CN213589738U - Solvent S-270 purification device - Google Patents

Abstract

The utility model provides a solvent S-270 purification device belongs to solvent purification technical field, including initial storehouse, material mouth, power access mouth and transmission pipe, the top left side position fixed mounting in initial storehouse has the material mouth, and the left side position fixed mounting in initial storehouse has the power access mouth, and the right side position fixed mounting of material mouth has the transmission pipe, and the positive central point in initial storehouse puts fixed mounting and has switch controller. Through the improvement of the structure, the solvent S-270 purification device enables the device to carry out sealed triple purification treatment on the solvent S-270 through the arrangement of the initial bin and the treatment reaction bin in the actual use process, so that the purification effect of the solvent is good, the practicability is high, and the device for purifying the solvent S-270 can purify the generated gas through the arrangement of the purifier when in use, the device can purify the generated gas, the toxic and harmful gas generated after the device is purified through chemical reaction can not pollute the environment, the harm to the human body can not be caused, the safety of the device is good, and the environmental protection property is high.

Description

Solvent S-270 purification device

Technical Field

The utility model relates to a solvent purification technical field specifically is a solvent S-270 purification device.

Background

With the continuous improvement of scientific technology, the use of chemical substances is becoming more common, and the chemical substances can be generally classified into solid, liquid and gas, wherein the use of liquid chemical substances is particularly demanding, because liquid chemical substances are generally obtained through steps of dissolving, purifying, extracting and the like, and because the rigor of the use of chemical solvents makes great attention to the precision removal of impurities in liquid chemical components, the application of chemical solvents in analytical chemistry is extremely wide, and the grade and specification of the solvents should be selected according to specific use conditions and requirements.

The aromatic hydrocarbon solvent 270 is abbreviated as solvent S-270, has the characteristics of strong dissolving capacity, low toxicity, small smell, high boiling point, slow volatilization, no water or olefin, no chlorine or heavy metal, stable chemical and physical properties, good leveling property and the like, is mainly used for preparing a pesticide emulsifier in a solvent of paint and coating, and can also be used as a solvent of resin, cellulose acetate and raw materials of other organic matters.

However, the conventional solvent distillation and purification device for the solvent S-270 is composed of a distillation flask, a thorn-shaped fractionating column, a straight condenser and the like, and has the defects of random standard frame support, large floor area, easy damage of glass parts in the assembling and disassembling process and poor practicability, and when the conventional solvent S-270 purification device is used, the device can not purify the generated gas, and the device generates toxic and harmful gas after being purified by chemical reaction, so that the device is harmful to human bodies, and the safety of the device is poor.

Therefore, there is a need for upgrading and retrofitting existing solvent S-270 purification plants to overcome the existing problems and deficiencies.

SUMMERY OF THE UTILITY MODEL

The utility model aims to solve the problem that the common solvent distillation and purification device of the prior solvent S-270 purification device comprises a distillation flask, a thorn-shaped fractionating column, a straight condenser and the like, and has the defects of random standard frame support, large floor area, easy damage of glass parts in the loading and unloading process and poor practicability, and the prior solvent S-270 purification device can not purify the generated gas by equipment purification when in use, and the device generates poisonous and harmful gas after chemical reaction purification and causes harm to human body, thereby causing the poor safety of the device, and provides an initial bin, a material port, a power supply access port and a transmission pipe, so that the device passes through the improvement of the structure, and the device passes through the arrangement of the initial bin and the treatment reaction bin in the actual use process, so that the solvent S-270 is subjected to device sealing triple purification treatment, thereby having good solvent purification effect, the practicability is strong, and the solvent S-270 purification device can purify the generated gas through the purifier when in use, and the device can not pollute the environment and harm the human body due to the generation of toxic and harmful gas after the purification through chemical reaction, so that the device has good safety and strong environmental protection.

In order to achieve the purpose, the utility model provides the following technical proposal, a solvent S-270 purifying device comprises an initial bin, a material port, a power supply access port and a transmission pipe, a material port is fixedly arranged at the left side position of the top end of the initial bin, a power supply access port is fixedly arranged at the left side position of the initial bin, a transmission pipe is fixedly arranged at the right side position of the material port, a switch controller is fixedly arranged at the center position of the front surface of the initial bin, a treatment reaction bin is fixedly connected at the right side position of the transmission pipe, a reaction solvent port is fixedly arranged at the left side position of the top end of the treatment reaction bin, a water inlet pipe is fixedly arranged at the right rear position of the reaction solvent port, a purifier is fixedly arranged at the right side position of the reaction solvent port, the reaction treatment bin is characterized in that a data display meter is fixedly arranged in the middle of the front surface of the reaction treatment bin, and a purification outlet is fixedly connected to the lower right side of the reaction treatment bin.

Preferably, the inside upper left side position fixed mounting in initial storehouse has the workbin, and the top fixedly connected with material mouth of workbin to the bottom fixedly connected with power pump of workbin, the right side fixedly connected with hydrone filter screen of workbin simultaneously.

Preferably, the upper right position of the water molecule filter screen is fixedly connected with a compression box, the bottom end position of the compression box is fixedly connected with a fixed base, the fixed base and the compression box are vertically distributed in the center, and meanwhile, the right side position of the compression box is fixedly connected with a guide pipe.

Preferably, handle the inside upper left end position fixedly connected with solvent pipe in reaction storehouse, and the bottom fixedly connected with agitator tank of solvent pipe to the bottom fixed connection of agitator tank has reaction purification case, and the bottom fixed mounting of reaction purification case has the heater simultaneously, and the position of heater and reaction purification case is parallel distribution.

Preferably, the inside intermediate position through connection of handling the reaction storehouse has the water pipe, and the bottom fixedly connected with condensing tank of water pipe to condensing tank and condensation filter are fixed connection, and condensation filter's right side position fixedly connected with export simultaneously.

Preferably, the right end position of the reaction purification box is fixedly connected with a reaction gas pipe, the top end position of the reaction gas pipe is fixedly connected with a solid-liquid filter, the middle position of the left side of the solid-liquid filter is fixedly connected with a recovery pipeline, the top end position of the solid-liquid filter is fixedly connected with a gas pipeline, and the reaction gas pipe, the recovery pipeline and the gas pipeline are vertically distributed by taking the solid-liquid filter as the center.

Preferably, the bottom end of the purifier is fixedly connected with a gas pipeline, the interior of the purifier is fixedly provided with a plurality of filter layers, and the top end of each filter layer is fixedly connected with a purification outlet.

Has the advantages that:

(1) through the improvement of the structure, the solvent S-270 purification device enables the device to carry out sealed triple purification treatment on the solvent S-270 through the arrangement of the initial bin and the treatment reaction bin in the actual use process, so that the purification effect of the solvent is good, the practicability is strong, and the device for purifying the solvent S-270 can purify the generated gas through the arrangement of the purifier when in use, the device can purify the generated gas, the toxic and harmful gas generated after the device is purified through chemical reaction can not pollute the environment, the harm to the human body can not be caused, and the device is good in safety and strong in environmental protection.

(2) The solvent S-270 purification device has the advantages that: because the top right side position fixed mounting in initial storehouse has the transmission pipe, the right side position fixedly connected with of transmission pipe handles the reaction storehouse, handle the top left side position fixed mounting in reaction storehouse and have the reaction solvent mouth, this device is moisture in the solvent passes through initial storehouse prefiltration solvent when in-service use, can carry out density compression purification to the solvent simultaneously and transmit to the processing reaction incasement by the transmission pipe and carry out follow-up purification processing, the device sealed adds reaction solvent to the solvent by the reaction solvent mouth and carries out chemical reaction distillation processing in the use, multiple purification makes solvent purification effectual, therefore, the clothes hanger is strong in practicability.

(3) Secondly, the method comprises the following steps: because the right-hand member position fixed connection reaction gas pipe of reaction purification case, and the top position fixedly connected with solid-liquid state filter of reaction gas pipe, and the left side intermediate position fixedly connected with recovery pipeline of solid-liquid state filter, simultaneously solid-liquid filter's top position fixedly connected with gas pipeline, the gas that produces through reaction purification case purification is collected in the solid-liquid state filter by the reaction gas pipe, solid-liquid state filter can carry out liquid, gas separation, liquid is retrieved by recovery pipeline and is recycled, thereby can not cause the waste, harmful gas can transmit through gas pipeline and purify simultaneously, thereby the recovery reuse of device makes the device practicality good with harmful gas's purification, can not cause harm to the environment human body, the security is strong.

Drawings

In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings that are required to be used in the embodiments will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present invention, and therefore should not be considered as limiting the scope, and for those skilled in the art, other related drawings can be obtained according to the drawings without inventive efforts.

Fig. 1 is a schematic view of the overall structure of the present invention.

Fig. 2 is the internal structure diagram of the initial bin of the present invention.

Fig. 3 is the schematic diagram of the internal structure of the reaction treatment bin of the present invention.

Fig. 4 is a schematic diagram of the internal structure of the purifier of the present invention.

In FIGS. 1-4: 1. an initial bin; 101. a material box; 102. a power pump; 103. a water molecule filter screen; 104. a compression box; 105. a fixed base; 106. a conduit; 2. a material port; 3. a power supply access port; 4. a conveying pipe; 5. a switch controller; 6. treating the reaction bin; 601. a solvent tube; 602. a stirring box; 603. a reaction purification box; 604. a heater; 605. a water pipe; 606. a condenser tank; 607. a condensation filter; 608. an outlet; 7. a reaction solvent port; 8. connecting a water pipe; 9. a purifier; 901. a reaction gas tube; 902. a solid-liquid filter; 903. a recovery pipeline; 904. a gas conduit; 905. a plurality of filter layers; 906. a purified outlet; 10. a data display table; 11. and (5) a purification outlet.

Detailed Description

In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all, embodiments of the present invention.

Example (b):

with reference to the figures 1-4 of the drawings,

the solvent S-270 purifying device provided by the embodiment comprises an initial bin 1 and a material port 2, power access mouth 3 and transmission pipe 4, the top left side position fixed mounting in initial storehouse 1 has material mouth 2, the left side position fixed mounting in initial storehouse 1 has power access mouth 3, the right side position fixed mounting of material mouth 2 has transmission pipe 4, the positive central point fixed mounting in initial storehouse 1 has on-off controller 5, the right side position fixed connection of transmission pipe 4 handles reaction chamber 6, the top left side position fixed mounting who handles reaction chamber 6 has reaction solvent mouth 7, the right back position fixed mounting of reaction solvent mouth 7 has access water pipe 8, the right side position fixed mounting of reaction solvent mouth 7 has clarifier 9, 6 positive intermediate position fixed mounting in reaction treatment chamber has data display table 10, the right downside position fixed connection of reaction treatment chamber 6 has purification export 11.

Further, a feed box 101 is fixedly arranged at the left upper side position inside the initial bin 1, the top end of the feed box 101 is fixedly connected with a material port 2, the bottom end of the feed box 101 is fixedly connected with a power pump 102, and the right side of the feed box 102 is fixedly connected with a water molecule filter screen 103;

in this embodiment, the solvent enters the bin 101 inside the initial bin 1 through the material port 2, the power pump 102 at the bottom end provides power when the device is used, so that the solvent is transmitted to the water molecule filter screen 103, and the water molecule filter screen 103 can dehydrate and filter the solvent to realize preliminary purification.

Further, a compression box 104 is fixedly connected to the upper right position of the water molecule filter screen 103, a fixed base 105 is fixedly connected to the bottom end position of the compression box 104, the fixed base 105 and the compression box 104 are centrally and vertically distributed, and a guide pipe 106 is fixedly connected to the right side position of the compression box 104;

in this embodiment, the solvent reaches the compression box 104 after being primarily purified by the water molecule filter screen 103 to be compressed and purified, and meanwhile, the fixing base 105 and the compression box 104 are distributed at positions perpendicular to the center of the compression box 104, so that the compression box 104 is good in fixing effect, and the compressed and purified solvent is transmitted by the guide pipe 106.

Further, a solvent tube 601 is fixedly connected to the left upper end of the interior of the treatment reaction bin 6, the bottom end of the solvent tube 601 is fixedly connected with a stirring box 602, the bottom end of the stirring box 602 is fixedly connected with a reaction purification box 603, a heater 604 is fixedly mounted at the bottom end of the reaction purification box 603, and the heater 604 and the reaction purification box 603 are distributed in parallel;

in this embodiment, the reaction solvent passes through the transport of solvent pipe 601 and in agitator tank 602, the solvent after preliminary purification also transmits in agitator tank 602 and the reaction solvent carries out the intensive mixing and fuses and carry out chemical reaction and reach reaction purification case 603 in, reaction purification case 603 carries out the second time purification and reacts impurity in the solvent, and heater 604 heats the solvent in the reaction simultaneously to make the double purification of device effectual, satisfied the biggest pure rate of purification.

Furthermore, a water pipe 605 is connected to the middle position inside the treatment reaction chamber 6 in a penetrating manner, the bottom end of the water pipe 605 is fixedly connected with a condensation tank 606, the condensation tank 606 is fixedly connected with a condensation filter 607, and an outlet 608 is fixedly connected to the right side position of the condensation filter 607;

in this embodiment, water enters the condenser box 606 through the water pipe 605, the condenser box 606 cools and the purified solvent is cooled and distilled through the condensing filter 607, the distilled solvent can meet the required purity, and then the purified solvent is discharged through the outlet 608, so that the purification effect is good.

Further, a reaction gas pipe 901 is fixedly connected to the right end of the reaction purification box 603, a solid-liquid filter 902 is fixedly connected to the top end of the reaction gas pipe 901, a recovery pipeline 903 is fixedly connected to the middle position of the left side of the solid-liquid filter 902, a gas pipeline 904 is fixedly connected to the top end of the solid-liquid filter 902, and the reaction gas pipe 901, the recovery pipeline 903 and the gas pipeline 904 are vertically distributed with the solid-liquid filter 902 as the center;

in this embodiment, the solvent can produce solid-liquid state gas through the purification of reaction purification case 603, solid-liquid state gas is collected solid-liquid state filter 902 by reaction gas pipe 901 during the equipment uses in, solid-liquid state filter 902 can filter the collection to liquid molecule and retrieve the reaction by recovery pipeline 903 again, thereby make the solvent can not be extravagant, reuse efficiency is high, the harmful gas of separation is carried by gas pipeline 904 simultaneously, and the central vertical distribution of this position makes the device filterability good.

Further, the bottom end of the purifier 9 is fixedly connected with a gas pipeline 904, a plurality of filter layers 905 are fixedly arranged inside the purifier 9, and the top end of the plurality of filter layers 905 is fixedly connected with a purification outlet 906;

in this embodiment, harmful gas carries the clarifier 9 through gas pipeline 904 in, and the inside multilayer filter layer 905 of clarifier 9 can fully filter harmful gas for gas after the filtration satisfies national exhaust emission standard, and harmful gas after the filtration is discharged by purifying export 906, thereby makes the device can satisfy the protection to the environment, reaches the purpose of environmental protection.

The working principle is as follows:

when the solvent S-270 purification device provided by the embodiment is used, the tightness of connection among all parts of the device is firstly checked, then the device is placed at a proper position, after a power supply is connected through a power supply access port 3, the device is enabled to work through a switch controller 5, the solvent is injected into an initial bin 1 through a material port 2 so as to reach an internal material bin 101, when the device is used, a power pump 102 at the bottom end provides power to enable the solvent to be transmitted to a water molecule filter screen 103, the water molecule filter screen 103 can carry out dehydration and filtration on the solvent to realize primary purification, the solvent reaches a compression box 104 after the primary purification to be subjected to compression and purification treatment, the solvent after the compression and purification is transmitted into a transmission pipe 4 through a guide pipe 106, the transmission pipe 4 is transmitted into a treatment reaction bin 6, and meanwhile, a reaction solvent port 7 at the top end of the treatment reaction bin 6 is added into a, then the solvent after preliminary purification and the reaction solvent reach the stirring box 602 for stirring and fusion, and then reach the reaction purification box 603 for chemical reaction purification, the data display table 10 can monitor the internal purification situation in real time, meanwhile, the heater 604 heats the solvent in the reaction, so that the double purification effect of the device reaches the maximum, and water is conveyed to the water pipe 605 in the treatment reaction bin 6 by the access water pipe and then enters the condenser 606, the condenser 606 performs refrigeration, the purified solvent is cooled and distilled by the condenser filter 607, the distilled solvent can meet the required purity, the solvent can generate solid-liquid gas through the purification of the reaction purification box 603, the solid-liquid gas is collected into the solid-liquid filter 902 by the reaction gas pipe 901, the solid-liquid filter 902 can filter and collect liquid molecules and carry out recovery reaction again by the recovery pipeline 903, meanwhile, the filtered harmful gas is conveyed into the purifier 9 through the gas pipeline 904, the harmful gas can be fully filtered by the multilayer filter layers 905 in the purifier 9, so that the filtered gas meets the national waste gas emission standard, the filtered harmful gas is discharged from the purification outlet 906, and the purified solvent after cooling and distillation is collected from the purification outlet 11.

The preferred embodiments of the present invention disclosed above are intended only to help illustrate the present invention. The preferred embodiments are not exhaustive and do not limit the invention to the precise embodiments disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and its practical applications, to thereby enable others skilled in the art to best understand the invention for and utilize the invention. The present invention is limited only by the claims and their full scope and equivalents.

Claims (7)

1. The utility model provides a solvent S-270 purification device, includes initial storehouse (1), material mouth (2), power access mouth (3) and transmission pipe (4), its characterized in that, the top left side position fixed mounting of initial storehouse (1) has material mouth (2), the left side position fixed mounting of initial storehouse (1) has power access mouth (3), the right side position fixed mounting of material mouth (2) has transmission pipe (4), the positive central point position fixed mounting of initial storehouse (1) has switch controller (5), the right side position fixed connection of transmission pipe (4) has treatment reaction chamber (6), the top left side position fixed mounting of treatment reaction chamber (6) has reaction solvent mouth (7), the right rear side position fixed mounting of reaction solvent mouth (7) has access water pipe (8), the right side position fixed mounting of reaction solvent mouth (7) has clarifier (9), the treatment reaction bin (6) is fixedly provided with a data display table (10) in the middle of the front surface, and the lower right side of the treatment reaction bin (6) is fixedly connected with a purification outlet (11).

2. The solvent S-270 purification apparatus according to claim 1, wherein a bin (101) is fixedly installed at the upper left position inside the primary bin (1), a material port (2) is fixedly connected to the top end of the bin (101), a power pump (102) is fixedly connected to the bottom end of the bin (101), and a water molecule filter screen (103) is fixedly connected to the right side of the bin (101).

3. The solvent S-270 purification apparatus as claimed in claim 2, wherein the compression box (104) is fixedly connected to the upper right position of the water molecule filter screen (103), the fixing base (105) is fixedly connected to the bottom end position of the compression box (104), the fixing base (105) and the compression box (104) are vertically distributed in the center, and the guide pipe (106) is fixedly connected to the right side position of the compression box (104).

4. The solvent S-270 purification device according to claim 1, wherein the solvent tube (601) is fixedly connected to the left upper end of the interior of the treatment reaction bin (6), the stirring box (602) is fixedly connected to the bottom end of the solvent tube (601), the reaction purification box (603) is fixedly connected to the bottom end of the stirring box (602), the heater (604) is fixedly installed at the bottom end of the reaction purification box (603), and the heater (604) and the reaction purification box (603) are distributed in parallel.

5. The solvent S-270 purification device according to claim 1, wherein a water pipe (605) is connected to the middle position inside the treatment reaction chamber (6) in a penetrating manner, a condensing tank (606) is fixedly connected to the bottom end of the water pipe (605), the condensing tank (606) is fixedly connected with the condensing filter (607), and an outlet (608) is fixedly connected to the right side position of the condensing filter (607).

6. The solvent S-270 purification device according to claim 4, wherein the reaction purification box (603) is fixedly connected with a reaction gas pipe (901) at a right end position, a solid-liquid filter (902) is fixedly connected with a top end position of the reaction gas pipe (901), a recovery pipeline (903) is fixedly connected with a left middle position of the solid-liquid filter (902), a gas pipeline (904) is fixedly connected with a top end position of the solid-liquid filter (902), and the reaction gas pipe (901), the recovery pipeline (903) and the gas pipeline (904) are vertically distributed with the solid-liquid filter (902) as a center.

7. The purification device of the solvent S-270 of claim 1, wherein the bottom end of the purifier (9) is fixedly connected with a gas pipeline (904), the interior of the purifier (9) is fixedly provided with a plurality of layers of filtering layers (905), and the top end of the plurality of layers of filtering layers (905) is fixedly connected with a purification outlet (906).

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