CN213556260U - Condensation, drop catching, gas-water separation device for preparing deuterium gas by electrolyzing deuterium water - Google Patents
Condensation, drop catching, gas-water separation device for preparing deuterium gas by electrolyzing deuterium water Download PDFInfo
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- CN213556260U CN213556260U CN202022330379.6U CN202022330379U CN213556260U CN 213556260 U CN213556260 U CN 213556260U CN 202022330379 U CN202022330379 U CN 202022330379U CN 213556260 U CN213556260 U CN 213556260U
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Abstract
The utility model discloses a condensation catching and dripping gas-water separation device for preparing deuterium gas by electrolyzing deuterium water, which relates to the technical field of preparing deuterium gas by electrolyzing heavy water, and comprises a heating mechanism and a condensation catching and dripping mechanism, wherein the heating mechanism comprises a heating pipe, a pipe plate is arranged in the heating pipe, the bottom of the pipe plate is provided with a first water outlet, one end of the heating pipe is provided with a first air inlet, and the other end of the heating pipe is provided with a first air outlet, the condensation catching and dripping mechanism comprises a cylinder body, a condensation pipe, a catching and dripping net and a saddle ring, the cylinder body is internally provided with the condensation pipe, the catching and dripping net and the saddle ring from top to bottom in sequence, deuterium gas passes through the pipe plate and the saddle ring to realize the first separation effect, further water-vapor separation is realized by the catching and dripping net again, deuterium gas reaches the condensation pipe, the residual hotter water vapor is cooled and changed into water drops, deuterium gas is discharged from a second, further separation is achieved, thereby increasing the purity of the deuterium gas.
Description
Technical Field
The utility model relates to an electrolysis deuterium gas preparation technical field, concretely relates to condensation of electrolysis deuterium gas preparation deuterium gas catches a water separator.
Background
The deuterium gas is prepared by electrolyzing heavy water, which is a convenient deuterium gas preparation method, an alkaline solution of the heavy water is pumped into an electrolytic cell, and the deuterium gas and oxygen are obtained through electrolysis, but because a large amount of heat is generated during electrolysis, the moisture content in the obtained deuterium gas is high, the purity of the deuterium gas is seriously influenced, and a simple method for filtering water vapor is urgently needed to obtain the high-purity deuterium gas.
SUMMERY OF THE UTILITY MODEL
In view of the problems existing in the prior art, the object of the utility model is to provide a condensation catch drop gas-water separation device for preparing deuterium gas by electrolyzing deuterium water, which has the characteristics of simple structure, simple operation and good separation effect.
The condensation drip-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized by comprising a heating mechanism and a condensation drip-catching mechanism, wherein the heating mechanism comprises a heating pipe, a pipe plate is arranged in the heating pipe, a first water outlet is formed in the bottom of the pipe plate, a first air inlet is formed in one end of the heating pipe, a first air outlet is formed in the other end of the heating pipe, the condensation drip-catching mechanism comprises a barrel body, a condensation pipe, a drip-catching net and a saddle ring, the condensation pipe, the drip-catching net and the saddle ring are sequentially arranged in the barrel body from top to bottom, a second air outlet and a second water outlet are respectively formed in the top and the bottom of the barrel body, a second air inlet is formed in the side face of the barrel body, and the first air outlet is connected with the second air.
The condensation and drop catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that the condensation pipe is provided with dense holes which are vertically stacked, and the mesh number of the holes is 150.
The condensation and drip-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that the mesh number of the drip-catching net is 200 meshes, and the drip-catching net is fixed on a cylinder body through welding.
The condensation and drop catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that the diameter of the saddle ring is 1.49-1.53 cm.
The condensation and droplet-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that the diameter of the second gas outlet, the diameter of the second gas inlet and the diameter of the second water outlet are all 5 cm.
The condensation and drop catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that the diameter of the cylinder body is 9.8-10.6cm, and the length of the cylinder body is 49.5-50.2 cm.
The condensation and drop catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that a group of round holes are formed in the surface of a tube plate, the round holes are distributed on the surface of the tube plate in an array shape, and the diameter of each round hole is 2 mm.
The condensation and droplet-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that the diameter of the first water outlet is 3cm, and the diameter of the first air inlet is 5 cm.
The condensation, catch-drop and gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that a heating sleeve is arranged outside a heating pipe, a heating wire is arranged inside the heating pipe, the length of the heating wire is 15cm, and the diameter of the heating wire is 7 cm.
The condensation and drop-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized in that a condensation pipe comprises a condensation pipe inlet and a condensation pipe outlet, the condensation pipe inlet and the condensation pipe outlet are respectively positioned on two sides of the upper part of a cylinder body, and the condensation pipe inlet and the condensation pipe outlet are both connected with a condensation pump.
Compared with the prior art, the beneficial effects of the utility model are that:
1) the utility model discloses the first air inlet, tube sheet and saddle ring that set up, the deuterium gas of preparation is behind the washing tank, and the steam content in the deuterium gas is high, and the deuterium gas that contains a large amount of steam passes through the tube sheet earlier behind first air inlet, and the round hole on tube sheet surface has obstructed partly the water droplet that is greater than its diameter, and the water droplet that is kept off is discharged through first delivery port, and the deuterium gas gets into saddle ring department, and the water droplet that steam is great can be stopped by the saddle ring, realizes first step separation;
2) the utility model discloses the net is dripped in catching that sets up, condenser pipe and second gas outlet, after the great water droplet of vapor in the deuterium gas is blockked by the saddlering, gas entering is subsequently caught and is dripped the net, because it is less to catch the net aperture of dripping to block vapor, realize further separation effect, reach the condenser pipe when the deuterium gas, remaining hotter vapor meets cold and becomes the water droplet, the deuterium gas is discharged from the second gas outlet, gas-liquid separation's effect has been realized, thereby the purity of deuterium gas has been improved.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention;
fig. 2 is a schematic top view of the tube sheet of the present invention;
fig. 3 is a schematic top view of the condenser tube of the present invention.
In the figure: 1-a heating mechanism; 2-a condensation drip catching mechanism; 3-heating the tube; 4-a tube plate; 5-a first water outlet; 6-a first air inlet; 7-a first air outlet; 8-barrel body; 9-a condenser pipe; 10-a drip catching net; 11-saddle ring; 12-a second outlet; 13-a second water outlet; 14-a second air inlet; 15-holes; 16-a circular hole; 17-inlet of condenser tube; 18-condenser outlet.
Detailed Description
The invention will be further described with reference to the accompanying drawings, but the scope of protection of the invention is not limited to the scope described.
As shown in fig. 1-3, a condensation droplet-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water comprises a heating mechanism 1 and a condensation droplet-catching mechanism 2, wherein the heating mechanism 1 comprises a heating pipe 3, a pipe plate 4 is arranged in the heating pipe 3, a first water outlet 5 is arranged at the bottom of the pipe plate 4, the diameter of the first water outlet 5 in this embodiment is 2.9-3.2cm, preferably 3cm, a first air inlet 6 is arranged at one end of the heating pipe 3, the diameter of the first air inlet 6 in this embodiment is 5cm, a first air outlet 7 is arranged at the other end of the first air inlet, a group of round holes are arranged on the surface of the pipe plate 4, round holes 16 are distributed on the surface of the pipe plate 4 in an array shape, and the diameter.
The utility model discloses a condensation of electrolysis deuterium water preparation deuterium gas catches drips air water separator, including the heating jacket, the heating jacket sets up in the outside of heating pipe 3, and the inside of heating pipe 3 is equipped with the heater strip, and the length of heater strip is 15cm in this embodiment, and its diameter is 7 cm.
The utility model discloses a condensation of electrolysis deuterium water preparation deuterium gas is caught and is dripped gas-water separation equipment, condensation are caught and are dripped mechanism 2 and include barrel 8, condenser pipe 9, catch and drip net 10 and saddle ring 11, and the diameter of barrel 8 is 9.8-10.6cm, preferably 10cm, and its length is 49.5-50.2cm, preferably 50 cm.
The utility model discloses a condensation of electrolysis deuterium water preparation deuterium gas is caught and is dripped gas-water separation equipment, the inside of barrel 8 is from last to being equipped with the condenser pipe 9 down in proper order, catch and drip net 10 and saddle ring 11, condenser pipe 9 is equipped with perpendicular accumulational intensive hole 15, the mesh number of hole 15 is 150 meshes, the mesh number of catching and dripping net 10 is 200 meshes, and the material of catching and dripping net 10 is the polypropylene fiber, alkali resistance has, catch in this embodiment and drip net 10 through welded fastening in barrel 8, the diameter of saddle ring 11 is 1.49-1.53cm, preferably 1.5cm, the material of saddle ring 11 is pottery in this embodiment.
The utility model discloses a condensation of electrolysis deuterium water preparation deuterium gas catches a water gas-water separation device, the top and the bottom of barrel 8 are equipped with second gas outlet 12 and second delivery port 13 respectively, and the side of barrel 8 is equipped with second air inlet 14, and first gas outlet 7 is connected with second air inlet 14, and the diameter of second gas outlet 12 in this embodiment, the diameter of second air inlet 14 and the diameter of second delivery port are 5cm, the utility model discloses the second delivery port 13 that sets up, the log raft of the saddle ring of being convenient for by the interception is discharged.
The utility model discloses a condensation of electrolysis deuterium water preparation deuterium gas is caught and is dripped gas-water separation equipment, condenser pipe 9 include condenser pipe import 17 and condenser pipe export 18, and condenser pipe import 17 and condenser pipe export 18 are located the both sides on the upper portion of barrel 8 respectively, and condenser pipe import 17 all is connected with the condensate pump with condenser pipe export 18, and the condensate liquid is the ethanol in this embodiment.
Specifically, after the prepared deuterium gas passes through a washing tank, the deuterium gas contains a large amount of water vapor, the deuterium gas containing a large amount of water vapor enters the heating mechanism 1 through the first air inlet 6, the deuterium gas entering the heating mechanism 1 firstly passes through the tube plate 4, under the action of the round hole 16 on the surface of the tube plate 4, a part of water drops larger than the diameter of the round hole 16 in the deuterium gas are blocked on the surface of the tube plate 4, the blocked water drops are discharged through the first water outlet 5, the deuterium gas is discharged from the first air outlet 7 and enters the cylinder 8 through the second air inlet 14, the deuterium gas reaches the saddle ring 11, the water drops with larger water vapor in the deuterium gas are blocked by the saddle ring 11 to realize primary separation, the deuterium gas passes through the droplet catching net 10, the mesh number of the droplet net 10 is 200 meshes, the water vapor is effectively and conveniently blocked to realize further separation, when the deuterium gas reaches the condenser pipe 9, the condensate enters from the condenser pipe inlet 17, the deuterium gas is discharged from the condensation pipe outlet 18 after passing through the condensation pipe 9, and then enters the condensation pipe inlet 17 again after being circulated by the condensation pump, the residual hotter water vapor is changed into water drops when being cooled, the deuterium gas is discharged from the second gas outlet 12, and the water drops and the water vapor blocked by the drip catching net 10 and the saddle ring 11 are discharged through the second water outlet 13, so that the gas-liquid separation effect is realized, and the purity of the deuterium gas is improved.
Claims (10)
1. A condensation, drip and gas-water separation device for preparing deuterium gas by electrolyzing deuterium water is characterized by comprising a heating mechanism (1) and a condensation drip mechanism (2), wherein the heating mechanism (1) comprises a heating pipe (3), a pipe plate (4) is arranged in the heating pipe (3), a first water outlet (5) is formed in the bottom of the pipe plate (4), a first air inlet (6) is formed in one end of the heating pipe (3), a first air outlet (7) is formed in the other end of the heating pipe, the condensation drip mechanism (2) comprises a cylinder body (8), a condensation pipe (9), a drip catching net (10) and a saddle ring (11), the condensation pipe (9), the drip catching net (10) and the saddle ring (11) are sequentially arranged in the cylinder body (8) from top to bottom, a second air outlet (12) and a second water outlet (13) are respectively formed in the top and the bottom of the cylinder body (8), and a second air inlet (14) is formed in the side surface of the cylinder body (8), and the first air outlet (7) is connected with the second air inlet (14) through a pipeline.
2. The condensation, drip-catching, gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1 wherein said condenser tube (9) is provided with vertically packed dense holes (15), said holes (15) having a mesh number of 150.
3. The condensation water-drop-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1 wherein the mesh number of said water-drop-catching net (10) is 200 mesh, said water-drop-catching net (10) is fixed to the cylinder (8) by welding.
4. The condensation, drip-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1 wherein said saddle ring (11) has a diameter of 1.49-1.53 cm.
5. The condensed drop-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1, wherein the diameter of said second outlet port (12), the diameter of said second inlet port (14) and the diameter of said second outlet port are all 5 cm.
6. The condensation, drip-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1 wherein the diameter of said cylinder (8) is 9.8-10.6cm and its length is 49.5-50.2 cm.
7. The condensation, droplet-catching, gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1, wherein the surface of said tube plate (4) is provided with a set of circular holes, said circular holes (16) are distributed on the surface of said tube plate (4) in an array, and the diameter of said circular holes (16) is 2 mm.
8. The condensation, droplet-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1 wherein the diameter of said first water outlet (5) is 3cm and the diameter of said first gas inlet (6) is 5 cm.
9. The condensation, droplet-catching, gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1, wherein said heating tube (3) is provided with a heating jacket on the outside and a heating wire on the inside, said heating wire having a length of 15cm and a diameter of 7 cm.
10. The condensation droplet-catching gas-water separation device for preparing deuterium gas by electrolyzing deuterium water as claimed in claim 1, wherein said condensation tube (9) comprises a condensation tube inlet (17) and a condensation tube outlet (18), said condensation tube inlet (17) and said condensation tube outlet (18) are respectively located at two sides of the upper portion of said cylinder (8), said condensation tube inlet (17) and said condensation tube outlet (18) are both connected to a condensation pump.
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CN202022330379.6U CN213556260U (en) | 2020-10-19 | 2020-10-19 | Condensation, drop catching, gas-water separation device for preparing deuterium gas by electrolyzing deuterium water |
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CN202022330379.6U CN213556260U (en) | 2020-10-19 | 2020-10-19 | Condensation, drop catching, gas-water separation device for preparing deuterium gas by electrolyzing deuterium water |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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JP7441369B1 (en) | 2023-10-30 | 2024-02-29 | 岩谷産業株式会社 | Deuterium production equipment |
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JP7441369B1 (en) | 2023-10-30 | 2024-02-29 | 岩谷産業株式会社 | Deuterium production equipment |
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