CN213853188U - A device for extracting chenopodium quinoa flavone - Google Patents
A device for extracting chenopodium quinoa flavone Download PDFInfo
- Publication number
- CN213853188U CN213853188U CN202022388106.7U CN202022388106U CN213853188U CN 213853188 U CN213853188 U CN 213853188U CN 202022388106 U CN202022388106 U CN 202022388106U CN 213853188 U CN213853188 U CN 213853188U
- Authority
- CN
- China
- Prior art keywords
- flavone
- cooling
- leaching tank
- quinoa
- crushing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title claims abstract description 48
- 229930003944 flavone Natural products 0.000 title claims abstract description 48
- 150000002212 flavone derivatives Chemical class 0.000 title claims abstract description 48
- 235000011949 flavones Nutrition 0.000 title claims abstract description 48
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title claims abstract description 48
- 240000006162 Chenopodium quinoa Species 0.000 title claims abstract description 37
- 235000015493 Chenopodium quinoa Nutrition 0.000 title description 10
- 238000002386 leaching Methods 0.000 claims abstract description 31
- 238000001816 cooling Methods 0.000 claims abstract description 28
- 238000000746 purification Methods 0.000 claims abstract description 21
- 238000000605 extraction Methods 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 239000000498 cooling water Substances 0.000 claims description 14
- 239000011347 resin Substances 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 3
- 238000009827 uniform distribution Methods 0.000 claims description 2
- 238000013016 damping Methods 0.000 abstract description 3
- 238000013461 design Methods 0.000 abstract description 3
- 239000003960 organic solvent Substances 0.000 abstract description 3
- 238000000926 separation method Methods 0.000 abstract description 2
- 238000012546 transfer Methods 0.000 abstract description 2
- 238000010992 reflux Methods 0.000 abstract 1
- 238000011160 research Methods 0.000 description 6
- 238000011161 development Methods 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000012216 screening Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 241000282414 Homo sapiens Species 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
- 230000005714 functional activity Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 241000554155 Andes Species 0.000 description 1
- 241000871189 Chenopodiaceae Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- -1 flavonoid compounds Chemical class 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000002390 rotary evaporation Methods 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
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- Extraction Or Liquid Replacement (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention discloses a device for extracting quinoa flavone, which comprises a rubber foot pad and a frame, wherein a leaching tank is arranged at the bottom of the frame, a pulverizer is arranged at the upper part of the frame, a separation sieve is arranged at the bottom of the pulverizer, and materials are sieved and then introduced into the leaching tank through a material conveying pipe; a damping device is arranged on the base of the frame and supports the leaching tank; a magnetic field device is arranged in the central inner cavity, and a stirrer is placed in the leaching tank; an infrared heating mechanism is arranged on the periphery of the leaching tank; a fixing bracket is arranged on the inner wall of the frame, and the cooling reflux device is fixed and connected with the purification column; the bottom of the frame is provided with a flavone collecting box for collecting the purified flavone. The utility model discloses a combined design of crushing system, leaching system, cooling system and purification system has reduced loaded down with trivial details extraction process in, can also reduce organic solvent's transfer number of times, reduces the pollution probability. The purification system improves the purity of the quinoa flavone and increases the utilization value of the quinoa flavone.
Description
Technical Field
The utility model relates to a flavone draws technical field, concretely relates to a device for drawing chenopodium quinoa flavone.
Background
Chenopodium Quinoa Willd (Chenopodium Quinoa Willd) also known as Chenopodium Quinoa, Chenopodium Quinoa L.grain, etc., is a herbaceous crop of Chenopodiaceae. Chenopodium quinoa is native to Andes mountain areas in south America, and has been planted for over 5000 years to date. China is introduced in 1987 and is now planted in Shanxi, Ningxia, Xinjiang, Gansu and other places in a large scale. Chenopodium quinoa willd is rich in functional nutritional ingredients, is identified as food which can meet basic nutritional requirements of human bodies by the Food and Agriculture Organization (FAO) of the United nations, is recommended to be full-nutritional food most suitable for human beings, and is praised as super grain and nutritional gold by international nutriologists.
Researches show that the quinoa contains flavonoid components, and the flavonoid compounds have the functional activities of scavenging free radicals, resisting oxidation, resisting aging, resisting tumors, resisting viruses, reducing blood pressure and blood fat, enhancing the immunity of the organism and the like, and have wide application prospects in the industries of medicine, health, food and the like.
Relatively few researches on extraction, purification and functional activity of quinoa flavone are carried out in China, related reports are reported from 2014, and fewer research reports on purification and extraction processes of quinoa flavone are carried out. Obviously, the research on the quinoa flavone in China is still insufficient, which is extremely not beneficial to the development of the quinoa industry and the development and application of the quinoa flavone. Therefore, along with the improvement of large-scale planting of the quinoa in China and the increase of comprehensive development and application appeal of the quinoa, the increase of related researches on the quinoa flavone is a necessary step.
Therefore, the research of extraction and purification of the flavone in the quinoa has positive significance for improving the appeal of comprehensive development and application of the quinoa.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the utility model provides a device for extracting chenopodium quinoa flavone, which perfects the defects of the prior art, has more reasonable structural design, and aims to solve the problems of complex operation and easy occurrence of splashing and ignition of organic solvent caused by the combined use of multiple devices of flavone extracting equipment in the prior art; and the requirements on technical personnel are high, the labor burden is large, and great inconvenience is brought to production.
(II) technical scheme
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes:
a device for extracting quinoa flavone is characterized by comprising a rack and a machine foot rubber pad, wherein the lower part of an inner cavity of the rack is provided with a leaching tank for extracting flavone, a flavone purification column and a flavone collecting box; a cooling system and a crushing system are arranged at the middle upper part of the inner cavity of the rack; the back sides of the leaching tank, the flavone purification system, the flavone collecting box, the cooling system and the crushing device are all fixedly arranged on the frame;
the magnetic field generator is characterized in that the leaching tank is of a cylindrical structure with an arc-shaped top, the leaching tank is fixed on the rack through a damping device, a magnetic stirrer is arranged at the center of the bottom of the leaching tank, and a magnetic field generator fixed on the rack is arranged right below the magnetic stirrer; the device is characterized in that infrared heating devices are arranged around the leaching tank, a material conveying pipeline capable of being completely closed is arranged above the leaching tank, and a crushing system is arranged above the material conveying pipeline.
The crushing system comprises a crushing motor fixed on the frame through a fixing screw, a power output end below the crushing motor is connected with a crushing paddle at the bottom of the crushing chamber, a separating screen is arranged below the crushing paddle, and the separating screen can be replaced in an inserting mode according to particle size requirements.
The cooling system comprises a cooling return pipe connected with a cooling water tank through a cooling water pipe, the cooling return pipe is connected with the leaching tank through a steam delivery pipe, the cooling return pipe is connected with the flavone purification column through a fixed support, and the flavone purification column is filled with macroporous adsorption resin and communicated with the flavone collection box.
Preferably, the cooling system comprises a cooling water pipe installed on the cooling return pipe, the cooling water pipe is connected with a cooling water tank, a cooling fan is installed on one side of the cooling water tank, and the cooling fan is fixedly installed above the outer wall of the rack.
Preferably, one side of the steam conveying pipe close to the leaching tank is hose-connected to realize quick detachment.
Preferably, the sorting screen is provided with small holes with uniform sizes and uniform distribution, and the sorting screen can be switched according to the requirement of particle size.
Preferably, the infrared heating devices arranged on the two sides of the leaching tank can be set according to the requirement of the extraction temperature.
Preferably, an automatic reset valve is arranged inside the material conveying pipe.
The utility model has the advantages that: through the combined design of the crushing system, the leaching system, the cooling system and the purification system, the independent operation of crushing equipment, screening equipment, heating equipment, stirring equipment and rotary evaporation equipment in the original extraction process is changed, the complicated extraction process is reduced, the transfer times of the organic solvent can be reduced, and the pollution probability is reduced. The purification system improves the purity of the quinoa flavone and increases the utilization value of the quinoa flavone.
Drawings
Fig. 1 is the structure schematic diagram of the device for extracting quinoa flavone of the utility model.
FIG. 2 is a schematic view of the structure of the return pipe in FIG. 1
FIG. 3 is a schematic view of the structure of the purification column of FIG. 1
FIG. 4 is a schematic view of the structure of the separation screen of FIG. 1
In the figure: 1. a frame; 2. a flavone collecting box; 3. purifying the column; 4. fixing a bracket; 5. a steam delivery pipe; 6. a cooling return pipe; 7. a water inlet pipe; 8. a water outlet pipe; 9. a pressure relief valve; 10. a cooling water tank; 11. a water injection port; 12. a motor; 13. fixing screws; 14. a filling opening; 15. a crushing cutter; 16. a discharge pipe; 17. sorting and screening; 18. a feed pipe; 19. an infrared heater; 20. a rubber tube; 21. a leaching tank; 22. a magnetic stirrer; 23. a magnetic field generator; 24. a fixed block; 25. a shock absorber; 26. a foot rubber pad; 27. a discharge valve port; 28. macroporous adsorption resin.
Detailed Description
The preferred embodiments of the present invention will be described in conjunction with the accompanying drawings, and it will be understood that they are presented herein only to illustrate and explain the present invention, and not to limit the present invention.
Referring to fig. 1-4, the present invention provides a technical solution: a device for extracting quinoa flavone is shown in the figure, and comprises a frame 1 provided with a foot rubber pad 26, wherein the bottom of the frame 1 is provided with a leaching tank 21, a magnetic field generator 23 and a flavone collecting box 2; install crushing motor 12 in frame 1 top, crushing motor 12 drives crushing cutter 15, be provided with discharging pipe 16 under the crushing cutter, the inside sorting sieve 17 that is equipped with of discharging pipe 16, sorting sieve below is provided with inlet pipe 18, the bayonet installation on leaching jar 21 of inlet pipe 18, leaching jar 21 both sides are equipped with infrared heater 19, the central department of its below is fixed on frame 1 through damping device 25 in leaching jar 21 of telling is provided with magnetic field generator 23, the bottom of leaching jar 21 that corresponds directly over magnetic field generator 23 is provided with magnetic stirrers 22, leaching jar 21 passes through rubber tube 20 and steam conveying pipe 5 and communicates with cooling back flow 6, cooling back flow 6 passes through inlet tube 7 and outlet pipe 8 and communicates with cooling water tank 10, cooling back flow 6 passes through fixed bolster 4 and communicates with the purification post 3 that fills up macroporous adsorbent resin 28, the lower end of the purification column 3 is connected with the flavone collecting box 2, and the bottom of the flavone collecting box is provided with a discharge valve port 27.
The utility model discloses a theory of operation is: the motor 1 is taken down by disassembling the fixed screw 13, the raw materials are placed in the crusher through the feed inlet 14, installing a motor 1 and fastening a fixing screw 13 to start the motor 1 to crush raw materials, screening the crushed raw materials through a sorting sieve 17, then, adding an ethanol solution (volume fraction is 60%) into the extraction tank 21 through the feeding pipe 18 according to a material-liquid ratio 20/1(mL/g) of the crushed materials, simultaneously, starting a magnetic field generator 23 to drive a magnetic stirrer 22 to fully mix the material liquid, feeding alcohol solution steam generated in the extraction process into a cooling return pipe 6 through a steam conveying pipe 5 to be cooled and then returning to a purification column 4, storing quinoa flavone purified by macroporous adsorption resin 28 in the purification column 4 in a flavone collection box, and finally, discharging the quinoa flavone out of the equipment through a discharge valve 27.
The embodiment of the present invention discloses a preferred embodiment, but not limited thereto, and those skilled in the art can easily understand the spirit of the present invention according to the above embodiment, and make different extensions and changes, but do not depart from the spirit of the present invention, all of which are within the protection scope of the present invention.
Claims (6)
1. A device for extracting quinoa flavone is characterized by comprising a rack and a machine foot rubber pad, wherein the lower part of an inner cavity of the rack is provided with a leaching tank, a flavone purification column and a flavone collecting box; a cooling system and a crushing system are arranged at the middle upper part of the inner cavity of the rack; the back sides of the leaching tank, the flavone purification system, the flavone collecting box, the cooling system and the crushing device are all fixedly arranged on the frame; the magnetic field generator is fixed on the rack under the magnetic stirrer; an infrared heating device is arranged around the leaching tank, a material conveying pipeline is arranged above the leaching tank, and a crushing system is arranged above the material conveying pipeline; the crushing system comprises a crushing motor fixed on the frame through a fixing screw, a power output end below the crushing motor is connected with a crushing paddle at the bottom of the crushing chamber, and a sorting screen is arranged below the crushing paddle; the cooling system comprises a cooling return pipe connected with a cooling water tank through a cooling water pipe, the cooling return pipe is connected with the leaching tank through a steam delivery pipe, the cooling return pipe is connected with the purification column through a fixed support, and the purification column is filled with macroporous adsorption resin and communicated with the flavone collecting box.
2. The apparatus for extracting quinoa flavone according to claim 1, wherein: the cooling system comprises a cooling water pipe arranged on a cooling return pipe, the cooling water pipe is connected with a cooling water tank, a cooling fan is arranged on one side of the cooling water tank, and the cooling fan is fixedly arranged above the outer wall of the rack.
3. The apparatus for extracting quinoa flavone according to claim 1, wherein: one side of the steam conveying pipe close to the leaching tank is hose-connected to realize quick detachment.
4. The apparatus for extracting quinoa flavone according to claim 1, wherein: the sorting screen is provided with small holes with uniform sizes and uniform distribution, and the sorting screen can be switched according to the requirement of particle size.
5. The apparatus for extracting quinoa flavone according to claim 1, wherein: the infrared heating devices arranged on the two sides of the leaching tank can be set according to the requirement of extraction temperature.
6. The apparatus for extracting quinoa flavone according to claim 1, wherein: and an automatic reset valve is arranged in the material conveying pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022388106.7U CN213853188U (en) | 2020-10-24 | 2020-10-24 | A device for extracting chenopodium quinoa flavone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022388106.7U CN213853188U (en) | 2020-10-24 | 2020-10-24 | A device for extracting chenopodium quinoa flavone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213853188U true CN213853188U (en) | 2021-08-03 |
Family
ID=77074267
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022388106.7U Expired - Fee Related CN213853188U (en) | 2020-10-24 | 2020-10-24 | A device for extracting chenopodium quinoa flavone |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213853188U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113559550A (en) * | 2021-08-26 | 2021-10-29 | 山西大学 | Method and device for extracting flavone from day lily |
-
2020
- 2020-10-24 CN CN202022388106.7U patent/CN213853188U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113559550A (en) * | 2021-08-26 | 2021-10-29 | 山西大学 | Method and device for extracting flavone from day lily |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210803 |