CN213314959U - Synthetic reaction kettle for producing diphenyl chlorophosphate - Google Patents

Abstract

The utility model belongs to the technical field of chemical production, in particular to a synthetic reaction kettle for producing diphenyl chlorophosphate, which comprises a reaction kettle body, wherein a sound insulation layer is fixedly arranged on the inner side wall of the reaction kettle body, the inner side wall of the sound insulation layer is fixedly provided with the inner wall of the reaction kettle, the top end surface of the reaction kettle body is fixedly connected with an upper cover through a bolt, and a through hole is arranged at the central position of the top end surface of the upper cover; after the filling is accomplished, open gear motor this moment, and then drive the stirring leaf and stir the reaction to the solution in the reactor, realize the rotatory operation of stirring leaf in the reactor, keep away from the reation kettle inner wall because of the reactor, just the fixed puigging that is equipped with of inside wall of reation kettle body, the fixed reation kettle inner wall that is equipped with of inside wall of puigging, and then reduce the reaction and produce the noise, after accomplishing the reaction, electric putter work this moment, and then drive fourth connecting rod pulling closure plate, and then make the reactor open, make the reaction liquid flow to next process from the discharge pipe.

Description

Synthetic reaction kettle for producing diphenyl chlorophosphate

Technical Field

The utility model belongs to the technical field of chemical production, concretely relates to production diphenyl chlorophosphate uses synthetic reation kettle.

Background

The reaction kettle is an important device in the chemical industry, is a heart of the whole chemical process flow, has a stainless steel container for physical or chemical reaction by the generalized understanding of the reaction kettle, and realizes the heating, evaporation, cooling and low-speed and high-speed mixing functions required by the process by the structural design and parameter configuration of the container, and the prior art has the following problems: the existing reaction kettle does not have the function of quantitative filling, most of noises of the existing reaction kettle are loosening and loosening of the stirrer, and accessories in the friction kettle cause very large noises, so that the earplugs must be worn by workers.

In order to solve the problems, the application provides a synthesis reaction kettle for producing diphenyl chlorophosphate.

SUMMERY OF THE UTILITY MODEL

To solve the problems set forth in the background art described above. The utility model provides a production diphenyl chlorophosphate uses synthetic reation kettle, has noise reduction and quantitative filling's characteristics.

In order to achieve the above object, the utility model provides a following technical scheme: a synthetic reaction kettle for producing diphenyl chlorophosphate comprises a reaction kettle body, wherein a sound insulation layer is fixedly arranged on the inner side wall of the reaction kettle body, the inner side wall of the sound insulation layer is fixedly provided with the inner wall of the reaction kettle, the top end face of the reaction kettle body is fixedly connected with an upper cover through a bolt, a through hole is formed in the central position of the top end face of the upper cover, a sealing ring is fixedly arranged on the inner side wall of the through hole of the top end face of the upper cover, a support is fixedly arranged on the top end face of the upper cover, a connecting block is fixedly arranged on the inner side of the top end face of the support, a speed reducing motor is fixedly arranged on the top end face of the support, a rotating shaft of the speed reducing motor penetrates through the connecting block, a second connecting rod is fixedly arranged at the tail end of the rotating shaft of the speed reducing motor, a pipeline is, and extend to the inside of reactor, the fixed stirring leaf that is equipped with of another terminal surface of second connecting rod, the lateral wall top sliding connection of reactor has the closing plate, the fixed constant delivery pump that is equipped with in top face left side of support, the fixed electric putter that is equipped with in upper cover top end face right side, electric putter's flexible end is fixed with the fourth connecting rod of meshing connection type structure, the fourth connecting rod runs through the top face of upper cover, just the other end of fourth connecting rod is rotated through the pivot and is connected with the third connecting rod, the other end of third connecting rod is rotated through pivot and closing plate and is connected, the fixed discharge pipe that is equipped with of reation kettle body bottom face central point department, just the one end of discharge pipe extends to the inside of reation kettle inner wall, the other end of discharge pipe extends to the outside of reation kettle body.

As the utility model relates to a synthetic reaction kettle for producing diphenyl chlorophosphate is preferred, the quantitative pump also comprises a hollow structure box body, a first motor, a cam, a first connecting rod, a slide block, a marble and a first water pipe, the box body is fixedly connected with a bracket, the first motor is fixedly connected with the rear end face of the box body, the rotating shaft of the first motor penetrates through the box body and extends to the inner side of the box body, the cam is fixedly connected with the rotating shaft of the first motor, the first connecting rod is rotatably connected with the cam through a rotating shaft, the other end of the first connecting rod is rotatably connected with the slide block through a rotating shaft, the first water pipe is fixedly connected with the right end face of the box body, the right side wall of the box body is provided with a 'one' type chute, the slide block is positioned in the 'one' type chute, the slide block is slidably connected with the box body, the first water pipe is communicated with the 'one' type chute, the right end of the inner side of the first-shaped sliding groove of the box body is provided with a diaphragm, the diaphragm is fixedly connected with the first water pipe, and the marble is arranged inside the first water pipe.

As the utility model relates to a production diphenyl chlorophosphate is preferred with synthetic reation kettle, the reactor still includes leak protection paster, spring, the arc spout has been seted up in the lateral wall of reactor right-hand member, the closure plate is located the arc spout and reactor sliding connection, the spring is located the arc spout, the one end and the closure plate fixed connection of spring, the other end and the reactor fixed connection of spring, the leak protection paster will the closure plate is located including the part parcel of arc spout, the leak protection paster with reactor sliding connection, the through-hole has been seted up to the bottom face of reactor.

As the utility model relates to a production diphenyl chlorophosphate is preferred with synthetic reation kettle, the fixed three base that is equipped with of bottom face of reation kettle body, and three the even distribution of base is at the bottom face of reation kettle body.

As the utility model relates to a production diphenyl chlorophosphate is preferred with synthetic reation kettle, first water pipe bottom face intercommunication has the second water pipe, the other end and the pipeline intercommunication of second water pipe.

Compared with the prior art, the beneficial effects of the utility model are that: after the filling is accomplished, open gear motor this moment, and then drive the stirring leaf and stir the reaction to the solution in the reactor, realize the rotatory operation of stirring leaf in the reactor, keep away from the reation kettle inner wall because of the reactor, just the fixed puigging that is equipped with of inside wall of reation kettle body, the fixed reation kettle inner wall that is equipped with of inside wall of puigging, and then reduce the reaction and produce the noise, after accomplishing the reaction, electric putter work this moment, and then drive fourth connecting rod pulling closure plate, and then make the reactor open, make the reaction liquid flow to next process from the discharge pipe, because of the through-hole inside wall fixedly connected with sealing washer of upper cover terminal surface, this setting ensures that outside air can not enter into reation kettle.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention. In the drawings:

fig. 1 is a schematic structural view of the present invention;

fig. 2 is a schematic top view of the present invention;

FIG. 3 is a schematic structural view of a reactor according to the present invention;

FIG. 4 is an enlarged schematic structural view of the position A of the present invention;

fig. 5 is a schematic structural view of the middle connection member of the present invention.

In the figure: 1. a reaction kettle body; 2. a sound insulating layer; 3. the inner wall of the reaction kettle; 4. an upper cover; 401. a seal ring; 5. a handle; 6. a support; 601. connecting blocks; 7. a constant delivery pump; 701. a box body; 702. a first motor; 703. a cam; 704. a first connecting rod; 705. a slider; 706. a diaphragm; 707. a marble; 708. a first water pipe; 8. a reduction motor; 9. a pipeline; 10. a second connecting rod; 11. stirring blades; 12. a reactor; 1201. an arc-shaped chute; 1202. leak-proof paster; 1203. a spring; 1204. a closing plate; 13. a third connecting rod; 14. a fourth connecting rod; 15. an electric push rod; 16. a discharge pipe; 17. a base; 18. a second water pipe.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Example 1

As shown in fig. 1, 3 and 5;

fig. 1 is a schematic structural view of the present invention;

FIG. 3 is a schematic structural view of a reactor according to the present invention;

FIG. 5 is a schematic structural view of the middle connection member of the present invention

A synthetic reaction kettle for producing diphenyl chlorophosphate comprises a reaction kettle body 1, wherein a sound insulation layer 2 is fixedly arranged on the inner side wall of the reaction kettle body 1, a reaction kettle inner wall 3 is fixedly arranged on the inner side wall of the sound insulation layer 2, an upper cover 4 is fixedly connected to the top end face of the reaction kettle body 1 through a bolt 5, a through hole is formed in the central position of the top end face of the upper cover 4, a sealing ring 401 is fixedly arranged on the inner side wall of the through hole of the top end face of the upper cover 4, a support 6 is fixedly arranged on the top end face of the upper cover 4, a connecting block 601 is fixedly arranged on the inner side of the top end face of the support 6, a speed reducing motor 8 is fixedly arranged on the top end face of the support 6, a rotating shaft of the speed reducing motor 8 penetrates through the connecting block 601, a second connecting rod 10 is fixedly arranged at the tail end of the rotating shaft of the speed, and extend to the inside of reactor 12, the other end face of second connecting rod 10 is fixedly provided with stirring vane 11, outer side wall top of reactor 12 is connected with closing plate 1204 in a sliding manner, top end face left side of support 6 is fixedly provided with dosing pump 7, top end face right side of upper cover 4 is fixedly provided with electric push rod 15, telescopic end of electric push rod 15 is fixedly provided with fourth connecting rod 14 of meshing connection type structure, fourth connecting rod 14 penetrates through top end face of upper cover 4, and the other end of fourth connecting rod 14 is connected with third connecting rod 13 through the pivot rotation, the other end of third connecting rod 13 is connected with closing plate 1204 through the pivot rotation, bottom end face central position department of reation kettle body 1 is fixedly provided with discharge pipe 16, and one end of discharge pipe 16 extends to the inside of reation kettle inner wall 3, the other end of discharge pipe 16 extends to the outside of reation kettle body 1.

It should be noted that: in this embodiment, the aperture of the position where the marble 707 is provided inside the first water pipe 708 is larger than that of the other places.

In an embodiment: after the filling is accomplished, gear motor 8 is opened this moment, and then drive stirring leaf 11 and stir the reaction to the solution in reactor 12, realize the rotatory operation of stirring leaf 11 in reactor 12, reation kettle inner wall 3 is kept away from because of reactor 12, and reation kettle body 1's inside wall is fixed and is equipped with puigging 2, the fixed reation kettle inner wall 3 that is equipped with of inside wall of puigging 2, and then reduce the reaction and produce the noise, after accomplishing the reaction, electric putter 15 work this moment, and then drive fourth connecting rod 14 pulling closure plate 1204, and then make reactor 12 open, make the reaction liquid flow out to next process from discharge pipe 16, because of the through-hole inside wall fixedly connected with sealing washer 401 of upper cover 4 top terminal surface, this setting ensures that outside air can not enter into reation kettle.

As shown in fig. 1 and 4;

fig. 1 is a schematic structural view of the present invention;

fig. 4 is an enlarged schematic structural diagram of the position a of the present invention.

In an alternative embodiment, the fixed displacement pump 7 further includes a box 701, a first motor 702, a cam 703, a first connecting rod 704, a sliding block 705, a marble 707, and a first water pipe 708, the box 701 is fixedly connected to the bracket 6, the first motor 702 is fixedly connected to the rear end surface of the box 701, a rotating shaft of the first motor 702 penetrates through the box 701 and extends to the inner side of the box 701, the cam 703 is fixedly connected to the rotating shaft of the first motor 702, the first connecting rod 704 is rotatably connected to the cam 703 through a rotating shaft, the first water pipe 708 is fixedly connected to the right end surface of the box 701, a "one" type chute is formed in the right side wall of the box 701, the sliding block 705 is located in the "one" type chute, the sliding block is slidably connected to the box 701, the first water pipe 708 is communicated with the "one" type chute of the box 701, a diaphragm 706 is disposed at the right end of the inner side of the "one" type chute of the box 701, the diaphragm, a marble 707 is provided inside the first water pipe 708.

In this embodiment: the staff opens the first motor 702, drives the cam 703 rotatory this moment, and then drives the spout of first connecting rod 704 on the box 701 and slide, and then extrudes the air between slider 705 and the diaphragm 706, and then makes marble 707 float from top to bottom, realizes the quantitative filling operation of solution from first water pipe 708 every time.

As shown in fig. 1 and 3;

fig. 1 is a schematic structural view of the present invention;

fig. 3 is a schematic structural diagram of the reactor of the present invention.

In an optional embodiment, the reactor 12 further includes a leakage-proof patch 1202 and a spring 1203, an arc chute 1201 is formed in an outer side wall of a right end of the reactor 12, a closing plate 1204 is located in the arc chute 1201 and slidably connected with the reactor 12, the spring 1203 is located in the arc chute 1201, one end of the spring 1203 is fixedly connected with the closing plate 1204, the other end of the spring 1203 is fixedly connected with the reactor 12, the leakage-proof patch 1202 wraps a portion of the closing plate 1204 located in the arc chute 1201, the leakage-proof patch 1202 is slidably connected with the reactor 12, and a through hole is formed in a bottom end face of the reactor 12.

It should be noted that: the closing plate 1204 is always in a closed state under the action of the spring 1203, when the closing plate 1204 is closed, the leakage-proof patches 1202 enable the through hole of the reactor 12 to be in a sealed state, and when the closing plate 1204 is opened, the solution in the reactor 12 can be discharged through the through hole of the reactor 12.

In this embodiment: when the staff fills the solution, the reactor 12 is closed, and after filling is completed, the closing plate 1204 is pulled, so that the closing plate 1204 slides to open the through hole on the bottom end surface of the reactor 12, which is blocked, and the arrangement ensures the tightness of the reactor 12.

As shown in fig. 1;

fig. 1 is a schematic structural diagram of the present invention.

In an alternative embodiment, three bases 17 are fixedly arranged on the bottom end surface of the reaction kettle body 1, and the three bases 17 are uniformly distributed on the bottom end surface of the reaction kettle body 1.

In this embodiment: this arrangement facilitates securing the base 17.

As shown in fig. 1;

fig. 1 is a schematic structural diagram of the present invention.

In an alternative embodiment, the bottom end face of the first water pipe 708 is communicated with the second water pipe 18, and the other end of the second water pipe 18 is communicated with the pipeline 9.

In this embodiment: this arrangement facilitates the entry of the solution filled by the staff member from the first water pipe 708 into the reactor 12 through the pipe 9.

The utility model discloses a theory of operation and use flow: place this device at the workplace, after the filling is accomplished, turn on gear motor 8 this moment, and then drive stirring leaf 11 and stir the reaction to the solution in reactor 12, realize the rotatory operation of stirring leaf 11 in reactor 12, keep away from reation kettle inner wall 3 because of reactor 12, and reation kettle body 1's inside wall is fixed and is equipped with puigging 2, the fixed reation kettle inner wall 3 that is equipped with of inside wall of puigging 2, and then reduce the reaction and produce the noise, after accomplishing the reaction, electric putter 15 works this moment, and then drive fourth connecting rod 14 pulling closure plate 1204, and then make reactor 12 open, make the reaction liquid flow out to next process from discharge pipe 16, because of the through-hole inside wall fixedly connected with sealing washer 401 of upper cover 4 top terminal surface, this setting ensures that the outside air can not enter into reation kettle.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (5)

1. The utility model provides a production diphenyl chlorophosphate uses synthetic reation kettle, includes reation kettle body (1) and bolt (5), its characterized in that: the inner side wall of the reaction kettle body (1) is fixedly provided with a sound insulation layer (2), the inner side wall of the sound insulation layer (2) is fixedly provided with a reaction kettle inner wall (3), the top end face of the reaction kettle body (1) is fixedly connected with an upper cover (4) through a bolt (5), the central position of the top end face of the upper cover (4) is provided with a through hole, the inner side wall of the through hole of the top end face of the upper cover (4) is fixedly provided with a sealing ring (401), the top end face of the upper cover (4) is fixedly provided with a support (6), the inner side of the top end face of the support (6) is fixedly provided with a connecting block (601), the top end face of the support (6) is fixedly provided with a speed reducing motor (8), the rotating shaft of the speed reducing motor (8) penetrates through the connecting block (601), the tail end of the rotating shaft of the speed reducing motor (8) is, the second connecting rod (10) is arranged on the inner side of the pipeline (9), the other end of the pipeline (9) is communicated with a reactor (12), the second connecting rod (10) extends to the inside of the reactor (12), the other end face of the second connecting rod (10) is fixedly provided with a stirring blade (11), the right upper part of the outer side wall of the reactor (12) is slidably connected with a closing plate (1204), the left side of the top end face of the bracket (6) is fixedly provided with a dosing pump (7), the right side of the top end face of the upper cover (4) is fixedly provided with an electric push rod (15), the telescopic end of the electric push rod (15) is fixedly provided with a fourth connecting rod (14) of a meshing connection type structure, the fourth connecting rod (14) penetrates through the top end face of the upper cover (4), and the other end of the fourth connecting rod (14) is rotatably connected with a third connecting rod (13) through, the other end of third connecting rod (13) is connected with closure plate (1204) rotation through the pivot, fixed discharge pipe (16) that is equipped with of reation kettle body (1) bottom end face central point department, just the one end of discharge pipe (16) extends to the inside of reation kettle inner wall (3), the other end of discharge pipe (16) extends to the outside of reation kettle body (1).

2. The synthesis reaction kettle for producing diphenyl chlorophosphate according to claim 1, wherein: the quantitative pump (7) further comprises a box body (701) with a hollow structure, a first motor (702), a cam (703), a first connecting rod (704), a sliding block (705), a marble (707) and a first water pipe (708), wherein the box body (701) is fixedly connected with a support (6), the first motor (702) is fixedly connected with the rear end face of the box body (701), a rotating shaft of the first motor (702) penetrates through the box body (701) and extends to the inner side of the box body (701), the cam (703) is fixedly connected with the rotating shaft of the first motor (702), the first connecting rod (704) is rotatably connected with the cam (703) through a rotating shaft, the other end of the first connecting rod (704) is rotatably connected with the sliding block (705) through a rotating shaft, the first water pipe (708) is fixedly connected with the right end face of the box body (701), a 'one' type chute is formed in the right side wall of the box body (701), the sliding block (705) is positioned in the one-shaped sliding groove, the sliding block (705) is connected with the box body (701) in a sliding mode, the first water pipe (708) is communicated with the one-shaped sliding groove of the box body (701), a diaphragm (706) is arranged at the right end of the inner side of the one-shaped sliding groove of the box body (701), the diaphragm (706) is fixedly connected with the first water pipe (708), and the marble (707) is arranged inside the first water pipe (708).

3. The synthesis reaction kettle for producing diphenyl chlorophosphate according to claim 1, wherein: the reactor (12) further comprises a leakage-proof patch (1202) and a spring (1203), an arc-shaped chute (1201) is formed in the outer side wall of the right end of the reactor (12), the closing plate (1204) is positioned in the arc-shaped chute (1201) and is in sliding connection with the reactor (12), the spring (1203) is positioned in the arc-shaped chute (1201), one end of the spring (1203) is fixedly connected with the closing plate (1204), the other end of the spring (1203) is fixedly connected with the reactor (12), the leakage-proof patch (1202) wraps the part, positioned in the arc-shaped chute (1201), of the closing plate (1204), the leakage-proof patch (1202) is in sliding connection with the reactor (12), a through hole is formed in the bottom end face of the reactor (12), the closing plate (1204) is always in a closed state under the elastic action of the spring (1203), and when the closing plate (1204) is closed, the leakage-proof patch (1202) enables the through hole of the reactor (12) to be in a sealed state, and when the closing plate (1204) is opened, the solution in the reactor (12) can be discharged through the through hole of the reactor (12).

4. The synthesis reaction kettle for producing diphenyl chlorophosphate according to claim 1, wherein: the bottom end face of reation kettle body (1) is fixed and is equipped with three base (17), and three base (17) even distribution is at the bottom end face of reation kettle body (1).

5. The synthesis reaction kettle for producing diphenyl chlorophosphate according to claim 2, wherein: the bottom end face of the first water pipe (708) is communicated with a second water pipe (18), and the other end of the second water pipe (18) is communicated with a pipeline (9).

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