CN213100902U - Novel crystallization kettle capable of improving evaporation crystallization efficiency - Google Patents
Novel crystallization kettle capable of improving evaporation crystallization efficiency Download PDFInfo
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- CN213100902U CN213100902U CN201922475436.7U CN201922475436U CN213100902U CN 213100902 U CN213100902 U CN 213100902U CN 201922475436 U CN201922475436 U CN 201922475436U CN 213100902 U CN213100902 U CN 213100902U
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- 238000002425 crystallisation Methods 0.000 title claims abstract description 66
- 230000008025 crystallization Effects 0.000 title claims abstract description 66
- 238000001704 evaporation Methods 0.000 title claims abstract description 25
- 230000008020 evaporation Effects 0.000 title claims abstract description 25
- 230000007246 mechanism Effects 0.000 claims abstract description 76
- 238000003756 stirring Methods 0.000 claims abstract description 75
- 238000010438 heat treatment Methods 0.000 claims abstract description 36
- 230000005540 biological transmission Effects 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims description 19
- 238000002347 injection Methods 0.000 claims description 8
- 239000007924 injection Substances 0.000 claims description 8
- 238000003466 welding Methods 0.000 claims description 4
- 238000009413 insulation Methods 0.000 claims description 2
- 230000002093 peripheral effect Effects 0.000 claims description 2
- 239000011550 stock solution Substances 0.000 abstract description 11
- 238000007790 scraping Methods 0.000 description 14
- 239000000463 material Substances 0.000 description 8
- 238000004321 preservation Methods 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 238000000034 method Methods 0.000 description 5
- 238000004140 cleaning Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000011229 interlayer Substances 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 238000005498 polishing Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005008 domestic process Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
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Abstract
本实用新型提供一种可以提高蒸发结晶效率的新型结晶釜，涉及结晶釜技术领域。该可以提高蒸发结晶效率的新型结晶釜，包括支撑架，所述支撑架的中心固定连接有结晶罐，所述结晶罐的顶部设置有罐盖，所述罐盖的顶部设置有支撑机构，所述支撑机构的一侧设置有传动机构，所述结晶罐的中心设置有离心搅拌机构，所述离心搅拌机构的中心安装有旋转搅拌机构，所述结晶罐与离心搅拌机构之间设置有加热机构，所述罐盖顶部外表面的一侧设置有出气口，所述结晶罐外壁一侧的底部设置有控制面板。通过传动机构、离心搅拌机构、旋转搅拌机构以及自动加热机构的相互配合，可以大大提高原液的蒸发结晶效率，既节约了大量的能源，同时也保证了加工效率。
The utility model provides a novel crystallization kettle which can improve the efficiency of evaporation and crystallization, and relates to the technical field of crystallization kettles. The novel crystallization kettle which can improve the evaporative crystallization efficiency includes a support frame, the center of the support frame is fixedly connected with a crystallizing tank, the top of the crystallizing tank is provided with a tank cover, and the top of the tank cover is provided with a support mechanism, so One side of the support mechanism is provided with a transmission mechanism, the center of the crystallizing tank is provided with a centrifugal stirring mechanism, the center of the centrifugal stirring mechanism is provided with a rotating stirring mechanism, and a heating mechanism is provided between the crystallizing tank and the centrifugal stirring mechanism , one side of the outer surface of the top of the tank cover is provided with an air outlet, and the bottom of one side of the outer wall of the crystallizing tank is provided with a control panel. Through the cooperation of transmission mechanism, centrifugal stirring mechanism, rotary stirring mechanism and automatic heating mechanism, the evaporation and crystallization efficiency of the stock solution can be greatly improved, which not only saves a lot of energy, but also ensures the processing efficiency.
Description
Technical Field
The utility model relates to a crystallization kettle technical field specifically is a can improve novel crystallization kettle of evaporation crystallization efficiency.
Background
The crystallization kettle is a crystallization device which needs chilled water or refrigerant water to be rapidly cooled in an interlayer after material mixing reaction, the key links of the crystallization kettle are the size of the area of the interlayer, the structural form and the material outlet form of a stirrer, high-precision polishing in a tank body and the requirement of no dead angle during cleaning in the tank body are met, the crystallization kettle can be selected according to the technological requirements of users, the inner and outer polishing treatment of a pipe body is carried out, a heating layer is divided into a spiral belt and a jacket type, heating energy is divided into steam and electric heating for selection, a 304 material is used as a heat insulation plate and filled with a polyurethane foaming agent, a sight glass, a stirring device, a hole charging port, a tank washer, a respirator, a liquid medicine inlet, an injection water inlet, a backflow port, a steam inlet, a condensate outlet, a cooling water inlet, an outlet, a material outlet, a drain outlet, a sampling port, a temperature measuring port, The mixing reaction equipment for domestic processes of material mixing, heating, cooling, stirring and the like in the industries of pharmacy, food and the like has the advantages that due to different processes and media, the conditions of flammability, explosiveness, great toxicity, high temperature and high pressure of materials are common, the requirements of stirring form, rotating speed, heating and cooling of the equipment are different, the design and material selection, structure and speed reducer explosion-proof and non-explosion-proof requirements of the equipment are also different, so the equipment has the characteristics of normal pressure and pressure containers, and provides fundamental application for users needing the equipment.
The evaporation refers to a process of separating the solvent from the solute in the solution by heating the solvent; crystallization is a process of changing solute polymerization into solid (crystal), and an evaporative crystallization kettle is important equipment for accelerating evaporative crystallization, but the design of the existing evaporative crystallization kettle has certain defects, the evaporative crystallization efficiency is low, the energy consumption is high, and the use is very inconvenient due to inconvenience and cleaning of the interior of the evaporative crystallization kettle.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
The utility model provides a not enough to prior art, the utility model provides a can improve evaporation crystallization efficiency's novel crystallization kettle, the design of having solved present evaporation crystallization kettle also has certain defect, and evaporation crystallization efficiency is lower, and energy resource consumption is more, moreover inconvenient and rinse its inside, use very inconvenient problem.
(II) technical scheme
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes: the utility model provides a can improve evaporation crystallization efficiency's novel crystallization kettle, includes the support frame, its the central fixedly connected with crystallizer of support frame, the top of crystallizer is provided with the cover, one side at cover top is provided with annotates the liquid mouth, the top of cover is provided with supporting mechanism, one side of supporting mechanism is provided with drive mechanism, the center of crystallizer is provided with centrifugal rabbling mechanism, rotatory rabbling mechanism is installed at centrifugal rabbling mechanism's center, be provided with heating mechanism between crystallizer and the centrifugal rabbling mechanism, one side of cover top surface is provided with the gas outlet, the center of crystallizer bottom is provided with the liquid outlet corresponding with centrifugal rabbling mechanism, the thermometer is installed to one side of crystallizer outer wall, the bottom of crystallizer outer wall one side is provided with control panel.
Preferably, the support frame is fixedly connected with the crystallizing tank by welding.
Preferably, the supporting mechanism includes the connecting pipe, the top fixed block of connecting pipe is connected with the ring flange, the top fixedly connected with braced frame of ring flange, first bearing is installed at the center at braced frame top, the top cap is installed at braced frame's top, the top fixedly connected with second bearing of connecting pipe inner wall, one side fixedly connected with supporting seat of ring flange outer wall.
Preferably, the transmission mechanism comprises a servo motor, the servo motor is installed at the top of the supporting seat, one end of an output shaft of the servo motor is fixedly connected with a transmission bevel gear, and the top and the bottom of the transmission bevel gear are respectively meshed with a first bevel gear and a second bevel gear.
Preferably, centrifugal stirring mechanism includes the inner tank, the bottom fixedly connected with inner tank of second bevel gear, the top fixedly connected with of inner tank and the corresponding protection ring of notes liquid mouth, a plurality of through-holes have been seted up to the week side at inner tank top center, the bottom fixedly connected with drain pipe of inner tank, the third bearing corresponding with the drain pipe is installed to the bottom of crystallizer inner wall.
Preferably, the rotary stirring mechanism comprises a stirring shaft, the center of the first bevel gear is fixedly connected with the stirring shaft, the center of the outer wall of the stirring shaft is fixedly connected with a plurality of connecting blocks, the connecting blocks are fixedly connected with stirring rods on two sides, the stirring rods are far away from one ends of the connecting blocks and are fixedly connected with transverse scraping pieces and longitudinal scraping pieces respectively, connecting rods are fixedly connected with two sides of the outer wall of the stirring shaft and are arranged at one ends of the connecting rods far away from the stirring shaft, inclined scraping pieces are arranged at one ends of the connecting rods, and a fourth bearing corresponding to the stirring shaft is arranged at the bottom of the inner wall.
Preferably, the second bevel gear is of a hollow structure, the stirring shaft penetrates through the second bevel gear and extends towards the bottom of the inner tank, and the top of the stirring shaft is fixedly connected with the first bevel gear.
Preferably, heating mechanism includes the heating pipe, be provided with multiunit heating pipe between crystallizer and the centrifugal stirring mechanism, multiunit the heating pipe all is through connecting wire parallel connection, the week side of crystallizer inner wall is provided with the heat preservation inner membrance corresponding with multiunit heating pipe.
The working principle is as follows: when the novel crystallization kettle is used, stock solution to be subjected to evaporative crystallization can be injected into the inner tank 701 from the liquid injection port 4, after the liquid injection is finished, a plurality of groups of heating pipes 901 can be controlled by the control panel 13 to uniformly heat the inner tank 701 so as to promote the rapid evaporation of water in the stock solution, the heat preservation inner film 903 corresponding to the plurality of groups of heating pipes 901 is arranged on the peripheral side of the inner wall of the crystallization tank 2 so as to achieve a good heat preservation effect, thereby reducing the loss of heat and improving the heating and heat preservation efficiency, after the heating is carried out to a set temperature, the servo motor 601 can be started, the output shaft of the servo motor 601 drives the transmission bevel gear 602 to rotate, the first bevel gear 603 and the second bevel gear 604 are meshed with the transmission bevel gear 602, so that the transmission bevel gear 602 can drive the first bevel gear 603 and the second bevel gear 604 to synchronously rotate, after the servo motor 601 is started, the second bevel gear 604 will drive the inner tank 701 to rotate, so that the inner tank 701 can drive the stock solution in the tank to carry out centrifugal stirring, and at the same time, the stirring shaft 801 fixedly connected with the first bevel gear 603 can drive the stirring rods 803, the transverse scraping blades 804, the longitudinal scraping blades 805, the connecting rods 806 and the inclined scraping blades 807 to carry out rapid rotation, thereby realizing the rapid stirring of the stock solution at the center of the inner tank 701, accelerating the evaporation of the stock solution through the matching with the centrifugal stirring mechanism 7, thereby greatly improving the evaporation efficiency of the stock solution, discharging the evaporated water vapor in the stock solution through a plurality of through holes 703 arranged on the periphery of the top center of the inner tank 701, then the water is discharged out of the tank through a gas outlet 10, after the water is evaporated, the evaporated concentrated solution is discharged from a liquid outlet 11 at the bottom of the crystallizing tank 2, and then the concentrated solution enters the next procedure for processing.
(III) advantageous effects
The utility model provides a can improve evaporation crystallization efficiency's novel crystallization kettle. The method has the following beneficial effects:
1. this kind of can improve evaporation crystallization efficiency's novel crystallization kettle through the simple drive mechanism of design, can realize going on in step of two kinds of stirring modes, both can the energy saving, has also guaranteed stirring efficiency simultaneously, after using, can also utilize rabbling mechanism to realize the self-cleaning to the inner tank to practiced thrift a large amount of manpower and materials, also prolonged its life simultaneously.
2. This kind of can improve evaporation crystallization efficiency's novel crystallization kettle, through mutually supporting of drive mechanism, centrifugal rabbling mechanism, rotatory rabbling mechanism and self-heating mechanism, can improve the evaporation crystallization efficiency of stoste greatly, both practiced thrift a large amount of energy, also guaranteed machining efficiency simultaneously, be worth wideling popularize.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
fig. 3 is a schematic view of the mounting structure of the supporting mechanism of the present invention;
fig. 4 is a schematic structural view of the transmission mechanism of the present invention;
fig. 5 is a schematic structural view of the rotary stirring mechanism of the present invention;
fig. 6 is a partially enlarged view of a portion a in fig. 2.
Wherein, 1, a support frame; 2. a crystallization tank; 3. a can lid; 4. a liquid injection port; 5. a support mechanism; 501. a connecting pipe; 502. a flange plate; 503. a support frame; 504. a first bearing; 505. a top cover; 506. a second bearing; 507. a supporting seat; 6. a transmission mechanism; 601. a servo motor; 602. a drive bevel gear; 603. A first bevel gear; 604. a second bevel gear; 7. a centrifugal stirring mechanism; 701. an inner tank; 702. a guard ring; 703. a through hole; 704. a liquid outlet pipe; 705. a third bearing; 8. rotating the stirring mechanism; 801. a stirring shaft; 802. connecting blocks; 803. a stirring rod; 804. transverse scraping; 805. longitudinal scraping blade; 806. a connecting rod; 807. oblique scraping; 808. a fourth bearing; 9. a heating mechanism; 901. heating a tube; 902. connecting a lead; 903. insulating the inner film; 10. an air outlet; 11. a liquid outlet; 12. a thermometer; 13. a control panel.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Example (b):
as shown in fig. 1-6, the embodiment of the present invention provides a novel crystallization kettle capable of improving evaporation crystallization efficiency, including a support frame 1, a crystallization tank 2 is fixedly connected to the center of the support frame 1, a tank cover 3 is provided at the top of the crystallization tank 2, one side of the top of the tank cover 3 is provided with a liquid injection port 4, the top of the tank cover 3 is provided with a support mechanism 5, one side of the support mechanism 5 is provided with a transmission mechanism 6, the center of the crystallization tank 2 is provided with a centrifugal stirring mechanism 7, a rotary stirring mechanism 8 is installed at the center of the centrifugal stirring mechanism 7, a heating mechanism 9 is provided between the crystallization tank 2 and the centrifugal stirring mechanism 7, one side of the top outer surface of the tank cover 3 is provided with a gas outlet 10, the center of the bottom of the crystallization tank 2 is provided with a liquid outlet 11 corresponding to the centrifugal stirring mechanism 7, a thermometer 12 is installed at.
The support frame 1 is fixedly connected with the crystallizing tank 2 through welding, and the structure of the support frame is more firm through welding and fixed connection, so that the support frame cannot be easily damaged.
Supporting mechanism 5 includes connecting pipe 501, the top fixed block of connecting pipe 501 is connected with ring flange 502, the top fixedly connected with braced frame 503 of ring flange 502, first bearing 504 is installed at the center at braced frame 503 top, top cap 505 is installed at braced frame 503's top, the top fixedly connected with second bearing 506 of connecting pipe 501 inner wall, one side fixedly connected with supporting seat 507 of ring flange 502 outer wall, supporting mechanism 5 can play the supporting role to the top of centrifugal mixing mechanism 7 and rotatory rabbling mechanism 8.
The transmission mechanism 6 comprises a servo motor 601, the servo motor 601 is installed on the top of the supporting seat 507, one end of an output shaft of the servo motor 601 is fixedly connected with a transmission bevel gear 602, the top and the bottom of the transmission bevel gear 602 are respectively engaged with a first bevel gear 603 and a second bevel gear 604, when the crystallization kettle is used, the servo motor 601 can be started, so that the output shaft of the servo motor 601 drives the transmission bevel gear 602 to rotate, the first bevel gear 603 and the second bevel gear 604 are engaged with the transmission bevel gear 602, and the transmission bevel gear 602 drives the first bevel gear 603 and the second bevel gear 604 to synchronously rotate.
Centrifugal stirring mechanism 7 includes inner tank 701, the bottom fixedly connected with inner tank 701 of second bevel gear 604, the top fixedly connected with of inner tank 701 and annotate the corresponding protection ring 702 of liquid mouth 4, a plurality of through-holes 703 have been seted up to the week side at inner tank 701 top center, the bottom fixedly connected with drain pipe 704 of inner tank 701, third bearing 705 corresponding with drain pipe 704 is installed to the bottom of crystallizer 2 inner walls, after servo motor 601 starts, second bevel gear 604 can drive inner tank 701 and rotate, thereby make inner tank 701 can drive the interior stock solution of jar and carry out centrifugal stirring.
The rotary stirring mechanism 8 comprises a stirring shaft 801, a stirring shaft 801 is fixedly connected to the center of a first bevel gear 603, a plurality of connecting blocks 802 are fixedly connected to the center of the outer wall of the stirring shaft 801, stirring rods 803 are fixedly connected to both sides of the plurality of connecting blocks 802, a transverse scraping blade 804 and a longitudinal scraping blade 805 are respectively fixedly connected to one ends of the plurality of stirring rods 803, which are far away from the connecting blocks 802, connecting rods 806 are fixedly connected to both sides of the bottom of the outer wall of the stirring shaft 801, an inclined scraping blade 807 is mounted to one end of each connecting rod 806, which is far away from the stirring shaft 801, a fourth bearing 808 corresponding to the stirring shaft 801 is mounted to the bottom of the inner wall of the inner tank 701, after the servo motor 601 is started, the stirring shaft 801 fixedly connected to the first bevel gear 603 drives the plurality of stirring rods 803, the transverse scraping blade 804, the longitudinal scraping blade 805, through the cooperation with centrifugal stirring mechanism 7, can accelerate the evaporation of stoste to improve the evaporation efficiency of stoste greatly, after using, we can also carry out self-cleaning to the inner wall of inner tank 701 through water injection in to inner tank 701, then through a plurality of horizontal doctor-bars 804 and vertical doctor-bar 805.
The second bevel gear 604 is arranged in a hollow structure, the stirring shaft 801 penetrates through the second bevel gear 604 and extends towards the bottom of the inner tank 701, the top of the stirring shaft 801 is fixedly connected with the first bevel gear 603, and the second bevel gear 604 arranged in the hollow structure can drive the inner tank 701 to rotate and simultaneously does not influence the rotation of the stirring shaft 801.
Heating mechanism 9 includes heating pipe 901, be provided with multiunit heating pipe 901 between crystallizer 2 and the centrifugal stirring mechanism 7, multiunit heating pipe 901 all is through connecting wire 902 parallel connection, the week side of crystallizer 2 inner wall is provided with the heat preservation inner membrane 903 corresponding with multiunit heating pipe 901, after stock solution pours into inner tank 701 into, we can utilize multiunit heating pipe 901 to carry out even heating to inner tank 701 earlier, thereby realize promoting the rapid evaporation of moisture in the stock solution, the week side of crystallizer 2 inner wall is provided with the heat preservation inner membrane 903 corresponding with multiunit heating pipe 901 and can play fine heat preservation effect, thereby can reduce thermal scattering and disappearing, improve heating heat preservation efficiency.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
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| Application Number | Priority Date | Filing Date | Title |
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| CN201922475436.7U CN213100902U (en) | 2019-12-31 | 2019-12-31 | Novel crystallization kettle capable of improving evaporation crystallization efficiency |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201922475436.7U CN213100902U (en) | 2019-12-31 | 2019-12-31 | Novel crystallization kettle capable of improving evaporation crystallization efficiency |
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| CN213100902U true CN213100902U (en) | 2021-05-04 |
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| CN201922475436.7U Active CN213100902U (en) | 2019-12-31 | 2019-12-31 | Novel crystallization kettle capable of improving evaporation crystallization efficiency |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111097187A (en) * | 2019-12-31 | 2020-05-05 | 南京紫晶藤节能科技有限公司 | A new type of crystallization kettle that can improve the efficiency of evaporative crystallization |
| CN117326735A (en) * | 2023-10-11 | 2024-01-02 | 河北乐恒节能设备有限公司 | Sodium sulfate solution recovery device and process |
| CN118384518A (en) * | 2024-06-25 | 2024-07-26 | 福建光启化学有限公司 | Concentrated crystallization kettle is used in medicine preparation |
-
2019
- 2019-12-31 CN CN201922475436.7U patent/CN213100902U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111097187A (en) * | 2019-12-31 | 2020-05-05 | 南京紫晶藤节能科技有限公司 | A new type of crystallization kettle that can improve the efficiency of evaporative crystallization |
| CN117326735A (en) * | 2023-10-11 | 2024-01-02 | 河北乐恒节能设备有限公司 | Sodium sulfate solution recovery device and process |
| CN118384518A (en) * | 2024-06-25 | 2024-07-26 | 福建光启化学有限公司 | Concentrated crystallization kettle is used in medicine preparation |
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