the upper edge of the bottom of the filter, a plurality of fixing columns are arranged on the lower flange, connecting holes corresponding to the fixing columns are formed in the upper flange, and fixing devices used for fixing the upper flange and the lower flange are arranged at the tops of the fixing columns.
In another arrangement, a plurality of brackets are provided on the filter base.
In one scheme, the main body part of the bottom of the filter is in an inverted cone shape and sequentially comprises a support frame, a cavity at the bottom of the filter and a filtering outlet from top to bottom.
In another scheme, a circulating medium outlet of the high-low temperature circulating machine is connected with the heat preservation medium inlet through a pipeline, and a circulating medium inlet of the high-low temperature circulating machine is connected with the heat preservation medium outlet through a pipeline.
The utility model has the advantages that: the filtering device can accurately control the temperature inside the filter tank body through the high-low temperature circulator and the heat-preservation jacket in the positive pressure filtering process, so that the whole filtering process is kept in a rated constant temperature state, and the filtering device is particularly suitable for substances which are sensitive to temperature, such as pyrimidine compounds and the like. This device can make the filtration process go on under high temperature, also can make the filtration process go on at low temperature, can match the temperature of treating the filtrate or the required temperature of technology completely, has avoided the filtration process to produce adverse effect to whole experiment or production flow.
Drawings
Fig. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic structural diagram of the positive pressure filter of the present invention;
FIG. 3 is a schematic view of an assembly of the positive pressure filter of the present invention;
in the figure, 1-positive pressure filter, 2-compressed gas container, 3-high and low temperature circulator, 11-filtering inlet, 12-filter tank, 13-heat preservation jacket, 14-fixing device, 15-upper flange, 16-connecting hole, 17-gasket, 18-filter membrane or filter paper, 19-lower flange, 20-fixing column, 21-bracket, 22-filter bottom, 23-heat preservation medium outlet and 24-heat preservation medium inlet.
Detailed Description
The present invention will be further described with reference to the accompanying drawings and examples.
As shown in the figure, the positive pressure filtering device capable of adjusting the temperature of the pyrimidine compounds comprises a compressed gas container 2, a positive pressure filter 1 and a high-low temperature circulator 3. Wherein, the compressed gas container 2 contains compressed gas or is connected with an external compressor for storing the compressed gas; the air outlet of the compressed gas container 2 is connected with a filtering inlet 11 at the top of the positive pressure filter 1 through a pipeline to provide positive pressure for the filtering device.
The positive pressure filter includes a filter canister 12, a filter membrane or paper 18, and a filter bottom 22. Wherein the inner wall or the outer wall of the filter tank body 12 is provided with a heat preservation jacket 13, a heat preservation medium inlet and a heat preservation medium outlet which are communicated with the interior of the heat preservation jacket are respectively arranged below and above the filter tank body, and a circulating medium inlet and a circulating medium outlet of the high-low temperature circulator are respectively connected with the heat preservation medium inlet and the heat preservation medium outlet through pipelines; furthermore, a circulating medium outlet of the high-low temperature circulating machine is connected with the heat preservation medium inlet through a pipeline, and a circulating medium inlet of the high-low temperature circulating machine is connected with the heat preservation medium outlet through a pipeline.
The filter tank body 12 is connected with the filter bottom 22 through a flange, an upper flange 15 is arranged on the lower edge of the filter tank body 12, a lower flange 19 is arranged on the upper edge of the filter bottom 22, a plurality of fixing columns 20 are arranged on the lower flange 19, connecting holes 16 corresponding to the fixing columns 20 are formed in the upper flange 15, and the fixing columns 20 penetrate into the connecting holes 16 when the upper flange and the lower flange are connected. On top of the fixing post 20, there is provided a fixing means 14, such as a nut, a bolt, etc., for fixing the upper and lower flanges.
A gasket 17 for sealing is provided between the filter tank 12 and the filter bottom 22.
The main body of the filter bottom 22 is in the shape of an inverted cone, and the filter bottom comprises a support frame, a filter bottom cavity and a filter outlet from top to bottom in sequence. Namely, the support frame is arranged at the upper part of the bottom of the filter, the filter membrane or the filter paper is arranged on the support frame, and the filtering outlet is arranged below the bottom of the filter. The bottom of the filter is provided with a plurality of brackets for supporting the positive pressure filter.
When the device is used, the positive pressure filter tank body 12 and the filter bottom 22 are assembled, the filter membrane or the filter paper 18 is put in the assembling process, the high-low temperature circulator 3 is switched on to maintain the interior of the filter tank body 12 at a preset temperature, then the solution to be filtered is poured in through the filtering inlet 11 at the top of the positive pressure filter 1, and then the solution to be filtered is connected with the compressed gas container 2 through the filtering inlet 11 for heat preservation and positive pressure filtration. The filtrate flows out of the filtration outlet of the filter bottom 22.

Claims (5)

1. A positive pressure filtering device capable of adjusting temperature for pyrimidine compounds is characterized by comprising a compressed gas container (2), a positive pressure filter (1) and a high-low temperature circulator (3), the air outlet of the compressed gas container (2) is connected with a filtering inlet (11) at the top of the positive pressure filter (1) through a pipeline, the positive pressure filter (1) comprises a filter tank body (12), a filter membrane or filter paper (18) and a filter bottom (22), a heat-insulating jacket (13) is arranged on the inner wall or the outer wall of the filter tank body (12), a heat preservation medium inlet (24) and a heat preservation medium outlet (23) which are communicated with the interior of the heat preservation jacket (13) are respectively arranged below and above the filter tank body (12), a circulating medium inlet and a circulating medium outlet of the high-low temperature circulator (3) are respectively connected with the heat preservation medium inlet (24) and the heat preservation medium outlet (23) through pipelines; the filter tank body (12) is connected with the filter bottom (22) through a flange, and a gasket (17) for sealing is arranged between the filter tank body and the filter bottom; the upper part of the filter bottom (22) is provided with a support frame, the filter membrane or the filter paper (18) is positioned on the support frame, and a filter outlet is arranged below the filter bottom (22).
2. The positive pressure filtration device capable of adjusting the temperature of pyrimidine compounds according to claim 1, wherein an upper flange (15) is arranged at the lower edge of the filter tank body (12), a lower flange (19) is arranged at the upper edge of the filter bottom (22), a plurality of fixing posts (20) are arranged on the lower flange (19), connecting holes (16) corresponding to the fixing posts (20) are arranged on the upper flange (15), and a fixing device (14) for fixing the upper flange (15) and the lower flange (19) is arranged at the top of the fixing posts (20).
3. A temperature regulated positive pressure filtration device of pyrimidine compounds according to claim 1 characterised in that a plurality of brackets (21) are provided on the filter base (22).
4. The positive pressure filtration device capable of adjusting the temperature of pyrimidine compounds according to claim 1, wherein the main body of the filter bottom (22) is in an inverted cone shape, and the filter bottom comprises a support frame, a filter bottom cavity and a filtration outlet from top to bottom.
5. The positive pressure filtration device capable of adjusting the temperature of pyrimidine compounds according to claim 1, wherein the circulating medium outlet of the high and low temperature circulator (3) is connected with the heat preservation medium inlet (24) through a pipeline, and the circulating medium inlet of the high and low temperature circulator (3) is connected with the heat preservation medium outlet (23) through a pipeline.
CN202022096300.8U 2020-09-22 2020-09-22 Pyrimidine compound temperature-adjustable positive pressure filtering device Active CN214106001U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202022096300.8U CN214106001U (en) 2020-09-22 2020-09-22 Pyrimidine compound temperature-adjustable positive pressure filtering device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202022096300.8U CN214106001U (en) 2020-09-22 2020-09-22 Pyrimidine compound temperature-adjustable positive pressure filtering device

Publications (1)

Publication Number Publication Date
CN214106001U true CN214106001U (en) 2021-09-03

Family

ID=77497288

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202022096300.8U Active CN214106001U (en) 2020-09-22 2020-09-22 Pyrimidine compound temperature-adjustable positive pressure filtering device

Country Status (1)

Country Link
CN (1) CN214106001U (en)

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