CN213376604U - Device for synthesizing methyl phenyl silicone oil - Google Patents
Device for synthesizing methyl phenyl silicone oil Download PDFInfo
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- CN213376604U CN213376604U CN202021808890.6U CN202021808890U CN213376604U CN 213376604 U CN213376604 U CN 213376604U CN 202021808890 U CN202021808890 U CN 202021808890U CN 213376604 U CN213376604 U CN 213376604U
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- reaction kettle
- water inlet
- water outlet
- hot water
- cooling water
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Abstract
The utility model relates to a device for synthesizing methyl phenyl silicone oil, which comprises a reaction kettle, wherein a plurality of feed pipes are arranged on a top cover of the reaction kettle, a valve 201 and a flowmeter 202 are arranged on the feed pipes, a stirring paddle is also arranged in the reaction kettle, the upper part of the stirring paddle passes through the top cover to be connected with a motor 4, the reaction kettle is connected with a reflux tower 5 through a pipeline, the reflux tower 5 is connected with a condenser 6 through a pipeline, an exhaust port 601 of the condenser 6 is connected with a waste gas treatment device, and the lower end of the condenser 6 is connected with a liquid recovery tank 7 through a pipeline; the bottom surface of the reaction kettle 1 is provided with a discharge outlet 101, the bottom surface is further provided with a plurality of U-shaped pipes 8, and the U-shaped pipes 8 are provided with a water inlet 801 and a water outlet 802; the side wall of the reaction kettle 1 is provided with an interlayer 102, and the interlayer 9 is provided with a cooling water inlet 901, a cooling water outlet 902, a hot water inlet 903 and a hot water outlet 904. The utility model discloses the structure sets up ingenious, energy-efficient, is suitable for wide application.
Description
Technical Field
The utility model relates to a chemical industry equipment technical field, concretely relates to equipment of synthetic methyl phenyl silicone oil.
Background
The polysiloxane with the main chain composed of methyl phenyl siloxane chain units is solid regardless of the degree of polymerization, and is not in the category of silicone oil. The linear methyl phenyl silicone oil can be regarded as a product of methyl silicone oil with part of methyl substituted by phenyl, and has the advantages of high temperature resistance, irradiation resistance, lubricating property, high refractive index and the like. During the synthesis process of the methyl phenyl silicone oil, the temperature needs to be accurately controlled, so that the generation of byproducts is reduced. The existing synthesis equipment can not accurately control the temperature, thereby bringing the problems of more byproducts, low yield, high temperature control cost and the like of the methyl phenyl silicone oil. Therefore, it is necessary to design a device for synthesizing methyl phenyl silicone oil, so as to realize flexible temperature adjustment.
SUMMERY OF THE UTILITY MODEL
In order to solve the problems existing in the prior art, the utility model provides a device for synthesizing methyl phenyl silicone oil, the concrete technical scheme is as follows:
the device for synthesizing methyl phenyl silicone oil comprises a reaction kettle (1), wherein a plurality of feeding pipes (2) are arranged on a top cover of the reaction kettle (1), valves (201) and flow meters (202) are arranged on the feeding pipes (2), a stirring paddle (3) is further arranged in the reaction kettle (2), the upper part of the stirring paddle (3) penetrates through the top cover to be connected with a motor (4),
the reaction kettle (2) is connected with a reflux tower (5) through a pipeline, the reflux tower (5) is connected with a condenser (6) through a pipeline, an exhaust port (601) of the condenser (6) is connected with a waste gas treatment device, and the lower end of the condenser (6) is connected with a liquid recovery tank (7) through a pipeline;
a discharge outlet (101) is formed in the bottom surface of the reaction kettle (1), a plurality of U-shaped pipes (8) are further arranged on the bottom surface, and a water inlet (801) and a water outlet (802) are formed in each U-shaped pipe (8);
the side wall of the reaction kettle (1) is provided with an interlayer (102), the interlayer (9) is provided with a cooling water inlet (901), a cooling water outlet (902), a hot water inlet (903) and a hot water outlet (904), and the cooling water inlet (901), the cooling water outlet (902), the hot water inlet (903) and the hot water outlet (904) are respectively connected with a cooling water tank (10) and a hot water tank (11) through pipelines.
Further, reation kettle (1) in install thermodetector (12), reation kettle (1) the lateral wall on be provided with display screen (13), thermodetector (12) with display screen (13) electricity be connected.
Furthermore, a water inlet (801) and a water outlet (802) of the U-shaped pipe (8) are respectively connected with a cooling water tank (10) or a hot water tank (11).
The utility model has the advantages that: the utility model provides a set up a plurality of condensations in the synthesizer and with irritate U type pipe, can adjust cooling water and hydrothermal proportion in U type pipe and the intermediate layer at any time according to the temperature that thermodetector detected to adjustment reation kettle's temperature reachs quick, high-efficient temperature regulation's purpose, and the energy can be saved. The utility model discloses the structure sets up ingenious, energy-efficient, is suitable for wide application.
Drawings
Fig. 1 is a schematic structural diagram of an apparatus for synthesizing methyl phenyl silicone oil according to an embodiment of the present invention.
The system comprises a reaction kettle, a discharge port, a feeding pipe, a valve, a flow meter, a stirring paddle, a motor, a reflux tower, a condenser, a gas exhaust port, a liquid recovery tank, a 8-U-shaped pipe, a 801-water inlet, an 802-water outlet, a 9-interlayer, a cooling water inlet, a cooling water outlet, a 903-hot water inlet, a hot water outlet, a 904-hot water outlet, a 10-cooling water tank, a 11-hot water tank, a 12-temperature detector and a 13-display screen, wherein the reaction kettle is 1-arranged, the discharge port is 101-arranged, the feeding pipe is 2-arranged, the valve is 201-arranged, the flow meter is 202-arranged.
The specific implementation mode is as follows:
in order to deepen understanding of the present invention, the following detailed description is made on the embodiments of the present invention with reference to the accompanying drawings.
It should be understood that the structure, ratio, size and the like shown in the drawings attached to the present specification are only used for matching with the content disclosed in the specification, so as to be known and read by those skilled in the art, and are not used for limiting the limit conditions that the present invention can be implemented, so that the present invention has no technical essential meaning, and any structure modification, ratio relation change or size adjustment should still fall within the scope that the technical content disclosed in the present invention can cover without affecting the function and the achievable purpose of the present invention.
Examples
With reference to figure 1 of the drawings,
an apparatus for synthesizing methyl phenyl silicone oil comprises a reaction kettle 1, a plurality of feed pipes 2 are arranged on a top cover of the reaction kettle 1, a valve 201 and a flowmeter 202 are arranged on the feed pipes 2, a stirring paddle 3 is also arranged in the reaction kettle 2, the upper part of the stirring paddle 3 passes through the top cover to be connected with a motor 4,
the reaction kettle 2 is connected with a reflux tower 5 through a pipeline, the reflux tower 5 is connected with a condenser 6 through a pipeline, an exhaust port 601 of the condenser 6 is connected with a waste gas treatment device, and the lower end of the condenser 6 is connected with a liquid recovery tank 7 through a pipeline;
the bottom surface of the reaction kettle 1 is provided with a discharge outlet 101, the bottom surface is further provided with a plurality of U-shaped pipes 8, and the U-shaped pipes 8 are provided with a water inlet 801 and a water outlet 802;
the side wall of the reaction kettle 1 is provided with an interlayer 102, the interlayer 9 is provided with a cooling water inlet 901, a cooling water outlet 902, a hot water inlet 903 and a hot water outlet 904, and the cooling water inlet 901, the cooling water outlet 902, the hot water inlet 903 and the hot water outlet 904 are respectively connected with a cooling water tank 10 and a hot water tank 11 through pipelines.
Further, a temperature detector 12 is installed in the reaction kettle 1, a display screen 13 is arranged on the side wall of the reaction kettle 1, and the temperature detector 12 is electrically connected with the display screen 13.
Further, the water inlet 801 and the water outlet 802 of the U-shaped pipe 8 are respectively connected with the cooling water tank 10 or the hot water tank 11.
The technical means disclosed by the scheme of the utility model is not limited to the technical means disclosed by the technical means, but also comprises the technical scheme consisting of the equivalent replacement of the technical features. The present invention is not to be considered as the best thing, and belongs to the common general knowledge of the technicians in the field.
Claims (3)
1. The device for synthesizing methyl phenyl silicone oil is characterized by comprising a reaction kettle (1), wherein a plurality of feeding pipes (2) are arranged on a top cover of the reaction kettle (1), valves (201) and flow meters (202) are arranged on the feeding pipes (2), a stirring paddle (3) is further arranged in the reaction kettle (1), the upper part of the stirring paddle (3) penetrates through the top cover to be connected with a motor (4),
the reaction kettle (1) is connected with a reflux tower (5) through a pipeline, the reflux tower (5) is connected with a condenser (6) through a pipeline, an exhaust port (601) of the condenser (6) is connected with a waste gas treatment device, and the lower end of the condenser (6) is connected with a liquid recovery tank (7) through a pipeline;
a discharge outlet (101) is formed in the bottom surface of the reaction kettle (1), a plurality of U-shaped pipes (8) are further arranged on the bottom surface, and a water inlet (801) and a water outlet (802) are formed in each U-shaped pipe (8);
the side wall of the reaction kettle (1) is provided with an interlayer (9), the interlayer (9) is provided with a cooling water inlet (901), a cooling water outlet (902), a hot water inlet (903) and a hot water outlet (904), and the cooling water inlet (901), the cooling water outlet (902), the hot water inlet (903) and the hot water outlet (904) are respectively connected with a cooling water tank (10) and a hot water tank (11) through pipelines.
2. The apparatus for synthesizing methyl phenyl silicone oil according to claim 1, wherein a temperature detector (12) is installed in the reaction kettle (1), a display screen (13) is arranged on the side wall of the reaction kettle (1), and the temperature detector (12) is electrically connected with the display screen (13).
3. The apparatus for synthesizing methyl phenyl silicone oil according to claim 1, wherein the water inlet (801) and the water outlet (802) of the U-shaped pipe (8) are respectively connected with a cooling water tank (10) or a hot water tank (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021808890.6U CN213376604U (en) | 2020-08-26 | 2020-08-26 | Device for synthesizing methyl phenyl silicone oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021808890.6U CN213376604U (en) | 2020-08-26 | 2020-08-26 | Device for synthesizing methyl phenyl silicone oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213376604U true CN213376604U (en) | 2021-06-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021808890.6U Active CN213376604U (en) | 2020-08-26 | 2020-08-26 | Device for synthesizing methyl phenyl silicone oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213376604U (en) |
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2020
- 2020-08-26 CN CN202021808890.6U patent/CN213376604U/en active Active
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