CN213995837U - Novel reation kettle is used in material preparation - Google Patents
Novel reation kettle is used in material preparation Download PDFInfo
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- CN213995837U CN213995837U CN202022151768.2U CN202022151768U CN213995837U CN 213995837 U CN213995837 U CN 213995837U CN 202022151768 U CN202022151768 U CN 202022151768U CN 213995837 U CN213995837 U CN 213995837U
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- reation kettle
- fixedly connected
- pipe
- ultrasonic wave
- wave generating
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- 239000000463 material Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 238000006243 chemical reaction Methods 0.000 claims abstract description 45
- 238000003756 stirring Methods 0.000 claims description 12
- 238000007599 discharging Methods 0.000 claims description 9
- 238000007790 scraping Methods 0.000 claims description 5
- 239000002086 nanomaterial Substances 0.000 abstract description 7
- 230000009977 dual effect Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000002105 nanoparticle Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- 239000011858 nanopowder Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000011882 ultra-fine particle Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011236 particulate material Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 230000005641 tunneling Effects 0.000 description 1
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Abstract
The utility model discloses a novel reation kettle is used in material preparation, including reation kettle, reation kettle's middle part upper end fixedly connected with device box, reation kettle's middle part upper end fixedly connected with motor, reation kettle's upper end and the fixedly connected with second atomizer in the both sides department of device box, one side of second atomizer is provided with the second atomizing pipe, the first atomizer of reation kettle's lower extreme both sides fixedly connected with, one side of first atomizing pipe is provided with the atomizer, reation kettle's lateral wall is provided with first ultrasonic wave generating tube, reation kettle's lateral wall and keep away from first ultrasonic wave generating tube department and be provided with second ultrasonic wave generating tube, first ultrasonic wave generating tube is provided with the control panel with one side of second ultrasonic wave generating tube. The utility model discloses in, reation kettle sets up dual atomizing device and ultrasonic wave generating device, can make the nano-material reaction complete.
Description
Technical Field
The utility model relates to a reation kettle field especially relates to a novel reation kettle is used in material preparation.
Background
The nano-scale structural material in China is referred to as nano-material (nanometerial), which means that the size of the structural unit is between 1 nanometer and 100 nanometers. Since its size is already close to the coherence length of the electrons, its properties vary greatly due to self-organization by strong coherence. Moreover, its dimensions are close to the wavelength of light, plus it has the special effect of a large surface, so that its properties, such as melting point, magnetic, optical, thermal, electrical conductivity, etc., are often different from the properties that the substance exhibits in its bulk state.
Nanoparticle materials, also known as ultrafine particulate materials, are composed of nanoparticles (nanoparticles). Nanoparticles are also called as ultrafine particles, generally refer to particles with the size of 1-100 nm, and are located in a transition region between an atomic cluster and a macroscopic object, and from the general point of view of microcosmic and macroscopic view, the system is not a typical microcosmic system or a typical macroscopic system, and is a typical mesoscopic system, and has a surface effect, a small-size effect and a macroscopic quantum tunneling effect. When a macroscopic object is subdivided into ultrafine particles (nanoscale), it will exhibit a number of unusual characteristics, namely its optical, thermal, electrical, magnetic, mechanical and chemical properties, which are significantly different from those of a bulk solid.
The particles of the nano material are very easy to agglomerate to cause the enlargement of the particles because of small particle size, large surface atom proportion, large specific area and large surface energy and are in an energy unstable state. The agglomeration of the nano powder is a phenomenon that the original nano powder particles are connected with each other in the processes of preparation, separation, treatment and storage, and a large particle cluster is formed by a plurality of particles. When the existing device is used for preparing nano materials, the general reaction device reduces the growth of particles in a mechanical stirring mode, only improves local agglomeration, but the overall effect is not very ideal
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects existing in the prior art and providing a novel reaction kettle for material preparation.
In order to achieve the above purpose, the utility model adopts the following technical scheme: a reaction kettle for preparing a novel material comprises a reaction kettle, wherein a device box is fixedly connected to the upper middle end of the reaction kettle, a motor is fixedly connected to the upper middle end of the reaction kettle and arranged inside the device box, two second atomizing machines are fixedly connected to the upper end of the reaction kettle and on two sides of the device box, a second atomizing pipe is arranged on one side of each second atomizing machine, and the second atomizing pipes penetrate through the reaction kettle;
two sides of the lower end of the reaction kettle are fixedly connected with first atomizers, one side of each first atomizer is provided with a first atomizing pipe, one side of each first atomizing pipe is provided with four atomizing nozzles, and the number of the atomizing nozzles is four;
the lateral wall of reation kettle is provided with first ultrasonic wave generating pipe, reation kettle's lateral wall just keeps away from first ultrasonic wave generating pipe department and is provided with second ultrasonic wave generating pipe, one side of first ultrasonic wave generating pipe and second ultrasonic wave generating pipe is provided with the control panel.
As a further description of the above technical solution:
the one end extension department of motor is provided with motor shaft, motor shaft's lateral wall fixedly connected with first fixed column, the lateral wall of first fixed column and the inner wall department fixedly connected with doctor-bar that is close to reation kettle, motor shaft's lower extreme lateral wall fixedly connected with stirring board.
As a further description of the above technical solution:
the inner wall of the reaction kettle is fixedly connected with a second fixing column.
As a further description of the above technical solution:
the reactor is characterized in that an inlet pipe is arranged on one side of the upper end of the reactor, and an inlet pipe is arranged on the other side of the upper end of the reactor.
As a further description of the above technical solution:
the middle part lower extreme of reation kettle is provided with the discharging pipe, the lateral wall of discharging pipe is provided with first ooff valve, reation kettle's lower extreme one side is provided with the outlet pipe, the lateral wall of outlet pipe is provided with the second ooff valve.
As a further description of the above technical solution:
the inner wall of the lower end of the reaction kettle is fixedly connected with an auxiliary rod close to the first atomizing pipe.
As a further description of the above technical solution:
the lower extreme fixedly connected with support column of reation kettle, and the quantity of support column is three.
As a further description of the above technical solution:
the number of the second fixing columns is four, and the two second fixing columns are fixedly connected to the upper side and the lower side of the scraping blade respectively.
As a further description of the above technical solution:
the auxiliary rod is arranged on the inner side of the first atomizing pipe.
As a further description of the above technical solution:
the stirring plate is arranged on the inner side of the auxiliary rod.
The utility model discloses following beneficial effect has:
1. the utility model discloses be provided with two atomizing devices, coact in raw and other materials, prevent raw and other materials reunion, make raw and other materials intensive mixing.
2. The lateral wall of device is provided with two-layer ultrasonic wave generating pipe, utilizes the ultrasonic wave to make the raw materials can disperse more evenly and thoroughly, through the stirring of inside (mixing) shaft, intensive mixing raw and other materials.
3. The utility model discloses an upper end is provided with the outlet pipe that inlet tube and lower extreme set up, can carry out reation kettle's clearance through inlet tube and outlet pipe, guarantees reation kettle's totally.
Drawings
FIG. 1 is a sectional view of a reaction vessel for preparing a novel material, which is provided by the utility model;
FIG. 2 is a front view of a reaction vessel for preparing a novel material provided by the present invention;
FIG. 3 is a top view of a novel material preparation reaction kettle provided by the present invention;
fig. 4 is a bottom view of the reaction kettle for preparing the novel material provided by the utility model.
Illustration of the drawings:
1. a feed pipe; 2. a first atomization tube; 3. an atomizing spray head; 4. a first atomizer; 5. a support pillar; 6. A discharge pipe; 7. a first on-off valve; 8. a second on-off valve; 9. a water outlet pipe; 10. scraping a blade; 11. a first ultrasonic wave generating tube; 12. a motor shaft; 13. a water inlet pipe; 14. a second atomizer; 15. a device cartridge; 16. an electric motor; 17. a second atomization tube; 18. a control panel; 19. a second ultrasonic wave generating tube; 20. A stirring plate; 21. a first fixed column; 22. a reaction kettle; 23. an auxiliary rod; 24. and a second fixing column.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus, should not be construed as limiting the present invention; the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance, and furthermore, unless otherwise explicitly stated or limited, the terms "mounted," "connected," and "connected" are to be construed broadly and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-4, the present invention provides an embodiment: a novel material preparation reaction kettle comprises a reaction kettle 22, wherein a device box 15 is fixedly connected to the upper end of the middle of the reaction kettle 22, a motor 16 is fixedly connected to the upper end of the middle of the reaction kettle 22, the motor 16 is arranged inside the device box 15, a motor shaft 12 is arranged at the extending position of one end of the motor 16, a first fixed column 21 is fixedly connected to the side wall of the motor shaft 12, a scraping blade 10 is fixedly connected to the side wall of the first fixed column 21 and the inner wall of the reaction kettle 22, a stirring plate 20 is fixedly connected to the side wall of the lower end of the motor shaft 12, the motor shaft 12 can be rotated by the rotation of the motor 16, and the first fixed column 21 and the stirring plate 20 arranged on the side wall of the other end of the motor shaft 12 are driven to rotate together;
the upper end of the reaction kettle 22 and the two sides of the device box 15 are fixedly connected with two second atomizers 14, the number of the second atomizers 14 is two, one side of the second atomizers 14 is provided with a second atomizing pipe 17, the second atomizing pipe 17 penetrates through the reaction kettle 22, and the second atomizers 14 work and can atomize into the reaction kettle 22 through the second atomizing pipe 17;
the two sides of the lower end of the reaction kettle 22 are fixedly connected with first atomizers 4, one side of each first atomizer 4 is provided with a first atomizing pipe 2, one side of each first atomizing pipe 2 is provided with an atomizing nozzle 3, the number of the atomizing nozzles 3 is four, the first atomizers 4 work, the first atomizing pipes 2 spray out the atomizing nozzles 3 to atomize nanotechnology, the side wall of the reaction kettle 22 is provided with a first ultrasonic wave generating pipe 11, the side wall of the reaction kettle 22, far away from the first ultrasonic wave generating pipe 11, is provided with a second ultrasonic wave generating pipe 19, one side of each first ultrasonic wave generating pipe 11 and one side of each second ultrasonic wave generating pipe 19 are provided with a control panel 18, and the control panels 18 control the first ultrasonic wave generating pipe 11 and the second ultrasonic wave generating pipe 19 to crush the nanometer materials in the reaction kettle 22;
a second fixing column 24 is fixedly connected to the inner wall of the reaction kettle 22, a feeding pipe 1 is arranged on one side of the upper end of the reaction kettle 22, the feeding pipe 1 can convey nano materials into the reaction kettle 22, a water inlet pipe 13 is arranged on the other side of the upper end of the reaction kettle 22, a discharging pipe 6 is arranged on the lower end of the middle of the reaction kettle 22, the discharging pipe 6 can output prepared nano materials, a first switch valve 7 is arranged on the side wall of the discharging pipe 6, a water outlet pipe 9 is arranged on one side of the lower end of the reaction kettle 22, a second switch valve 8 is arranged on the side wall of the water outlet pipe 9, an auxiliary rod 23 is fixedly connected to the inner wall of the lower end of the reaction kettle 22 and close to the first atomizing pipe 2, support columns 5 are fixedly connected to the lower end of the reaction kettle 22, the number of the support columns 5 is three, the auxiliary rods 23 are arranged on the inner side of the first atomizing pipe 2, a stirring plate 20 is arranged on the inner side of the auxiliary rod 23, the auxiliary rod 23 and the second fixing column 24 can jointly act with a stirring shaft, the raw materials were stirred well.
The working principle is as follows: send into raw and other materials by the inlet pipe 1 in, motor 16 begins work, it rotates to drive motor shaft 12, the first fixed column 21 of motor shaft 12 lateral wall fixedly connected with drives raw and other materials and stirs the board 20 and stir raw and other materials evenly, first atomizer 4 works, can not atomize raw and other materials by atomizer 3 through first atomizer 2, prevent raw and other materials reunion, second atomizer 14 works, atomize raw and other materials through second atomizer 17, the first ultrasonic wave generating tube 11 that reation kettle 22's lateral wall set up passes through control panel 18's control with second ultrasonic wave generating tube 19, prevent raw and other materials polymerization more deeply, the complete nano-material of final reaction is discharged by discharging pipe 6, the export of discharging pipe 6 can be closed to the first ooff valve 7 of lateral wall, reation kettle's upper end inlet tube 13 can let in the clear water, clearance reation kettle, sewage is discharged by outlet pipe 9.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications and variations can be made in the embodiments or in part of the technical features of the embodiments without departing from the spirit and the scope of the invention.
Claims (10)
1. A novel reation kettle is used in material preparation, includes reation kettle (22), its characterized in that: the device box (15) is fixedly connected to the upper end of the middle of the reaction kettle (22), the motor (16) is arranged inside the device box (15), the second atomizers (14) are fixedly connected to the upper end of the reaction kettle (22) and two sides of the device box (15), the number of the second atomizers (14) is two, the second atomizing pipe (17) is arranged on one side of each second atomizer (14), and the second atomizing pipe (17) penetrates through the reaction kettle (22);
two sides of the lower end of the reaction kettle (22) are fixedly connected with first atomizers (4), one side of each first atomizer (4) is provided with a first atomizing pipe (2), one side of each first atomizing pipe (2) is provided with four atomizing nozzles (3), and the number of the atomizing nozzles (3) is four;
the lateral wall of reation kettle (22) is provided with first ultrasonic wave generating pipe (11), the lateral wall of reation kettle (22) just keeps away from first ultrasonic wave generating pipe (11) department and is provided with second ultrasonic wave generating pipe (19), one side of first ultrasonic wave generating pipe (11) and second ultrasonic wave generating pipe (19) is provided with control panel (18).
2. The reactor for preparing the novel material as claimed in claim 1, wherein: one end of the motor (16) is provided with a motor shaft (12) in an extending position, a first fixing column (21) is fixedly connected to the side wall of the motor shaft (12), a scraping blade (10) is fixedly connected to the side wall of the first fixing column (21) and the inner wall close to the reaction kettle (22), and a stirring plate (20) is fixedly connected to the side wall of the lower end of the motor shaft (12).
3. The reactor for preparing the novel material as claimed in claim 1, wherein: the inner wall of the reaction kettle (22) is fixedly connected with a second fixing column (24).
4. The reactor for preparing the novel material as claimed in claim 1, wherein: the utility model discloses a reactor, including reation kettle (22), the upper end one side of reation kettle (22) is provided with inlet pipe (1), the upper end opposite side of reation kettle (22) is provided with inlet tube (13).
5. The reactor for preparing the novel material as claimed in claim 1, wherein: the middle part lower extreme of reation kettle (22) is provided with discharging pipe (6), the lateral wall of discharging pipe (6) is provided with first ooff valve (7), the lower extreme one side of reation kettle (22) is provided with outlet pipe (9), the lateral wall of outlet pipe (9) is provided with second ooff valve (8).
6. The reactor for preparing the novel material as claimed in claim 1, wherein: the lower end inner wall of the reaction kettle (22) is fixedly connected with an auxiliary rod (23) close to the first atomizing pipe (2).
7. The reactor for preparing the novel material as claimed in claim 1, wherein: the lower extreme fixedly connected with support column (5) of reation kettle (22), and the quantity of support column (5) is three.
8. The reactor for preparing the novel material as claimed in claim 3, wherein: the number of the second fixing columns (24) is four, and the two second fixing columns (24) are respectively and fixedly connected to the upper side and the lower side of the scraping blade (10).
9. The reactor for preparing the novel material as claimed in claim 6, wherein: the auxiliary rod (23) is arranged on the inner side of the first atomizing pipe (2).
10. The reactor for preparing the novel material as claimed in claim 2, wherein: the stirring plate (20) is arranged on the inner side of the auxiliary rod (23).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022151768.2U CN213995837U (en) | 2020-09-27 | 2020-09-27 | Novel reation kettle is used in material preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022151768.2U CN213995837U (en) | 2020-09-27 | 2020-09-27 | Novel reation kettle is used in material preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213995837U true CN213995837U (en) | 2021-08-20 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022151768.2U Expired - Fee Related CN213995837U (en) | 2020-09-27 | 2020-09-27 | Novel reation kettle is used in material preparation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213995837U (en) |
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2020
- 2020-09-27 CN CN202022151768.2U patent/CN213995837U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210820 |