CN213901983U

CN213901983U - Multistage condensation structure is used in phosphorus pentachloride production

Info

Publication number: CN213901983U
Application number: CN202022750016.8U
Authority: CN
Inventors: 常天赐; 常贺; 李荣金; 常德启
Original assignee: Xuzhou Yongli Fine Chemical Co ltd
Current assignee: Xuzhou Yongli Fine Chemical Co ltd
Priority date: 2020-11-25
Filing date: 2020-11-25
Publication date: 2021-08-06
Anticipated expiration: 2030-11-25

Abstract

The utility model relates to a phosphorus pentachloride production technical field just discloses a multistage condensation structure is used in phosphorus pentachloride production, including the water-cooling box, the water-cooling box internal fixation pegs graft and has the passage, the passage slope sets up downwards, the fixed intercommunication of lateral wall of water-cooling box upside has the water pipe, the fixed intercommunication of lower extreme of water pipe has violently the pipe, the fixed intercommunication of pipe wall of violently managing the downside has a plurality of shower heads, the left outer wall fixedly connected with fixed plate of water-cooling box, the lateral wall fixedly connected with pump machine of fixed plate upside. The utility model discloses can carry out multistage condensation, effectual condensation effect and the condensation efficiency of having improved, and improve the smooth and easy degree of condensation structure operation.

Description

Multistage condensation structure is used in phosphorus pentachloride production

Technical Field

The utility model relates to a phosphorus pentachloride production technical field especially relates to a multistage condensation structure is used in phosphorus pentachloride production.

Background

Phosphorus pentachloride is an inorganic compound, is a colorless, hygroscopic solid, is mainly used as a chlorinating agent, and can have different structures under different conditions. The condensation process is needed to carry out the condensation treatment on the phosphorus pentachloride in the production and processing process.

For example, chinese patent No. CN209085384U discloses a condenser for preparing phosphorus pentachloride, which comprises a base, a condensing box fixedly connected to the top of the base, a condensing tube disposed in the condensing box, one end of the condensing tube penetrating the top of the inner wall of one side of the condensing box and extending outward, and the other end of the condensing tube penetrating the bottom of the inner wall of the condensing box and extending outward. The condenser for preparing phosphorus pentachloride in the patent has the following defects: above-mentioned condenser uses snakelike condenser pipe to condense when using, and the material in snakelike condenser pipe leads to behind congealing can lead to the condenser pipe to block up to influence the normal flow of material, influence the normal use of condenser.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the problem that the snake-shaped condensing tube of the condenser is easy to block in the prior art, and providing a multistage condensation structure for producing phosphorus pentachloride.

In order to achieve the above purpose, the utility model adopts the following technical scheme:

a multistage condensation structure for phosphorus pentachloride production comprises a water cooling tank, wherein a material guide pipe is fixedly inserted in the water cooling tank, the material guide pipe is obliquely and downwards arranged, a water pipe is fixedly communicated with the side wall of the upper side of the water cooling tank, the lower end of the water pipe is fixedly communicated with a transverse pipe, a plurality of spray headers are fixedly communicated with the pipe wall of the lower side of the transverse pipe, a fixed plate is fixedly connected with the outer wall of the left side of the water cooling tank, a pump is fixedly connected with the side wall of the upper side of the fixed plate, a water inlet of the pump is fixedly communicated with a water pumping pipe, the water pumping pipe is fixedly communicated with the water cooling tank, a condensation tank is fixedly communicated with the lower end of the material guide pipe, a refrigerating pipe is fixedly connected with the side wall of the upper side of the condensation tank, two mounting holes are symmetrically and fixedly connected with the side wall of the upper side of the condensation tank, a fan is fixedly connected with the two mounting holes, and a plurality of inclined plates are fixedly connected with the inner wall of the condensation tank, a plurality of the swash plate is crisscross to be set up, the fixed intercommunication of bottom of condensing box has the unloading pipe.

Preferably, the upper end of the material guide pipe is fixedly connected with a conical discharging hopper.

Preferably, the lateral wall symmetry fixedly connected with two dustproof otter boards of condensing box upside, two dustproof otter board is located two fans directly over respectively.

Preferably, the bottom of the water cooling tank is fixedly connected with two support rods, and the upper ends of the support rods are fixedly connected with the outer wall of the material guide pipe.

Preferably, the water cooling tank and the bottom of the condensing tank are fixedly connected with the same connecting plate.

Preferably, the material guide pipe is an aluminum pipe.

Compared with the prior art, the utility model provides a multistage condensation structure is used in phosphorus pentachloride production possesses following beneficial effect:

the multistage condensation structure for producing phosphorus pentachloride is characterized in that a water cooling tank, a material guide pipe, a water pipe, a horizontal pipe, a spray header, a fixed plate, a pump, a water pumping pipe, a condensation box, a refrigeration pipe, a mounting hole, a fan, an inclined plate and a discharging pipe are arranged, when the multistage condensation structure is used, a substance to be condensed is guided into the material guide pipe, water is conveyed into the horizontal pipe through the water pipe and is sprayed out through a plurality of spray headers, the sprayed water is contacted with the material guide pipe and can absorb heat on the material guide pipe, so that the substance in the material guide pipe can be cooled, the sprayed water falls into the water cooling tank, the material guide pipe is soaked in the water, so that the water cooling effect can be improved, the water in the water cooling tank is discharged through the pump at regular time, when the substance enters the condensation tank through the material guide pipe, the refrigeration pipe is controlled to carry out refrigeration, so that the temperature in the condensation tank can be reduced, and the material can be condensed, and the inclined plates can slowly flow downwards, thereby can improve the condensation time, thereby can improve the condensation effect, the control fan rotates, and the air current that the fan drove is reduced by the temperature when refrigerating the pipe, thereby can be with low temperature gas diffusion to in the condenser box, the effectual condensation efficiency that has improved, and passage and swash plate all are the slope setting, and the material can be smooth and easy flow to the unloading pipe in, the problem of jam can not appear, the effectual smooth and easy degree that improves condensation structure and use.

The part that does not relate to among the device all is the same with prior art or can adopt prior art to realize, the utility model discloses can carry out multistage condensation, the effectual condensation effect and the condensation efficiency that has improved, and improve the smooth and easy degree of condensation structure operation.

Drawings

FIG. 1 is a schematic structural view of a multistage condensation structure for producing phosphorus pentachloride according to the present invention;

fig. 2 is a schematic structural view of a portion a in fig. 1.

In the figure: 1 water cooling tank, 2 material guide pipes, 3 water pipes, 4 transverse pipes, 5 spray headers, 6 fixing plates, 7 pumps, 8 water pumping pipes, 9 condensation tanks, 10 refrigeration pipes, 11 mounting holes, 12 fans, 13 inclined plates, 14 discharging pipes, 15 conical discharging hoppers, 16 dustproof mesh plates, 17 supporting rods and 18 connecting plates.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.

In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.

Referring to fig. 1-2, a multistage condensation structure for phosphorus pentachloride production comprises a water cooling tank 1, a material guide pipe 2 is fixedly inserted in the water cooling tank 1, the material guide pipe 2 is arranged obliquely downwards, a water pipe 3 is fixedly communicated with the side wall of the upper side of the water cooling tank 1, the lower end of the water pipe 3 is fixedly communicated with a transverse pipe 4, the pipe wall of the lower side of the transverse pipe 4 is fixedly communicated with a plurality of spray headers 5, the outer wall of the left side of the water cooling tank 1 is fixedly connected with a fixed plate 6, the side wall of the upper side of the fixed plate 6 is fixedly connected with a pump 7, a water inlet of the pump 7 is fixedly communicated with a water pumping pipe 8, the water pumping pipe 8 is fixedly communicated with the water cooling tank 1, the lower end of the material guide pipe 2 is fixedly communicated with a condensation tank 9, the side wall of the upper side of the condensation tank 9 is fixedly connected with a refrigeration pipe 10, the side wall of the upper side of the condensation tank 9 is symmetrically and fixedly connected with two mounting holes 11, and the hole walls of the two mounting holes 11 are both fixedly connected with a fan 12, the inner wall of the condensing box 9 is fixedly connected with a plurality of inclined plates 13, the inclined plates 13 are arranged in a staggered manner, the bottom of the condensing box 9 is fixedly communicated with a discharging pipe 14, when the condensing box is used, a substance to be condensed is guided into the material guide pipe 2, water is conveyed into the transverse pipe 4 through the water pipe 3 and is sprayed out through the plurality of spray heads 5, the sprayed water is contacted with the material guide pipe 2 and can absorb heat on the material guide pipe 2, so that the substance in the material guide pipe 2 can be cooled, the sprayed water falls into the water cooling box 1, the material guide pipe 2 is soaked in the water, so that the water cooling effect can be improved, the water in the water cooling box 1 is discharged through the pump 7 at regular time, when the substance enters the condensing box 9 through the material guide pipe 2, the cooling pipe 10 is controlled to run for cooling, so that the temperature inside the condensing box 9 can be reduced, so that the substance can be condensed, and the arranged inclined plates 13 can make the substance slowly flow downwards, thereby can improve the condensation time, thereby can improve the condensation effect, control fan 12 rotates, the air current that fan 12 drove is reduced by the temperature when the refrigeration pipe 10, thereby can be with low temperature gas diffusion to the condensing box 9 in, the effectual condensation efficiency that has improved, and passage 2 and swash plate 13 all are the slope setting, the material can be smooth and easy flow to the unloading pipe 14 in, the problem of jam can not appear, the effectual smooth and easy degree that improves the use of condensation structure.

The upper end of the material guide pipe 2 is fixedly connected with a conical blanking hopper 15, so that the material can be conveniently fed into the material guide pipe 2.

Two dustproof mesh plates 16 are symmetrically and fixedly connected to the side wall of the upper side of the condensation box 9, the two dustproof mesh plates 16 are respectively located right above the two fans 12, and the dustproof mesh plates 16 can prevent dust from entering the condensation box 9.

Two bracing pieces 17 of bottom fixedly connected with of water-cooling box 1, the upper end of bracing piece 17 and the outer wall fixed connection of passage 2, bracing piece 17 can support passage 2, the effectual stability that improves passage 2.

The bottom fixedly connected with same connecting plate 18 of water-cooling tank 1 and condensing box 9, connecting plate 18 can improve the stability of water-cooling tank 1 and condensing box 9.

The material guide pipe 2 is an aluminum pipe, and the heat conducting property of aluminum is good, so that the condensation efficiency can be improved.

In the utility model, when in use, the material to be condensed is guided into the material guiding pipe 2, water is conveyed into the transverse pipe 4 through the water pipe 3, the water is sprayed out through the plurality of spray heads 5, the sprayed water is contacted with the material guiding pipe 2 and can absorb the heat on the material guiding pipe 2, thereby the material in the material guiding pipe 2 can be cooled, the sprayed water falls into the water cooling box 1, the material guiding pipe 2 is soaked in the water, thereby the water cooling effect can be improved, the water in the water cooling box 1 is discharged through the pump 7 at regular time, when the material enters the condensing box 9 through the material guiding pipe 2, the operation of the cooling pipe 10 is controlled to refrigerate, thereby the temperature inside the condensing box 9 can be reduced, thereby the material can be condensed, and the plurality of sloping plates 13 are arranged, the material can slowly flow downwards, thereby the condensing time can be improved, thereby the condensing effect can be improved, the fan 12 is controlled to rotate, the temperature is reduced when the air current that fan 12 drove is through refrigeration pipe 10 to can be with low temperature gas diffusion to the condensing box 9 in, the effectual condensation efficiency that has improved, and passage 2 and swash plate 13 all are the slope setting, and the material can be smooth and easy flows to unloading pipe 14 in, the problem of jam can not appear, the effectual smooth and easy degree that improves the use of condensation structure.

The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims

1. A multistage condensation structure for phosphorus pentachloride production comprises a water cooling tank (1) and is characterized in that a material guide pipe (2) is fixedly inserted in the water cooling tank (1), the material guide pipe (2) is obliquely and downwards arranged, a water pipe (3) is fixedly communicated with the side wall of the upper side of the water cooling tank (1), a transverse pipe (4) is fixedly communicated with the lower end of the water pipe (3), a plurality of spray headers (5) are fixedly communicated with the pipe wall of the lower side of the transverse pipe (4), a fixed plate (6) is fixedly connected with the outer wall of the left side of the water cooling tank (1), a pump (7) is fixedly connected with the side wall of the upper side of the fixed plate (6), a water suction pipe (8) is fixedly communicated with the water inlet of the pump (7), the water suction pipe (8) is fixedly communicated with the water cooling tank (1), a condensation tank (9) is fixedly communicated with the lower end of the material guide pipe (2), and a cooling pipe (10) is fixedly connected with the side wall of the upper side of the condensation tank (9), the utility model discloses a condenser box, including condenser box (9), lateral wall symmetry fixedly connected with two mounting holes (11), two of condenser box (9) upside the equal fixedly connected with fan (12) of pore wall of mounting hole (11), a plurality of swash plates (13) of inner wall fixedly connected with of condenser box (9), it is a plurality of swash plate (13) set up crisscross, the fixed intercommunication in bottom of condenser box (9) has unloading pipe (14).

2. The multistage condensation structure for phosphorus pentachloride production according to claim 1, wherein the upper end of the material guiding pipe (2) is fixedly connected with a conical discharging hopper (15).

3. The multistage condensation structure for phosphorus pentachloride production according to claim 1, wherein two dustproof mesh plates (16) are symmetrically and fixedly connected to the side wall of the upper side of the condensation box (9), and the two dustproof mesh plates (16) are respectively positioned right above the two fans (12).

4. The multistage condensation structure for phosphorus pentachloride production according to claim 1, wherein two support rods (17) are fixedly connected to the bottom of the water cooling tank (1), and the upper ends of the support rods (17) are fixedly connected to the outer wall of the material guide pipe (2).

5. The multistage condensation structure for phosphorus pentachloride production according to claim 1, wherein the bottom of the water cooling tank (1) and the bottom of the condensation tank (9) are fixedly connected with the same connecting plate (18).

6. The multistage condensation structure for phosphorus pentachloride production according to claim 1, wherein the material guiding pipe (2) is an aluminum pipe.