CN213159467U - High-content geniposide crystallization preparation facilities - Google Patents

High-content geniposide crystallization preparation facilities Download PDF

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Publication number
CN213159467U
CN213159467U CN202021222422.0U CN202021222422U CN213159467U CN 213159467 U CN213159467 U CN 213159467U CN 202021222422 U CN202021222422 U CN 202021222422U CN 213159467 U CN213159467 U CN 213159467U
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fixedly connected
crystallizer
crystallization
content
filter frame
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CN202021222422.0U
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Chinese (zh)
Inventor
谈满良
罗炼辉
李小冬
吴建忠
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Nanjing Kangqi Bio Tech Co ltd
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Nanjing Kangqi Bio Tech Co ltd
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Abstract

The utility model discloses a high content geniposide crystallization preparation facilities, including the crystallizer, crystallizer top block is connected with the top cap, the upper surface central point of top cap puts and runs through the rotation and is connected with the puddler, the surface cover of the one end that the puddler is located the crystallizer inside is equipped with multiunit stirring leaf, the puddler is located the one end surface of crystallizer inside and is close to the symmetry fixedly connected with horizontal pole of top cap. The utility model discloses in, the motor rotates and drives the stirring leaf and rotate, the stirring leaf rotates and makes the material fully contact, thereby further improvement the speed of crystallization, the spiral leaf rotates and to stir the material in the discharging tube, thereby avoid extravagant, the utilization ratio of material is improved, first scraping the crystal of flitch on the crystallizer inner wall strikes off, the second scrapes the crystallization of flitch to the inside bottom of crystallizer and strikes off, thereby can avoid the crystallization to glue on the inner wall of crystallizer, the production efficiency of geniposide crystallization has been improved.

Description

High-content geniposide crystallization preparation facilities
Technical Field
The utility model relates to a geniposide crystallization preparation technical field especially relates to a high content geniposide crystallization preparation facilities.
Background
Geniposide is hydrolyzed into genipin (genipin) by beta-glucosidase, namely the geniposide can exert curative effect only after being metabolized into the genipin in intestinal tract, has the efficacies of protecting liver and benefiting gallbladder, reducing blood pressure, relaxing bowels, relieving type II diabetes, diminishing inflammation, resisting thrombus, resisting tumor, resisting aging and the like, has extremely high medicinal value, and is an effective monomer for producing intermediates and crude drugs of gardenia blue, gardenia red and gardenia purple;
the existing gardenoside crystallization preparation device is in the crystallization process, the effect of material mixing is not ideal due to the small and narrow action area of the stirring paddle, so that the crystallization efficiency is low, the material in the discharge pipe at the bottom of the device cannot be stirred, the production requirement cannot be met, the time required by stirring production is increased, the production efficiency is reduced, crystals crystallized on the inner wall of the device cannot be collected, and the material is greatly wasted.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects existing in the prior art and providing a high-content jasminoidin crystallization preparation device.
In order to achieve the above purpose, the utility model adopts the following technical scheme: a high-content geniposide crystallization preparation device comprises a crystallization tank, wherein a top cover is connected to the top of the crystallization tank in a clamping manner, the central position of the upper surface of the top cover is connected with a stirring rod in a penetrating and rotating manner, a plurality of groups of stirring blades are sleeved on the outer surface of one end of the stirring rod, which is positioned inside the crystallization tank, a cross rod is symmetrically and fixedly connected to the outer surface of one end of the stirring rod, which is positioned inside the crystallization tank, and is close to the top cover, a first scraping plate is fixedly connected to one end of the cross rod, which is close to the inner wall of the crystallization tank, one side of the outer surface of the first scraping plate is attached to the inner wall of the crystallization tank, connecting rods are symmetrically and fixedly connected to the outer surface of the bottom of the stirring rod, a second scraping plate is fixedly connected to one ends of the two connecting rods, which are far, the bottom end of the stirring rod is fixedly connected with a connecting block, the lower surface of the connecting block is fixedly connected with a rotating rod, one end of the rotating rod extends into the discharging pipe, and the outer surface of one end of the rotating rod, which is positioned in the discharge pipe, is sleeved and fixedly connected with a spiral blade, the central position of the upper surface of the top cover is fixedly provided with a mounting rack, the upper surface of the top cover is symmetrically and fixedly connected with a first feeding pipe and a second feeding pipe in a penetrating way, a control valve is fixedly arranged at the position of the discharging pipe below the rotating rod, the bottom end of the discharge pipe is fixedly connected with a filter box in a penetrating way, the interior of the filter box is connected with a filter frame in a sliding way, a filter screen is fixedly connected with the lower surface of the filter frame in an embedded manner, an opening is arranged on one side of the outer surface of the filter box, the bottom of rose box runs through fixedly connected with drain pipe, the surface cover of crystallizer is equipped with the shell.
As a further description of the above technical solution:
the lower fixed surface of mounting bracket installs the motor, the output shaft of motor and the one end fixed connection of puddler.
As a further description of the above technical solution:
the inner wall of the filter box is symmetrically and fixedly connected with sliding plates at two sides below the filter frame, and the filter frame is connected with the sliding plates in a sliding mode.
As a further description of the above technical solution:
the filter frame runs through the opening and is connected with the opening in a sliding mode, and the outer surface of the filter frame is fixedly connected with a handle close to one side of the opening.
As a further description of the above technical solution:
be equipped with the condenser pipe between shell and the crystallizer, the both ends of condenser pipe run through the shell respectively and extend to the outside of shell.
As a further description of the above technical solution:
the outer surface of the crystallizing tank is fixedly connected with a support frame at a position close to the bottom.
The utility model discloses following beneficial effect has:
1. the high-content geniposide crystal preparation device comprises a motor, a stirring rod, a stirring blade, a rotating rod, a spiral blade, a cross rod, a first scraping plate, a connecting rod and a second scraping plate, wherein materials are added into a crystallization tank through a first feeding pipe and a second feeding pipe, the motor is started, the motor rotates to drive the stirring rod and the rotating rod to rotate so as to drive the stirring blade to rotate, the stirring blade rotates to enable the materials to be in full contact, the crystallization speed is further improved, the rotating rod rotates to drive the spiral blade to rotate, the materials in the discharging pipe are stirred, waste is avoided, the utilization rate of the materials is improved, the motor rotates to drive the cross rod and the connecting rod to rotate, the first scraping plate is driven to scrape crystals on the inner wall of the crystallization tank, the connecting rod rotates to drive the second scraping plate to scrape crystals at the bottom inside the crystallization tank, and the crystals are prevented from being stuck on the inner wall of the crystallization tank, improves the production efficiency of the geniposide crystal.
2. This high content geniposide crystallization preparation facilities, discharging pipe through setting up, the dwang, the spiral leaf, the control valve, the rose box, filter frame, filter screen and handle, open the control valve after the crystallization is accomplished, make the crystal pass through in the discharging pipe gets into the filter box, filter out the geniposide crystal through the filter screen in the filter frame, the dwang rotates and drives the spiral leaf and rotates, thereby can avoid the condition that the crystal was too much stopped up the discharging pipe, pull the handle after the filtration was accomplished and take out the filter frame, and the operation is simple, the people of being convenient for operate.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of the internal structure of the filtering box of the present invention;
fig. 3 is a side view of the present invention.
Illustration of the drawings:
1. a crystallization tank; 2. a top cover; 3. a stirring rod; 4. stirring blades; 5. a cross bar; 6. a first scraper plate; 7. a connecting rod; 8. a second scraper plate; 9. a discharge pipe; 10. connecting blocks; 11. rotating the rod; 12. helical leaves; 13. a mounting frame; 14. a motor; 15. a first feed tube; 16. a second feed tube; 17. a control valve; 18. a filter box; 19. a filter frame; 20. a filter screen; 21. a slide plate; 22. an opening; 23. a handle; 24. a liquid outlet pipe; 25. a housing; 26. a condenser tube; 27. a support frame.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus, should not be construed as limiting the present invention; the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance, and furthermore, unless otherwise explicitly stated or limited, the terms "mounted," "connected," and "connected" are to be construed broadly and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-3, the present invention provides an embodiment: a high-content geniposide crystallization preparation device comprises a crystallization tank 1, a top cover 2 is connected with the top of the crystallization tank 1 in a clamping manner, the central position of the upper surface of the top cover 2 is connected with a stirring rod 3 in a penetrating and rotating manner, the outer surface of one end of the stirring rod 3, which is positioned inside the crystallization tank 1, is sleeved with a plurality of groups of stirring blades 4, the outer surface of one end of the stirring rod 3, which is positioned inside the crystallization tank 1, is symmetrically and fixedly connected with a cross rod 5, the end, which is close to the inner wall of the crystallization tank 1, of the cross rod 5 is fixedly connected with a first scraping plate 6, one side of the outer surface of the first scraping plate 6 is attached to the inner wall of the crystallization tank 1, the outer surface of the bottom end of the stirring rod 3 is symmetrically and fixedly connected with connecting rods 7, the ends, which are far away from the stirring rod 3, of the two connecting rods 7 are fixedly, the bottom end of the stirring rod 3 is fixedly connected with a connecting block 10, the lower surface of the connecting block 10 is fixedly connected with a rotating rod 11, one end of the rotating rod 11 extends to the inside of the discharging pipe 9, and dwang 11 is located the inside one end overcoat of discharging pipe 9 and establishes fixedly connected with spiral leaf 12, the last surface central point of top cap 2 puts fixed mounting has mounting bracket 13, the upper surface symmetry of top cap 2 runs through first inlet pipe 15 and the second inlet pipe 16 of fixedly connected with, discharging pipe 9 is located the fixed mounting in position of dwang 11 below has control valve 17, fixedly connected with rose box 18 is run through to the bottom of discharging pipe 9, the inside sliding connection of rose box 18 has filter frame 19, the lower surface embedding fixedly connected with filter screen 20 of filter frame 19, opening 22 has been seted up to surface one side of rose box 18, fixedly connected with drain pipe 24 is run through to the bottom of rose box 18, the surface cover of crystallizer 1 is equipped with shell 25.
The lower surface of the mounting frame 13 is fixedly provided with a motor 14, and an output shaft of the motor 14 is fixedly connected with one end of the stirring rod 3, so that the motor 14 rotates to drive the stirring rod 3 and the rotating rod 11 to rotate, and the stirring blade 4 is driven to rotate; the sliding plates 21 are symmetrically and fixedly connected to the inner wall of the filtering box 18 and the two sides of the lower part of the filtering frame 19, the filtering frame 19 is in sliding connection with the sliding plates 21, and the sliding plates 21 are used for supporting the filtering frame 19 and preventing the filtering frame 19 from falling; the filter frame 19 penetrates through the opening 22 and is connected with the opening 22 in a sliding manner, and a handle 23 is fixedly connected to the outer surface of the filter frame 19 and one side close to the opening 22, so that the filter frame 19 can be pulled out of the filter box 18 conveniently; a condensing pipe 26 is arranged between the shell 25 and the crystallization tank 1, two ends of the condensing pipe 26 respectively penetrate through the shell 25 and extend to the outside of the shell 25, and the condensing pipe 26 is used for conveniently adjusting the temperature inside the crystallization tank 1; the outer surface of the crystallization tank 1 is fixedly connected with a support frame 27 at a position close to the bottom, so that the device can be conveniently fixed.
The working principle is as follows: when the high-content geniposide crystal preparation device is used, materials are added into a crystallization tank 1 through a first feeding pipe 15 and a second feeding pipe 16, a motor 14 is started, the motor 14 rotates to drive a stirring rod 3 and a rotating rod 11 to rotate, so that the stirring blade 4 is driven to rotate, the stirring blade 4 rotates to enable the materials to be in full contact, so that the crystallization speed is further improved, the rotating rod 11 rotates to drive a spiral blade 12 to rotate, so that the materials in a discharging pipe 9 are stirred, waste is avoided, the utilization rate of the materials is improved, the motor 14 rotates to drive a cross rod 5 and a connecting rod 7 to rotate, so that a first scraping plate 6 is driven to scrape crystals on the inner wall of the crystallization tank 1, the connecting rod 7 rotates to drive a second scraping plate 8 to scrape the crystals at the bottom inside the crystallization tank 1, so that the crystals are prevented from being stuck on the inner wall of the crystallization tank 1, and the production efficiency of, open control valve 17 after the crystallization is accomplished for the crystal passes through discharging pipe 9 and gets into in the rose box 18, filters out the geniposide crystal through filter screen 20 in filtering frame 19, and dwang 11 rotates and drives spiral leaf 12 and rotate, thereby can avoid the crystal too much condition of plugging up discharging pipe 9, pull handle 23 after the completion of filtering and take out filtering frame 19, easy operation, the people's of being convenient for operation.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications and variations can be made in the embodiments or in part of the technical features of the embodiments without departing from the spirit and the scope of the invention.

Claims (6)

1. The utility model provides a high content geniposide crystallization preparation facilities, includes crystallizer (1), its characterized in that: the top of the crystallizing tank (1) is connected with a top cover (2) in a clamping manner, the upper surface center of the top cover (2) is connected with a stirring rod (3) in a penetrating and rotating manner, a plurality of groups of stirring blades (4) are sleeved on the outer surface of one end of the stirring rod (3) which is positioned in the crystallizing tank (1), the stirring rod (3) is positioned on the outer surface of one end of the crystallizing tank (1) and is close to a cross rod (5) in a symmetrical and fixedly connected manner, one end of the cross rod (5) which is close to the inner wall of the crystallizing tank (1) is fixedly connected with a first scraping plate (6), one side of the outer surface of the first scraping plate (6) is attached to the inner wall of the crystallizing tank (1), connecting rods (7) are fixedly connected with the outer surface of the bottom of the stirring rod (3) in a symmetrical manner, one ends of the two connecting rods (, the lower surface of flitch (8) is scraped to the second and the inside bottom laminating of crystallizer (1), the bottom central point of crystallizer (1) puts and runs through fixedly connected with discharging pipe (9), the bottom fixedly connected with connecting block (10) of puddler (3), the lower fixed surface of connecting block (10) is connected with dwang (11), the one end of dwang (11) extends to the inside of discharging pipe (9), just fixedly connected with spiral leaf (12) are established to the one end surface cover that dwang (11) is located discharging pipe (9) inside, the upper surface central point of top cap (2) puts fixed mounting bracket (13), the upper surface symmetry of top cap (2) runs through first inlet pipe (15) of fixedly connected with and second inlet pipe (16), position fixed mounting that discharging pipe (9) is located dwang (11) below has control valve (17), fixedly connected with rose box (18) is run through to the bottom of discharging pipe (9), the inside sliding connection of rose box (18) has filter frame (19), the lower surface embedding fixedly connected with filter screen (20) of filter frame (19), opening (22) have been seted up to surface one side of rose box (18), fixedly connected with drain pipe (24) is run through to the bottom of rose box (18), the surface cover of crystallizer (1) is equipped with shell (25).
2. The high-content jasminoidin crystal preparation device as claimed in claim 1, wherein: the lower fixed surface of mounting bracket (13) installs motor (14), the output shaft of motor (14) and the one end fixed connection of puddler (3).
3. The high-content jasminoidin crystal preparation device as claimed in claim 1, wherein: the filter box is characterized in that sliding plates (21) are symmetrically and fixedly connected to the inner wall of the filter box (18) and located on two sides of the lower portion of the filter frame (19), and the filter frame (19) is in sliding connection with the sliding plates (21).
4. The high-content jasminoidin crystal preparation device as claimed in claim 1, wherein: the filter frame (19) penetrates through the opening (22) and is in sliding connection with the opening (22), and a handle (23) is fixedly connected to the outer surface of the filter frame (19) and one side close to the opening (22).
5. The high-content jasminoidin crystal preparation device as claimed in claim 1, wherein: be equipped with condenser pipe (26) between shell (25) and crystallizer (1), both ends of condenser pipe (26) run through shell (25) respectively and extend to the outside of shell (25).
6. The high-content jasminoidin crystal preparation device as claimed in claim 1, wherein: the outer surface of the crystallizing tank (1) and the position close to the bottom are fixedly connected with a supporting frame (27).
CN202021222422.0U 2020-06-29 2020-06-29 High-content geniposide crystallization preparation facilities Active CN213159467U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113559748A (en) * 2021-08-02 2021-10-29 福建永荣科技有限公司 Caprolactam processing is with high-efficient crystal system
CN113620266A (en) * 2021-09-17 2021-11-09 安徽东至广信农化有限公司 Method for recycling phosphorous acid from dimethyl ester rectification residual liquid
CN113683069A (en) * 2021-08-23 2021-11-23 常熟市圆启晶体材料有限公司 Preparation method of monopotassium phosphate crystal and crystallization tank

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113559748A (en) * 2021-08-02 2021-10-29 福建永荣科技有限公司 Caprolactam processing is with high-efficient crystal system
CN113683069A (en) * 2021-08-23 2021-11-23 常熟市圆启晶体材料有限公司 Preparation method of monopotassium phosphate crystal and crystallization tank
CN113620266A (en) * 2021-09-17 2021-11-09 安徽东至广信农化有限公司 Method for recycling phosphorous acid from dimethyl ester rectification residual liquid

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