CN213644149U - Device for dynamic hydrothermal synthesis of molecular sieve - Google Patents
Device for dynamic hydrothermal synthesis of molecular sieve Download PDFInfo
- Publication number
- CN213644149U CN213644149U CN202021860958.5U CN202021860958U CN213644149U CN 213644149 U CN213644149 U CN 213644149U CN 202021860958 U CN202021860958 U CN 202021860958U CN 213644149 U CN213644149 U CN 213644149U
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- Prior art keywords
- heater
- kettle
- reaction kettle
- molecular sieve
- motor
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 239000002808 molecular sieve Substances 0.000 title claims abstract description 16
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 238000001027 hydrothermal synthesis Methods 0.000 title claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 29
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 14
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 230000008878 coupling Effects 0.000 claims description 2
- 238000010168 coupling process Methods 0.000 claims description 2
- 238000005859 coupling reaction Methods 0.000 claims description 2
- 238000009423 ventilation Methods 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 9
- 230000015572 biosynthetic process Effects 0.000 abstract description 8
- 238000003786 synthesis reaction Methods 0.000 abstract description 8
- 238000000034 method Methods 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 230000002000 scavenging effect Effects 0.000 description 3
- 230000003068 static effect Effects 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Abstract
The utility model provides a device for molecular sieve dynamic hydrothermal synthesis, which comprises a reaction kettle, a feed inlet and a discharge outlet are arranged on the reaction kettle, and the device also comprises a heater, a rotary box and supporting legs, when in use, the reaction kettle is arranged in the heater according to the requirement, then the heater and the reaction kettle are placed in the three-jaw chuck, then substances such as water and the like are fed into the reaction kettle through the feed inlet, then the feed inlet is closed, the heater starts to work, the first motor works, the first gear rotates, and therefore the three-jaw chuck is driven to rotate, thereby driving the rotation of the heater and the reaction kettle, and the substance in the reaction kettle shakes to realize the dynamic synthesis process of the substance in the reaction kettle, thereby improve the synthetic efficiency of material and quality, the setting of second motor, speed reducer, (mixing) shaft and stirring rake is stirred the material in the reation kettle to improve the synthetic effect of material.
Description
Technical Field
The utility model belongs to the technical field of reation kettle, concretely relates to a device for molecular sieve dynamic hydrothermal synthesis.
Background
Hydrothermal synthesis means that the temperature is 100~1000 ℃, and pressure is synthesis that material chemical reaction goes on in the aqueous solution under the 1MPa ~1GPa condition, and during hydrothermal synthesis reaction, the material that needs in the reation kettle carries out heating reaction, but current molecular sieve is in the synthetic process, and reation kettle is static synthesis, and the synthesis efficiency is low, how when molecular sieve hydrothermal synthesis, be dynamic synthesis in the reation kettle to improve the synthetic efficiency of molecular sieve and the quality of product, be the utility model discloses the problem that awaits a trial and error.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a device for molecular sieve dynamic hydrothermal synthesis to solve the problem that proposes among the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: a device for molecular sieve dynamic hydrothermal synthesis comprises a reaction kettle, wherein a feed inlet and a discharge outlet are arranged on the reaction kettle, the device further comprises a heater, a rotary box and supporting legs, the heater is of a hollow structure with an open upper part, the reaction kettle is arranged on the heater, the discharge outlet penetrates through the heater, the supporting legs are fixedly arranged on the lower part of the rotary box, the inside of the rotary box is of a hollow structure, a first motor is fixedly arranged inside the rotary box, a first gear is fixedly arranged at the output end of the first motor, the first gear is connected with a second gear in a meshed mode, the second gear is axially and fixedly connected with a rotating shaft, one end of the rotating shaft is connected with the bottom side of the rotary box through a bearing seat bearing, the other end of the rotating shaft penetrates through the upper part of the rotary box, a three-jaw chuck is fixedly arranged at the other end of the rotating shaft, the heater is placed on the three-jaw chuck, the second gear is axially sleeved with a rotating shaft and is in transmission connection with the rotating shaft.
As optimization, the reaction kettle comprises a kettle body and a kettle cover, the kettle body is connected with a kettle cover through a flange, a feed inlet is formed in the kettle cover, a discharge outlet is formed in the kettle body, a second motor and a speed reducer are fixedly mounted on the upper portion of the kettle cover, the output end of the second motor is connected with the input end of the speed reducer through a coupler, a stirring shaft is fixedly mounted at the output end of the speed reducer and penetrates through the kettle cover, stirring paddles are fixedly mounted on the side face of the stirring shaft and located in the kettle body, the second motor selects a motor with the model of YD100L2-6/4 for example, the speed reducer selects a speed reducer with the model of JZQ250 for example, and the stirring shaft penetrates through the kettle cover and.
Preferably, the heater is a cylindrical barrel.
Preferably, the kettle cover is provided with a scavenging valve, a pressure gauge such as a YTF-100H (Y-100BF) gauge and a thermometer such as an SBWZP-230 thermometer.
Preferably, the heater is an electric heater, and the heater is, for example, a JYD-001 heater.
Compared with the prior art, the beneficial effects of the utility model are that: the utility model discloses in, the setting of first motor, first gear, second gear and axis of rotation in the rotatory incasement can drive the rotation of heater and reation kettle to what drive reation kettle interior material rocks realizes reation kettle dynamic synthesis's effect, thereby has solved the laboratory and has been the problem of static synthesis, establishes the basis for industrial development.
Drawings
Fig. 1 is a schematic view of the overall structure of a device for dynamic hydrothermal synthesis of molecular sieves according to the present invention.
In the figure: 1-a reaction kettle, 2-a heater, 3-a rotary box, 4-supporting legs, 5-a feed inlet, 6-a discharge outlet, 7-a first motor, 8-a first gear, 9-a second gear, 10-a rotating shaft, 11-a three-jaw chuck, 12-a kettle body, 13-a kettle cover, 14-a second motor, 15-a speed reducer, 16-a stirring shaft, 17-a stirring paddle, 18-a scavenging valve, 19-a pressure gauge and 20-a thermometer.
Detailed Description
The present invention will be further explained with reference to the accompanying drawings and embodiments, which are to be understood as illustrative only and not limiting the scope of the invention. It should be noted that the terms "front," "back," "left," "right," "upper" and "lower" used in the following description refer to directions in the drawings, and the terms "inner" and "outer" refer to directions toward and away from, respectively, the geometric center of a particular component.
Referring to fig. 1, a device for dynamic hydrothermal synthesis of molecular sieve comprises a reaction kettle 1, a feed inlet 5 and a discharge outlet 6 arranged on the reaction kettle 1, a heater 2, rotatory case 3 and landing leg 4, heater 2 is the open hollow structure in upper portion, reation kettle 1 installs on heater 2, discharge gate 6 runs through heater 2, 3 lower part fixed mounting of rotatory case have landing leg 4, 3 inside hollow structure that are of rotatory case, 3 inside fixed mounting of rotatory case have first motor 7, 7 output end fixed mounting of first motor have first gear 8, 8 meshing of first gear is connected with second gear 9, 9 axial fixedly connected with axis of rotation 10 of second gear, 10 one end of axis of rotation and 3 bottom sides of rotatory case are connected through the bearing frame bearing, the axis of rotation 10 other ends run through 3 upper portions of rotatory case, 10 other end fixed mounting of axis of rotation has three-jaw chuck 11, heater 2 places on three-jaw chuck 11.
The heater 2 is a cylindrical cartridge.
The kettle cover 13 is provided with a scavenging valve 18, a pressure gauge 19 and a thermometer 20.
The heater 2 is an electric heater.
The working principle is as follows: a device for dynamic hydrothermal synthesis of a molecular sieve comprises a reaction kettle 1, wherein a feed inlet 5 and a discharge outlet 6 are arranged on the reaction kettle 1, the device further comprises a heater 2, a rotary box 3 and support legs 4, the heater 2 is of a hollow structure with an open upper part, the reaction kettle 1 is arranged on the heater 2, the discharge outlet 6 penetrates through the heater 2, the support legs 4 are fixedly arranged on the lower part of the rotary box 3, when the device works, the reaction kettle 1 is placed in the heater 2 according to needs, then the heater 2 and the reaction kettle 1 are placed in a three-jaw chuck 11, then substances such as water and the like are fed into the reaction kettle 1 through the feed inlet 5, then the feed inlet 5 is closed, the heater 2 starts to work, a first motor 7 works, a first gear 8 rotates to drive the three-jaw chuck 11 to rotate, so as to drive the rotation of the heater 2 and the reaction kettle 1, substances in the reaction kettle 1 shake, so as to realize the dynamic synthesis process of, thereby improve synthetic efficiency of material and quality, the setting of second motor 14, speed reducer 15, (mixing) shaft 16 and stirring rake 17 stirs the material in reation kettle 1 to improve the synthetic effect of material.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and variations may be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents, and it is intended that the described embodiments be construed as merely illustrative of some embodiments and not restrictive of all embodiments of the invention. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Claims (5)
1. The utility model provides a device for molecular sieve dynamic hydrothermal is synthetic, includes reation kettle (1), be equipped with feed inlet (5) and discharge gate (6) on reation kettle (1), its characterized in that: the reaction kettle is characterized by further comprising a heater (2), a rotating box (3) and supporting legs (4), wherein the heater (2) is of an open hollow structure at the upper part, the reaction kettle (1) is installed on the heater (2), the discharge port (6) penetrates through the heater (2), the supporting legs (4) are fixedly installed at the lower part of the rotating box (3), the rotating box (3) is internally of a hollow structure, a first motor (7) is fixedly installed inside the rotating box (3), a first gear (8) is fixedly installed at the output end of the first motor (7), a second gear (9) is meshed and connected with the first gear (8), a rotating shaft (10) is fixedly connected to the second gear (9) in the axial direction, one end of the rotating shaft (10) is connected with the bottom side of the rotating box (3) through a bearing seat bearing, and the other end of the rotating shaft (10) penetrates through the upper part of, the other end of the rotating shaft (10) is fixedly provided with a three-jaw chuck (11), and the heater (2) is placed on the three-jaw chuck (11).
2. The apparatus of claim 1, wherein: reation kettle (1) is including the cauldron body (12) and kettle cover (13), the cauldron body (12) and kettle cover (13) flange joint, feed inlet (5) set up on kettle cover (13), discharge gate (6) set up on the cauldron body (12), kettle cover (13) upper portion fixed mounting has second motor (14) and speed reducer (15), second motor (14) output and speed reducer (15) input pass through shaft coupling interconnect, speed reducer (15) output fixed mounting has (mixing) shaft (16), (mixing) shaft (16) run through kettle cover (13), mixing shaft (16) side fixed mounting has stirring rake (17), stirring rake (17) are located the cauldron body (12) are inside.
3. An apparatus for molecular sieve dynamic hydrothermal synthesis according to claim 2, characterized in that: the heater (2) is a cylindrical cylinder.
4. An apparatus for molecular sieve dynamic hydrothermal synthesis according to claim 3, characterized in that: and a ventilation valve (18), a pressure gauge (19) and a thermometer (20) are arranged on the kettle cover (13).
5. An apparatus for molecular sieve dynamic hydrothermal synthesis according to claim 4, characterized in that: the heater (2) is an electric heater.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021860958.5U CN213644149U (en) | 2020-08-31 | 2020-08-31 | Device for dynamic hydrothermal synthesis of molecular sieve |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021860958.5U CN213644149U (en) | 2020-08-31 | 2020-08-31 | Device for dynamic hydrothermal synthesis of molecular sieve |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213644149U true CN213644149U (en) | 2021-07-09 |
Family
ID=76693958
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021860958.5U Expired - Fee Related CN213644149U (en) | 2020-08-31 | 2020-08-31 | Device for dynamic hydrothermal synthesis of molecular sieve |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213644149U (en) |
-
2020
- 2020-08-31 CN CN202021860958.5U patent/CN213644149U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210709 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |