CN213467807U - Automatic batching system of acetylation material - Google Patents
Automatic batching system of acetylation material Download PDFInfo
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- CN213467807U CN213467807U CN202022392404.3U CN202022392404U CN213467807U CN 213467807 U CN213467807 U CN 213467807U CN 202022392404 U CN202022392404 U CN 202022392404U CN 213467807 U CN213467807 U CN 213467807U
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- cauldron
- kettle
- pipeline
- proportioning
- acetylation
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Abstract
The utility model discloses an automatic batching system of acetylated materials, comprising an acetyl reaction kettle and a batching kettle, wherein the acetyl reaction kettle and the batching kettle are arranged side by side, a material transferring kettle is arranged between the acetyl reaction kettle and the batching kettle, a first pipeline is arranged on one side surface of the material transferring kettle, the other end of the first pipeline is communicated with the acetyl reaction kettle, a second pipeline is fixed on the other side surface of the material transferring kettle, and the other end of the second pipeline is communicated with the batching kettle; through being provided with material cauldron, second pipeline, electric heat tracing and proportioning cauldron, be convenient for avoid needing to slice through the slicer, lead to artifical intensity of labour big, cause environmental pollution to the outside, the device is simple, easy to use.
Description
Technical Field
The utility model belongs to the technical field of the material batching, concretely relates to automatic blending system of acetylation material.
Background
In the process of processing and proportioning acetylated materials, adding glacial acetic acid into o (p) aminobenzyl ether to perform a heating reaction through heat conduction oil to generate o (p) ethyl ether aminobenzyl ether, slowly putting the o (p) acetamino methyl ether into a material transferring kettle, cooling and slicing the o (p) acetamino methyl ether in a slicer, packaging and weighing to obtain an intermediate product, keeping the o (p) acetamino methyl ether for later use, performing nitration reaction in the next procedure, putting the weighed o (p) acetamino methyl ether into a nitration reaction kettle according to a specified amount, adding a solvent dichloromethane according to a certain proportion, stirring, heating, and dropwise adding nitric acid to perform nitration reaction.
When the existing automatic batching system for acetylated materials is used, the materials need to be manually and slowly placed into a slicing machine for cooling and slicing, the labor intensity of workers is greatly increased, pollution can be caused to the outer side, the using effect is not good, cooling and slicing are not convenient to reduce, and therefore the automatic batching system for acetylated materials is provided.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide an automatic blending system of acetylation material to the automatic blending system who proposes current acetylation material in solving above-mentioned background art when using, the material needs the manual work to slowly put into the slicer and cools off the section, very big increase artifical intensity of labour, and still can cause the pollution to the outside, the result of use is not good, is not convenient for reduce the sliced problem of cooling.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides an automatic blending system of acetylation material, includes acetyl reaction cauldron and proportioning cauldron, acetyl reaction cauldron sets up side by side with the proportioning cauldron, the material cauldron of changeing has been installed between acetyl reaction cauldron and the proportioning cauldron, it is provided with first pipeline to change material cauldron side surface, the first pipeline other end and acetyl reaction cauldron intercommunication, it is fixed with the second pipeline to change material cauldron opposite side surface, the second pipeline other end and proportioning cauldron intercommunication, second pipeline outside cover is equipped with the electric tracing.
Preferably, the electric tracing is strip-shaped, and the electric tracing is uniformly distributed around the second pipeline.
Preferably, the top end of the material transferring kettle is fixed with a motor, the lower end of the motor is provided with a stirring rod, and the stirring rod extends into the inner side of the material transferring kettle.
Preferably, the lower end of one side surface of the proportioning pot is provided with a discharge pipe, and the discharge pipe is communicated with the inside of the proportioning pot.
Preferably, the upper end of the acetyl reaction kettle is provided with a maintenance manhole, and a sealing plate is fixed at the top end of the maintenance manhole.
Compared with the prior art, the beneficial effects of the utility model are that:
through being provided with material cauldron, second pipeline, electric tracing and proportioning cauldron, be convenient for avoid needing to slice through the slicer, lead to artifical intensity of labour big, cause environmental pollution to the outside, the device is simple, and accessible electric tracing reduces the pipe blockage, easy to use.
Drawings
Fig. 1 is a schematic structural view of the present invention;
in the figure: 1. an acetyl reaction kettle; 2. a first conduit; 3. transferring the material to a kettle; 4. a second conduit; 5. a dosing kettle; 6. electric tracing; 7. an electric motor.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1, the present invention provides a technical solution: the utility model provides an automatic blending system of acetylation material, including acetyl reaction cauldron 1 and proportioning cauldron 5, acetyl reaction cauldron 1 sets up side by side with proportioning cauldron 5, it changes material cauldron 3 to have installed between acetyl reaction cauldron 1 and the proportioning cauldron 5, be convenient for store the material, 3 side surfaces of material cauldron are provided with first pipeline 2 to change, the 2 other ends of first pipeline and 1 intercommunication of acetyl reaction cauldron, it flows into material cauldron 3 inboards to be convenient for make acetyl reaction cauldron 1 material, it is fixed with second pipeline 4 to change material cauldron 3 opposite side surfaces, the 4 other ends of second pipeline and proportioning cauldron 5 intercommunication, be convenient for make the material flow out from material cauldron 3 that changes, 4 outside covers of second pipeline are equipped with companion's electric heat 6, be convenient for heat second pipeline 4, it solidifies to reduce the material and causes the jam.
In this embodiment, preferably, the electric tracing 6 is in a strip shape, and the electric tracing 6 is uniformly distributed around the second pipeline 4, so as to heat the second pipeline 4 more uniformly.
In this embodiment, preferred, 3 tops of material transferring kettle are fixed with motor 7, and 7 lower extremes of motor are provided with the puddler, and the puddler stretches into material transferring kettle 3 inboardly, is convenient for stir material transferring kettle 3 inboardly.
In this embodiment, preferably, the lower end of one side surface of the dosing kettle 5 is provided with a discharge pipe, and the discharge pipe is communicated with the inside of the dosing kettle 5, so that the materials can be discharged better.
In this embodiment, preferably, the upper end of the acetyl reaction kettle 1 is provided with a maintenance manhole, and a sealing plate is fixed at the top end of the maintenance manhole, so that the maintenance of the inner side of the acetyl reaction kettle 1 is facilitated.
The utility model discloses a theory of operation and use flow: when in use, the o-p-anisidine and the glacial acetic acid which are used as raw materials are subjected to acylation reaction to produce the o-p-acetamino anisole, pressing o-p-acetamino anisole into a material transferring kettle 3 by nitrogen, newly configuring a proportioning kettle 5, firstly adding a solvent dichloromethane into the proportioning kettle 5 according to a certain material proportion, heating and stirring, then slowly adding o-p-acetamino anisole into the proportioning kettle 5, opening a jacket for cooling by cold water, preparing o-p-acetamino anisole solution by the o-p-acetamino anisole and the dichloromethane solvent, the mixture is transferred into a standby storage tank through a pump, is pumped into a nitration kettle according to a certain amount, is added with nitric acid dropwise for nitration, and is not required to be sliced by a slicing machine, so that the labor intensity of workers is reduced, the environmental pollution is avoided, and the solidifying point of the material is higher, an electric tracing heat 6 is added on the second pipeline 4 between the material transferring kettle 3 and the proportioning kettle 5, so that the second pipeline 4 is prevented from being blocked.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (5)
1. The utility model provides an automatic blending system of acetylation material, includes acetyl reaction cauldron (1) and volume of proportioning cauldron (5), acetyl reaction cauldron (1) sets up its characterized in that side by side with volume of proportioning cauldron (5): install between acetyl reaction cauldron (1) and the batching cauldron (5) and change material cauldron (3), change material cauldron (3) side surface and be provided with first pipeline (2), first pipeline (2) other end and acetyl reaction cauldron (1) intercommunication, change material cauldron (3) opposite side surface and be fixed with second pipeline (4), second pipeline (4) other end and batching cauldron (5) intercommunication, second pipeline (4) outside cover is equipped with electric heat tracing (6).
2. An automated acetylation material dosing system according to claim 1, wherein: the electric tracing heat (6) is strip-shaped, and the electric tracing heat (6) is uniformly distributed around the second pipeline (4).
3. An automated acetylation material dosing system according to claim 1, wherein: the material transferring kettle is characterized in that a motor (7) is fixed at the top end of the material transferring kettle (3), a stirring rod is arranged at the lower end of the motor (7), and the stirring rod extends into the inner side of the material transferring kettle (3).
4. An automated acetylation material dosing system according to claim 1, wherein: and a discharge pipe is arranged at the lower end of the surface of one side of the proportioning pot (5), and the discharge pipe is communicated with the inside of the proportioning pot (5).
5. An automated acetylation material dosing system according to claim 1, wherein: a maintenance manhole is arranged at the upper end of the acetyl reaction kettle (1), and a sealing plate is fixed at the top end of the maintenance manhole.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022392404.3U CN213467807U (en) | 2020-10-23 | 2020-10-23 | Automatic batching system of acetylation material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022392404.3U CN213467807U (en) | 2020-10-23 | 2020-10-23 | Automatic batching system of acetylation material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213467807U true CN213467807U (en) | 2021-06-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022392404.3U Active CN213467807U (en) | 2020-10-23 | 2020-10-23 | Automatic batching system of acetylation material |
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| Country | Link |
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| CN (1) | CN213467807U (en) |
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2020
- 2020-10-23 CN CN202022392404.3U patent/CN213467807U/en active Active
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