CN213475849U - Purification device of choline - Google Patents
Purification device of choline Download PDFInfo
- Publication number
- CN213475849U CN213475849U CN202021946274.7U CN202021946274U CN213475849U CN 213475849 U CN213475849 U CN 213475849U CN 202021946274 U CN202021946274 U CN 202021946274U CN 213475849 U CN213475849 U CN 213475849U
- Authority
- CN
- China
- Prior art keywords
- box
- gas
- separation
- choline
- butt joint
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229960001231 choline Drugs 0.000 title claims abstract description 26
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 238000000746 purification Methods 0.000 title claims description 13
- 238000000926 separation method Methods 0.000 claims abstract description 61
- 239000007788 liquid Substances 0.000 claims abstract description 32
- 238000009434 installation Methods 0.000 claims abstract description 22
- 239000011347 resin Substances 0.000 claims abstract description 9
- 229920005989 resin Polymers 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- 210000001503 joint Anatomy 0.000 claims description 24
- 230000007704 transition Effects 0.000 claims description 11
- 238000007789 sealing Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 abstract description 5
- 239000004065 semiconductor Substances 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 14
- 239000007789 gas Substances 0.000 description 11
- 239000000243 solution Substances 0.000 description 10
- 230000008569 process Effects 0.000 description 8
- 230000009471 action Effects 0.000 description 4
- 239000011261 inert gas Substances 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 229910001424 calcium ion Inorganic materials 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- WTJKGGKOPKCXLL-RRHRGVEJSA-N phosphatidylcholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCCC=CCCCCCCCC WTJKGGKOPKCXLL-RRHRGVEJSA-N 0.000 description 2
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 231100000086 high toxicity Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 150000003248 quinolines Chemical class 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 1
Images
Landscapes
- Gas Separation By Absorption (AREA)
Abstract
The utility model discloses a choline purifying device, which comprises an installation box, a plurality of separating columns, a gas pressurizing device and a gas-liquid separating device, the mounting box is a rectangular box body, a plurality of separation columns are embedded between the opposite wall surfaces of the mounting box, the gas pressurizing device is arranged on one side of the installation box, the gas-liquid separating device is arranged on the opposite side of the gas pressurizing device, the utility model relates to the technical field of processing equipment for preparing auxiliary materials for precision semiconductors, the choline purifying device utilizes a series-type pressurization system to ensure that the solution mixed with choline rapidly passes through a plurality of separation columns under the pressurization condition, then gas-liquid separation is carried out, the flow velocity of the choline passing through the resin column is increased, the contact rate is accelerated, meanwhile, the contact area is increased, so that the treatment is quicker, the efficiency is higher, the whole structure of the equipment is simple, the operation is convenient, and the efficiency-cost ratio is good.
Description
Technical Field
The utility model relates to an accurate semiconductor preparation auxiliary material processing equipment technical field specifically is a purification device of choline.
Background
Electronic products such as semiconductor devices and integrated circuits have been developed for some purposes, and the cleaning process used in the production still continues to be a conventional cleaning process for over 40 years. Conventional cleaning processes typically use chemicals such as sulfuric acid, hydrochloric acid, hydrogen peroxide, ammonia, toluene, trichloroethylene, trichloroethane, and freon. The reagents are high in cost, have strong corrosive action and high toxicity, harm the safety and health of operators and pollute the environment.
The existing choline purification method is characterized in that an aqueous solution slowly passes through a purified water resin column to remove calcium ions and corresponding complex anions to obtain a phosphatidylcholine aqueous solution free of calcium ions, and then phosphatidylcholine is separated out in a crystallization mode.
SUMMERY OF THE UTILITY MODEL
Not enough to prior art, the utility model provides a purification device of choline has solved current equipment and has used the resin post to separate, and solution is slower through the speed of resin post, has restricted the problem of the separation and purification speed of equipment.
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes: a choline purification device comprises an installation box, a plurality of separation columns, a gas pressurizing device and a gas-liquid separation device, wherein the installation box is a box body with a rectangular structure, the separation columns are embedded between opposite wall surfaces of the installation box, the gas pressurizing device is installed on one side of the installation box, the gas-liquid separation device is installed on the opposite side of the gas pressurizing device, a plurality of through grooves are formed in the separation columns, the through grooves penetrate through the separation columns, and a plurality of discharge holes which are distributed in an annular array are communicated with the through grooves;
the gas pressurizing device includes: the device comprises a butt joint box, a plurality of water inlet grooves, a water inlet, a plurality of air inlet pipes, an air supply bottle and a plurality of connecting pipes;
the butt joint box is installed in install bin one side, and is a plurality of the separation column tip is equipped with a plurality of intake tanks, and is a plurality of the intake tank communicates with a plurality of through grooves, be equipped with the water inlet on the butt joint box, be equipped with a plurality of intake pipes in the butt joint box, it is a plurality of intake pipe and intake tank butt joint, butt joint box one side is equipped with the air supply bottle, the air supply bottle is with a plurality of communicate through a plurality of connecting pipes between the intake pipe.
Preferably, the gas-liquid separation device includes: the device comprises a transition pipe, a separation box, an air suction pump, an air suction nozzle, a liquid level sensor and a water outlet;
the improved oil-water separator is characterized in that a transition pipe is arranged on one side wall surface of the bottom end of the installation box, a separation box is arranged on one opposite side of the installation box and the butt joint box, an air suction pump is arranged on the separation box, an air suction nozzle is arranged on the upper wall of the separation box and communicated with the air suction nozzle, a liquid level sensor is arranged on the bottom surface of the separation box, and a water outlet is formed in the separation box.
Preferably, the separation box is a rectangular box body with a sealing cover hinged to the top end, and a plurality of support legs extend from the bottom surface of the separation box and are supported on the ground.
Preferably, the separation columns are cylindrical structural bodies made of resin, the water inlet groove is a tapered groove with a variable diameter structure, and one end with a smaller inner diameter of the tapered groove is communicated with the through groove.
Preferably, all be equipped with the control valve on transition pipe, water inlet and the outlet, be equipped with a plurality of governing valves on a plurality of connecting pipes.
Advantageous effects
The utility model provides a purification device of choline. The method has the following beneficial effects: this purification device of choline utilizes the turbocharging system of serial-type for mixed solution of choline passes through a plurality of separation columns fast under the pressure boost condition, then carries out gas-liquid separation again, has increased the velocity of flow that choline passes through the resin post, accelerates rate of contact, increases area of contact simultaneously, makes to handle more fast, and efficiency is higher, and equipment overall structure is simple, and convenient operation has good effect and costs and compares.
Drawings
Fig. 1 is a schematic view of a front sectional view of a choline purifying device of the present invention.
Figure 2 is a side view of the choline purification device of the present invention.
Fig. 3 is a schematic view of a partial cross-sectional structure of a choline purifying device according to the present invention.
In the figure: 1. installing a box; 2. a separation column; 3. passing through the slot; 4. a discharge hole; 5. a butt-joint box; 6. a water inlet groove; 7. a water inlet; 8. an air inlet pipe; 9. an air supply bottle; 10. a connecting pipe; 11. a transition duct; 12. a separation tank; 13. an air pump; 14. a suction nozzle; 15. a liquid level sensor; 16. a water outlet; 17. a control valve; 18. and adjusting the valve.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
All the electrical components in the present application are connected with the power supply adapted to the electrical components through a wire, and an appropriate controller and an appropriate encoder should be selected according to actual conditions to meet control requirements, and specific connection and control sequences should be obtained.
Example (b): as can be known from the attached drawings 1-3 of the specification, the choline purifying device comprises an installation box 1, a plurality of separation columns 2, a gas pressurizing device and a gas-liquid separating device, wherein the installation box 1 is a rectangular box body, the separation columns 2 are embedded between opposite wall surfaces of the installation box 1, the gas pressurizing device is installed on one side of the installation box 1, the gas-liquid separating device is installed on the opposite side of the gas pressurizing device, a plurality of through grooves 3 are formed in the separation columns 2, the through grooves 3 penetrate through the separation columns 2, a plurality of discharge holes 4 which are distributed in an annular array are communicated with the through grooves 3, in the specific implementation process, the separation columns 2 are in butt joint with the gas pressurizing device, gas is injected and pressurized into the separation columns 2 through the gas-pressure pressurizing device, so that gas-liquid mixed flow entering the separation columns 2 is in a high-pressure state, on one hand, the contact area of the liquid and the separation columns 2 is, on the other hand, the gas-liquid mixture can directly pass through the tail end of the groove 3 and then is discharged from the plurality of discharge holes 4, and after the gas-liquid mixture flows into the installation box 1 from the discharge holes 4, the gas-liquid mixture is gathered in the installation box 1 and then flows into the gas-liquid separation device for gas-liquid separation;
as can be seen from fig. 1 to 3 of the specification, the gas pressurizing device comprises: the butt joint box 5, a plurality of water inlet grooves 6, a water inlet 7, a plurality of air inlet pipes 8, an air supply bottle 9 and a plurality of connecting pipes 10 are connected in the following relation and position relation;
the butt joint box 5 is installed on one side of the installation box 1, a plurality of water inlet grooves 6 are formed in the end portions of the separation columns 2, the water inlet grooves 6 are communicated with the through grooves 3, a water inlet 7 is formed in the butt joint box 5, a plurality of air inlet pipes 8 are arranged in the butt joint box 5, the air inlet pipes 8 are in butt joint with the water inlet grooves 6, an air supply bottle 9 is arranged on one side of the butt joint box 5, and the air supply bottle 9 is communicated with the air inlet pipes 8 through a plurality of connecting pipes 10;
in the specific implementation in-process, butt joint box 5 constitutes a rectangle cavity box independent of install bin 1 with the sealed butt joint of install bin 1 based on the lateral wall of install bin 1, after injecting the material through water inlet 7, the material enters into through groove 3 in through intake tank 6, simultaneously gas supply bottle 9 opens, inject inert gas into intake pipe 8 through connecting pipe 10, inert gas mixed solution enters into through groove 3 from intake tank 6 jointly, inert gas lets in the solution on the one hand, reduce the solution volume that the single passes through the bubble that produces, increase the area of contact of solution and detached column 2, increase water pressure simultaneously, the velocity of flow of pressure boost solution accelerates through efficiency.
Preferably, as can be seen from fig. 1 to 3 of the specification, the gas-liquid separation device includes: the transition pipe 11, the separation box 12, the air suction pump 13, the air suction nozzle 14, the liquid level sensor 15 and the water discharge port 16 are connected and positioned as follows;
a transition pipe 11 is arranged on the wall surface of one side of the bottom end of the installation box 1, a separation box 12 is arranged on one side of the installation box 1 opposite to the butt joint box 5, an air suction pump 13 is arranged on the separation box 12, an air suction nozzle 14 is arranged on the upper wall of the separation box 12, the air suction pump 13 is communicated with the air suction nozzle 14, a liquid level sensor 15 is arranged on the bottom surface of the separation box 12, and a water outlet 16 is arranged on the separation box 12;
in the specific implementation process, the solution is gathered in the installation box 1 and is introduced into the separation box 12 from the transition pipe 11, the inert gas mixed in the solution floats upwards to expose the surface of the solution, and then is recovered under the suction of the suction pump 13, and meanwhile, the liquid level sensor 15 detects the height of the liquid level surface, so that the liquid in the separation box 12 is subjected to volume control, and the liquid is discharged from the water discharge port 16 when the liquid is accumulated too much.
Preferably, the separation box 12 is a rectangular box body with a top end hinged with a sealing cover, and a bottom surface extends with a plurality of support legs to be supported on the ground, the sealing cover is used for sealing the separation box 12, and the support legs at the bottom end are used for supporting the separation box 12 to be lifted off the ground.
As preferred scheme, further, a plurality of separation post 2 are the cylindrical structure body of resin material, and intake chamber 6 is the toper recess of reducing structure, and the less one end of toper recess internal diameter communicates with through groove 3, utilizes the venturi principle, reduces the water pressure in 8 tip backs of intake pipe, increases rivers and enters into the speed through groove 3.
Preferably, the transition pipe 11, the water inlet 7 and the water outlet 16 are all provided with control valves 17, and the plurality of connecting pipes 10 are provided with a plurality of regulating valves 18.
To sum up, this purification device of choline utilizes serial-type turbocharging system for the solution that mixes choline passes through a plurality of separation columns 2 fast under the pressure boost condition, then carries out gas-liquid separation again, has increased the velocity of flow that choline passed through the resin post for contact rate increases area of contact simultaneously, makes the processing faster, and efficiency is higher, and equipment overall structure is simple, and convenient operation has good effect to cost than.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation. The use of the phrase "comprising one of the elements does not exclude the presence of other like elements in the process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (5)
1. A choline purification device comprises an installation box (1), a plurality of separation columns (2), a gas pressurizing device and a gas-liquid separation device, and is characterized in that the installation box (1) is a rectangular box body, the separation columns (2) are embedded between opposite wall surfaces of the installation box (1), the gas pressurizing device is installed on one side of the installation box (1), the gas-liquid separation device is installed on one opposite side of the gas pressurizing device, a plurality of through grooves (3) are formed in the separation columns (2), the through grooves (3) penetrate through the separation columns (2), and the through grooves (3) are communicated with a plurality of discharge holes (4) which are distributed in an annular array;
the gas pressurizing device includes: the device comprises a butt joint box (5), a plurality of water inlet grooves (6), a water inlet (7), a plurality of air inlet pipes (8), an air supply bottle (9) and a plurality of connecting pipes (10);
butt joint case (5) are installed in install bin (1) one side, and are a plurality of separation post (2) tip is equipped with a plurality of intake chambers (6), and is a plurality of intake chamber (6) and a plurality of trough (3) intercommunication of passing through, be equipped with water inlet (7) on butt joint case (5), be equipped with a plurality of intake pipes (8) in butt joint case (5), and is a plurality of intake pipe (8) and intake chamber (6) butt joint, butt joint case (5) one side is equipped with gas supply bottle (9), gas supply bottle (9) and a plurality of communicate through a plurality of connecting pipes (10) between intake pipe (8).
2. The apparatus for purifying choline according to claim 1, wherein the gas-liquid separating device comprises: the device comprises a transition pipe (11), a separation box (12), an air suction pump (13), an air suction nozzle (14), a liquid level sensor (15) and a water outlet (16);
install bin (1) bottom lateral wall face is equipped with transition pipe (11), install bin (1) is equipped with separator box (12) with butt joint box (5) opposition one side, be equipped with aspiration pump (13) on separator box (12), suction mouth (14) have been seted up to separator box (12) upper wall, aspiration pump (13) and suction mouth (14) intercommunication, separator box (12) bottom surface is equipped with level sensor (15), be equipped with outlet (16) on separator box (12).
3. The choline purifying device as claimed in claim 2, wherein the separation tank (12) is a rectangular box with a sealing cover hinged to the top and a plurality of feet extending from the bottom to support on the ground.
4. The choline purification device according to claim 1, wherein the separation columns (2) are cylindrical structures made of resin, the water inlet groove (6) is a tapered groove with a diameter-variable structure, and one end of the tapered groove with a smaller inner diameter is communicated with the through groove (3).
5. A choline purifying device according to claim 2, wherein the transition pipe (11), the water inlet (7) and the water outlet (16) are all provided with control valves (17), and the connecting pipes (10) are provided with adjusting valves (18).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021946274.7U CN213475849U (en) | 2020-09-08 | 2020-09-08 | Purification device of choline |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021946274.7U CN213475849U (en) | 2020-09-08 | 2020-09-08 | Purification device of choline |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213475849U true CN213475849U (en) | 2021-06-18 |
Family
ID=76418414
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021946274.7U Active CN213475849U (en) | 2020-09-08 | 2020-09-08 | Purification device of choline |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213475849U (en) |
-
2020
- 2020-09-08 CN CN202021946274.7U patent/CN213475849U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1269575C (en) | Method and device for fluid inflation | |
| CN102701307B (en) | Wastewater ammonia nitrogen blow-off treatment reaction device | |
| WO2004071635A1 (en) | Method, device, and system for controlling dissolved amount of gas | |
| KR20200031649A (en) | Water treatment membrane cleaning device and cleaning method | |
| CN213475849U (en) | Purification device of choline | |
| CN202594818U (en) | Waste water ammonia nitrogen blowoff reaction device | |
| CN209128082U (en) | A kind of combination defoaming device for landfill leachate | |
| US5980613A (en) | Pressurized radon stripper | |
| US5336402A (en) | Sewage treatment apparatus | |
| CN202297196U (en) | Rotary flow flotation device for treating oily wastewater | |
| CN210543502U (en) | Resin regeneration treatment device for natural product separation and purification | |
| CN114477504A (en) | Dynamic separation and recovery device and driving and controlling method for water-based paint cleaning solvent | |
| CN1210092A (en) | Water treatment process by jet gas soluted floatation | |
| DE3865995D1 (en) | MOBILE DEVICE FOR SUCTIONING HARMFUL LIQUIDS. | |
| CN202717734U (en) | Energy-saving protein skimmer | |
| CN206607046U (en) | High efficient horizontal dissolving | |
| KR200258000Y1 (en) | bubble separate apparatus for circulation filtering type | |
| CN218709677U (en) | Saturated dissolved oxygen aeration device | |
| KR20170065142A (en) | Sludge flotation system using gas solution equipment | |
| JP3778184B2 (en) | Gas dissolving device | |
| CN220723874U (en) | Sewage treatment system | |
| CN203307145U (en) | Efficient air flotation device | |
| JPH1015580A (en) | Float type water area purifying apparatus | |
| CN219701167U (en) | Vacuum air-liquid separator | |
| CN111620403B (en) | Method for eliminating bubbles in ozone water liquid for crystal silicon surface treatment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20231127 Address after: Room 501, Floor 5, Building 4, No. 85, Mingnan Road, Songjiang District, Shanghai, 201600 Patentee after: Shanghai Xirun Electronic Materials Co.,Ltd. Address before: 201500 G8, room 505, 5th floor, No.13 Lane 16299, Puwei Road, Yang Town, Jinshan District, Shanghai Patentee before: Shi run Chemical Technology (Shanghai) Co.,Ltd. |