CN213977600U - Oil-water separation device with guide plate - Google Patents

Oil-water separation device with guide plate Download PDF

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Publication number
CN213977600U
CN213977600U CN202022669973.8U CN202022669973U CN213977600U CN 213977600 U CN213977600 U CN 213977600U CN 202022669973 U CN202022669973 U CN 202022669973U CN 213977600 U CN213977600 U CN 213977600U
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China
Prior art keywords
oil
guide plate
water separator
water
pipe
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CN202022669973.8U
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Chinese (zh)
Inventor
苏国岁
王龙
戴亚
何爱民
郝红玲
卜一凡
李杰辉
李远根
寇天舒
任志强
张艳芳
陈伟华
张晓静
阎瑾
马桂芹
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HEBEI CHINA TOBACCO INDUSTRY CO LTD
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HEBEI CHINA TOBACCO INDUSTRY CO LTD
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Abstract

The invention discloses an oil-water separation device with a guide plate, which comprises a conical oil-water separator, wherein the guide plate is arranged at the outlet end of an inlet pipe of the oil-water separator, the guide plate is in a segmental shape, the guide plate is fixedly connected with the inlet pipe through a rod-shaped body, an adjusting pipe is arranged at the lower part of the inlet pipe, the adjusting pipe is screwed or clamped with the inlet pipe, an oil taking port is formed in the upper part of the oil-water separator, and a condensing pipe and a backflow pipe are arranged at the bottom of the oil-water separator. The guide plate can impact the flow direction of the mixed liquid from vertical to downward, guide the mixed liquid to be uniformly distributed on the whole section along the radial direction of the guide plate and slowly move downward, so that the direct impact on the oil-water mixed liquid in the separator is eliminated, and part of the oil-water mixed liquid is prevented from returning to a distillation device or entering fresh flower dew without being separated. The invention can continuously and efficiently separate and collect the volatile oil, has the characteristics of high separation efficiency and good continuity on oil-water mixed liquid with lower content of the volatile oil, is easy to disassemble and replace, has low manufacturing cost, can be generally compatible with steam distillation equipment used in the prior production, and is suitable for popularization and application.

Description

Oil-water separation device with guide plate
Technical Field
The invention relates to an oil-water separation device for extracting volatile oil by a steam distillation method.
Background
The steam distillation method is the most common continuous dynamic extraction method of volatile oil, has the advantages of simple structure, simple and convenient operation, high efficiency, no pollution, no solvent residue in the prepared volatile oil and the like, and is widely applied to actual production.
The oil-water separator is a core component in the process of preparing volatile oil by a steam distillation method, and the oil-water separation effect is one of the main factors influencing the oil yield. The gravity settling oil-water separation method is a traditional and economic oil-water separation method, realizes the separation of volatile oil and water by utilizing the incompatibility and density difference between oil and water and through the mutual collision and aggregation of oil droplets with different particle diameters in a static or flowing state, and has the advantages of simple structure, small flow resistance, capability of treating large-flow oil-water mixtures and the like.
In the existing gravity settling oil-water separator, an oil-water mixture is generally vertically guided into a separation chamber by a guide pipe for separation. However, in the practical application process, the oil-water mixture in the separation chamber is disturbed because the oil-water mixture still has a higher initial speed when flowing out of the inlet pipe; meanwhile, a large amount of oil droplets are flushed into the bottom of the separation chamber along with water flow, so that the rising time of the oil droplets is increased, the wall sticking is increased, and a part of the oil droplets enter a return pipe along with the water flow and return to a distillation device or enter extracted fresh flower dew, so that the oil recovery rate is greatly reduced.
Disclosure of Invention
The invention provides an oil-water separation device with a guide plate, which is used for improving the oil-water separation efficiency and the oil yield.
The oil-water separator with the guide plate comprises an oil-water separator and is characterized in that the oil-water separator is of a conical structure, the guide plate is arranged at the outlet end of an inlet pipe of the oil-water separator, the guide plate is in a segmental shape, the guide plate is fixedly connected with the inner wall of the inlet pipe through a rod-shaped body, an adjusting pipe is arranged at the lower part of the inlet pipe, the adjusting pipe is screwed or clamped with the inlet pipe, an oil taking port is formed in the upper part of the oil-water separator, a condensing pipe and a return pipe are respectively arranged at the bottom of the oil-water separator, and the return pipe is connected with a distillation chamber of the distiller after passing through a U-shaped pipe.
The diameter of the guide plate is 1.5-3 times of the inner diameter of the guide pipe.
The invention achieves the technical progress that:
the invention solves the practical problems of low oil-water separation efficiency and large loss of volatile oil in the prior production by arranging the relative adjustable guide plate, the secondary condenser pipe and the oil-water separator with the conical structure, and particularly obviously improves the separation and collection of the volatile oil with low oil yield. Experiments prove that after the oil-water mixed liquid at the temperature of 30-40 ℃ enters the inlet pipe, the oil-water mixed liquid is guided by the segmental structure guide plate at the outlet end of the inlet pipe and then radially enters the conical oil-water separator for oil-water separation. After the oil-water mixed liquid with higher temperature enters the separator, the surface tension of oil droplets is favorably reduced, the collision coalescence capability is enhanced, oil drops in the mixed liquid form floatable oil as soon as possible, meanwhile, the solidification and adhesion of viscous volatile oil can be avoided, and the collection rate is improved.
Because the regulating tube is screwed or clamped at the lower part of the leading-in tube, the outlet at the bottom of the regulating tube can keep a proper vertical distance with the guide plate by regulating the height of the regulating tube, so that the mixed liquid is more uniformly distributed on the guide plate in the radial direction when flowing out, and the oil-water separation operation of oil-water mixture materials with different viscosities and different flows is adapted.
The guide plate with the segmental structure can impact the flow direction of the mixed liquid from vertical to downward, and is guided to be uniformly distributed on the whole section along the radial direction of the segmental guide plate and slowly move downward, so that the direct impact on the oil-water mixed liquid in the separator is eliminated, the phenomenon that part of the oil-water mixed liquid returns to a distillation device or enters fresh flower dew without being separated is avoided, and oil drops can be effectively prevented from being accumulated at the bottom of the guide plate.
The tapered oil-water separator at the outlet end of the inlet pipe has a larger cross section, so that the flow rate of oil-water mixed liquid is reduced, the oil-water separation time is prolonged, and meanwhile, the smaller volatile oil storage layer surface at the upper part of the tapered oil-water separator is more favorable for collecting volatile oil with lower oil yield.
Because the bottom of the conical oil-water separator is provided with the condenser pipe, the liquid which is about to return to the distillation device or enter the fresh flower dew can be cooled, the oil/water emulsification rate is reduced, and some substances which are insoluble or slightly soluble in cold water and easily soluble in hot water are further separated out at the position, so that the loss of effective components is reduced, and the increase of the components of the volatile oil is facilitated.
The invention can continuously and efficiently separate and collect the volatile oil extracted by the steam distillation method, maintains the advantages of simple structure, easy operation and the like of a separation chamber of the traditional oil-water separator, has the characteristics of high separation efficiency, good continuity and low cost for oil-water mixed liquid with lower volatile oil content, is easy to disassemble and replace, can be generally compatible with steam distillation equipment used in the prior production, and is suitable for popularization and application.
Drawings
FIG. 1 is a schematic view of the structure of the present invention.
Fig. 2 is a partially enlarged structural diagram of a in fig. 1.
Detailed Description
The present invention will be further described below with reference to the accompanying drawings by taking the steam distillation method for extracting the natural petal volatile oil as an example.
As shown in fig. 1 and 2, the oil-water separator with a baffle comprises an oil-water separator 3, the oil-water separator 3 is of a conical structure, a segmental guide plate 2 is arranged at the outlet end of the bottom of an inlet pipe 5 assembled at the inlet at the top of the oil-water separator 3, the diameter of the guide plate 2 is 1.5 to 3 times of the inner diameter of the guide-in pipe 5, the guide plate 2 is fixedly connected with the inner wall of the guide-in pipe 5 through at least three rod-shaped bodies 7, the lower end of each rod-shaped body 7 is fixedly connected with the inner wall of the guide plate 2 in a welding way, the three rod-shaped bodies 7 are distributed on the guide plate 2 in 120 degrees, a section of adjusting pipe 8 is arranged at the lower part of the guide-in pipe 5, the adjusting pipe 8 is connected (or clamped) with the leading-in pipe 5 in a rotating way, the upper part of the oil-water separator 3 is provided with an oil taking port 4, the bottom of the oil-water separator 3 is respectively provided with a condensing pipe 1 and a return pipe 6, and the return pipe 6 is connected with a distiller distillation chamber after passing through a U-shaped pipe.
The oil-water mixture that condenses to 30 ~ 40 ℃ collects the back via inlet tube 5, the 5 bottom export of inlet tube through the immersion liquid level flows perpendicularly in toper oil-water separator 3, the relative position of 5 bottom exports of inlet tube and guide plate 2 is adjusted to rotatory regulating tube 8, oil-water mixture moves down under the action of gravity and receives and block behind the guide plate 2, along the horizontal evenly distributed back of guide plate 2 radial direction at whole liquid level, the slow motion downwards, prevent that oil-water mixture from directly rushing into lower floor low temperature region and leading to the drop in temperature of oil, surface tension increases and scatters, the wall glues. Due to the cooling effect of the condenser pipe 1, the liquid on the bottom layer in the oil-water separator 3 further separates out the volatile components dissolved therein and floats to the upper layer. Because the density of the volatile oil is lower than that of water, oil droplets float to the upper liquid level while colliding and coalescing to form an oil-water separation layer, after an oil layer with a certain thickness is accumulated, the volatile oil can be discharged through the oil taking port 4 and collected by opening the flow guide valve, the inlet end of the return pipe 6 is positioned at the circle center of the bottom of the conical oil-water separator 3, and the oil layer in the conical oil-water separator 3 can be kept at the height of the oil taking port 4 all the time under the action of the U-shaped pipe.

Claims (2)

1. The utility model provides an oil-water separator with guide plate, it includes oil-water separator, its characterized in that oil-water separator is conical structure, oil-water separator inlet tube exit end is provided with the guide plate, the guide plate is the rounding form, the guide plate links firmly with the inlet tube inner wall through the rodlike body, an adjusting tube is installed to the inlet tube lower part, adjusting tube and inlet tube connect or joint soon, oil-water separator upper portion has been seted up and has been got the hydraulic fluid port, and the oil-water separator bottom is provided with condenser pipe and back flow respectively, the back flow meets with the distiller distillation chamber behind "U" venturi tube.
2. The oil-water separator with the baffle as recited in claim 1, wherein the diameter of the baffle is 1.5 to 3 times the inner diameter of the inlet pipe.
CN202022669973.8U 2020-11-18 2020-11-18 Oil-water separation device with guide plate Active CN213977600U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202022669973.8U CN213977600U (en) 2020-11-18 2020-11-18 Oil-water separation device with guide plate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202022669973.8U CN213977600U (en) 2020-11-18 2020-11-18 Oil-water separation device with guide plate

Publications (1)

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CN213977600U true CN213977600U (en) 2021-08-17

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112300866A (en) * 2020-11-18 2021-02-02 河北中烟工业有限责任公司 Oil-water separation device with guide plate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112300866A (en) * 2020-11-18 2021-02-02 河北中烟工业有限责任公司 Oil-water separation device with guide plate

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