CN212980831U - Dispersion storage device for electrochemical stripping preparation of double graphite electrodes - Google Patents
Dispersion storage device for electrochemical stripping preparation of double graphite electrodes Download PDFInfo
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- CN212980831U CN212980831U CN202021338561.XU CN202021338561U CN212980831U CN 212980831 U CN212980831 U CN 212980831U CN 202021338561 U CN202021338561 U CN 202021338561U CN 212980831 U CN212980831 U CN 212980831U
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- Prior art keywords
- bottle body
- bottle
- dispersion
- graphite electrodes
- storage device
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- 239000006185 dispersion Substances 0.000 title claims abstract description 51
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 229910002804 graphite Inorganic materials 0.000 title claims abstract description 35
- 239000010439 graphite Substances 0.000 title claims abstract description 35
- 238000003860 storage Methods 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 230000007246 mechanism Effects 0.000 claims abstract description 12
- 238000007789 sealing Methods 0.000 claims description 28
- 239000007788 liquid Substances 0.000 claims description 25
- 239000011229 interlayer Substances 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 19
- 238000002347 injection Methods 0.000 claims description 13
- 239000007924 injection Substances 0.000 claims description 13
- 238000003825 pressing Methods 0.000 claims description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 abstract description 14
- 229910052796 boron Inorganic materials 0.000 abstract description 14
- -1 graphite alkene Chemical class 0.000 abstract description 13
- 230000005518 electrochemistry Effects 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 7
- 229910021389 graphene Inorganic materials 0.000 description 15
- 238000000034 method Methods 0.000 description 4
- 239000003792 electrolyte Substances 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Abstract
The utility model belongs to the technical field of the dispersion storage, specifically be a two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device, including outer bottle, bottle lid, inner bottle body, intermediate layer, syringe and rabbling mechanism, the top of bottle lid screw assembly bottle outside, the inner bottle body is located the inside of outer bottle, and forms the intermediate layer between inner bottle body and the outer bottle, the syringe sets up the outside and the intercommunication intermediate layer of bottle outside, rabbling mechanism installs on the bottle lid, be equipped with the rubber circle on the outer wall of outer bottle, anti-skidding line has been seted up on the outer wall of rubber circle. This two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device stores boron doping graphite alkene dispersion through setting up the inner bottle body, utilizes the intermediate layer between outer bottle body and the inner bottle body, can improve boron doping graphite alkene dispersion's save time and effect to reducing the influence of external high temperature to the interior boron doping graphite alkene dispersion of inner bottle body.
Description
Technical Field
The utility model relates to a dispersion storage technology field especially relates to a two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device.
Background
Dissolving anion boron-containing soluble salt in deionized water to form electrolyte; putting double graphite electrodes into the electrolyte, connecting an alternating current power supply, and starting to react until the graphite electrodes are stripped; and cleaning the reacted electrolyte for multiple times to prepare the boron-doped graphene dispersion liquid, wherein the prepared boron-doped graphene dispersion liquid needs to be stored by means of a storage device.
Need relatively sealed and microthermal environment when boron doping graphite alkene dispersion is stored, however, do not have special storage device to store boron doping graphite alkene dispersion among the prior art, current boron doping graphite alkene dispersion storage device easily receives ambient temperature to influence, and the storage effect is relatively poor.
In order to solve the problems, the application provides a dispersion liquid storage device for electrochemical stripping preparation of a double-graphite electrode.
SUMMERY OF THE UTILITY MODEL
Objects of the invention
For solving the technical problem who exists among the background art, the utility model provides a two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device has the effectual characteristics of storage.
(II) technical scheme
In order to solve the technical problem, the utility model provides a dispersion storage device for preparing double graphite electrode by electrochemical stripping, which comprises an outer bottle body, a bottle cap, an inner bottle body, an interlayer, an injection tube and a stirring mechanism;
the injection bottle is characterized in that the bottle cap is assembled at the top of the outer bottle body in a threaded mode, the inner bottle body is located inside the outer bottle body, an interlayer is formed between the inner bottle body and the outer bottle body, the injection tube is arranged on the outer side of the outer bottle body and communicated with the interlayer, and the stirring mechanism is installed on the bottle cap.
Preferably, the outer wall of the outer bottle body is provided with a rubber ring, and the outer wall of the rubber ring is provided with anti-skid grains.
Preferably, a sealing head is arranged in the middle of the inner side of the bottle cap and is in extrusion contact with the inner wall of the inner bottle body.
Preferably, rabbling mechanism includes runner, pivot, connecting axle, fixing bolt, stirring leaf and sealing washer, pivot movable assembly is at the middle part of bottle lid, and the top fixedly connected with runner of pivot, be equipped with the suit in the bottle lid at the outlying sealing washer of pivot, the bottom of pivot is run through sealed head and is extended to interior bottle and through fixing bolt fixedly connected with connecting axle, the bottom of connecting axle is equipped with the stirring leaf.
Preferably, the bottom of one side of the outer bottle body is provided with a liquid discharge pipe communicated with the interlayer.
Preferably, the sealing head is of a circular truncated cone-shaped rubber structure, and a groove is formed in the middle of the bottom end of the sealing head.
Preferably, the annular array on the outer wall of the wheel has four handles.
The above technical scheme of the utility model has following profitable technological effect:
1. this two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device stores boron doping graphite alkene dispersion through setting up the inner bottle body, utilizes the intermediate layer between outer bottle body and the inner bottle body, can improve boron doping graphite alkene dispersion's save time and effect to reducing the influence of external high temperature to the interior boron doping graphite alkene dispersion of inner bottle body.
2. This two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device through set up the intermediate layer between outer bottle and inner bottle to set up the interbedded injection syringe of intercommunication, in the storage process, the accessible is to the intermediate layer injection low temperature gas or liquid, thereby improves the storage time and the effect of boron doping graphite alkene dispersion.
3. This two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device through setting up the sealed head at the bottle lid inboard, can seal bottle lid and outer bottle, and is sealed effectual, and boron doping graphite alkene dispersion is stored effectually, and this storage device can reach skid-proof purpose through setting up the rubber circle on outer bottle outer wall.
4. This two graphite electrode electrochemistry are peeled off preparation and are used dispersion storage device through setting up rabbling mechanism, after boron doping graphite alkene dispersion is long-time to be stored and is appeared gathering the sediment, and the person of facilitating the use stirs the dispersion to interior bottle internal boron doping graphite alkene dispersion before using.
Drawings
Fig. 1 is a front view of the overall structure of the present invention;
FIG. 2 is a cross-sectional view of the overall structure of the present invention;
FIG. 3 is a schematic view of the connecting shaft according to the present invention after rotating;
fig. 4 is an enlarged view of a portion a in fig. 3 according to the present invention.
Reference numerals:
1. an outer bottle body; 111. a rubber ring; 2. a bottle cap; 21. a sealing head; 3. an inner bottle body; 4. an interlayer; 5. an injection tube; 6. a rotating wheel; 7. a rotating shaft; 8. a connecting shaft; 9. fixing the bolt; 10. stirring blades; 11. and (5) sealing rings.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in detail with reference to the accompanying drawings. It should be understood that the description is intended to be illustrative only and is not intended to limit the scope of the present invention. Moreover, in the following description, descriptions of well-known structures and techniques are omitted so as to not unnecessarily obscure the concepts of the present invention.
Specific embodiments of the present invention will be described below with reference to the accompanying drawings.
Referring to fig. 2, the present invention provides a technical solution: a dispersion storage device for electrochemical stripping preparation of double graphite electrodes comprises an outer bottle body 1, a bottle cap 2, an inner bottle body 3, an interlayer 4, an injection tube 5 and a stirring mechanism.
As shown in FIG. 2, the inner body 3 is positioned inside the outer body 1, and an interlayer 4 is formed between the inner body 3 and the outer body 1.
Because boron-doped graphene dispersion needs to be stored at a low temperature, and a boron-doped graphene dispersion storage device in the prior art is generally of a single-layer structure, is easily influenced by external temperature, and is difficult to meet the storage requirement of the boron-doped graphene dispersion, in this embodiment, the interlayer 4 is arranged between the inner bottle body 3 and the outer bottle body 1, so that the purpose of heat insulation is achieved, and the storage time and the effect of the boron-doped graphene dispersion are improved.
The injection tube 5 is arranged at the outer side of the outer bottle body 1 and is communicated with the interlayer 4.
In this embodiment, by providing the injection pipe 5 communicating with the interlayer 4, in the storage process, a low-temperature gas or liquid can be injected into the interlayer 4 through the injection pipe 5, thereby further improving the storage effect and time of the boron-doped graphene dispersion liquid.
A liquid discharge pipe communicated with the interlayer 4 is arranged at the bottom of one side of the outer bottle body 1.
The liquid discharge pipe arranged at the bottom of one side of the outer bottle body 1 is convenient for discharging the gas or liquid filled in the interlayer 4.
It should be noted that the ends of the syringe 5 and the drain are provided with screw-mounted caps, and the caps are screwed into the syringe 5 and the drain to maintain a sealed state.
As shown in fig. 1, the outer wall of the outer bottle body 1 is provided with a rubber ring 111, and the outer wall of the rubber ring 111 is provided with anti-slip lines.
Because outer bottle 1 usually adopts the glass material, in the use, the phenomenon of skidding appears easily when especially taking out after the low temperature is preserved, for this reason, in this embodiment, through setting up the rubber circle 111 that has anti-skidding line, improves the frictional force between user's hand and the outer bottle 1 to avoid outer bottle landing breakage, and convenience of customers' use.
As shown in fig. 2, the bottle cap 2 is screw-assembled on the top of the outer body 1, and a sealing head 21 is provided at the middle of the inner side of the bottle cap 2, and the sealing head 21 is in pressing contact with the inner wall of the inner body 3.
In this embodiment, the sealing head 21 disposed inside the bottle cap 2 is used to seal the joint between the bottle cap 2 and the inner bottle body 3, so as to seal the inner bottle body 3, thereby facilitating storage of the boron-doped graphene dispersion.
It should be noted that, the sealing head 21 is arranged in an inverted circular truncated cone shape, which is more beneficial for the sealing connection between the bottle cap 2 and the inner bottle body 3.
Further, the sealing head 21 is of a circular truncated cone-shaped rubber structure, and a groove is formed in the middle of the bottom end of the sealing head 21.
The middle part of the sealing head 21 is provided with the groove, so that the material consumption of the sealing head 21 is reduced and the cost is saved under the condition that the use of the sealing head 21 is not influenced.
As shown in fig. 2-4, the stirring mechanism is mounted on the bottle cap 2. The stirring mechanism comprises a rotating wheel 6, a rotating shaft 7, a connecting shaft 8, a fixing bolt 9, a stirring blade 10 and a sealing ring 11.
The rotating shaft 7 is movably assembled in the middle of the bottle cap 2, the rotating wheel 6 is fixedly connected to the top of the rotating shaft 7, and four handles are arranged on the outer wall of the rotating wheel 6 in an annular array mode.
By utilizing the four handles arranged on the outer wall of the rotating wheel 6 in the annular array, a user can apply force to rotate the rotating wheel 6, so that the rotating shaft 7 is driven to rotate.
And a sealing ring 11 sleeved on the periphery of the rotating shaft 7 is arranged in the bottle cap 2.
The seal ring 11 seals between the cap 2 and the rotary shaft 7 while ensuring smooth rotation of the rotary shaft 7.
The bottom of the rotating shaft 7 penetrates through the sealing head 21, extends into the inner bottle body 3 and is fixedly connected with a connecting shaft 8 through a fixing bolt 9, and the bottom of the connecting shaft 8 is provided with a stirring blade 10.
In this embodiment, the rotating wheel 6 is rotated to drive the rotating shaft 7 to rotate, so as to drive the stirring blade 10 at the bottom of the connecting shaft 8 to rotate, and further, the boron-doped graphene dispersion liquid stored in the inner bottle body 3 can be stirred and dispersed.
It should be noted that, the fixing bolt 9 is used for mounting the rotating shaft 7 and the connecting shaft 8, so that the rotating shaft 7 and the connecting shaft 8 are convenient to detach, the use by a user is convenient, and the cleaning or the replacement of the stirring blade 10 is facilitated.
The utility model discloses a theory of operation and use flow: firstly, during storage, the bottle cap 2 is opened, the boron-doped graphene dispersion liquid is injected into the inner bottle body 3, and then the bottle cap 2 is screwed in, so that the outer wall of the sealing head 21 is tightly attached to the inner part of the inner bottle body 3, and the inner part of the inner bottle body 3 is sealed;
then, in the storage process, low-temperature gas or liquid can be injected into the interlayer 4 by opening the injection pipe 5, so that the boron-doped graphene dispersion liquid in the inner bottle body 3 is stored at low temperature, and after the boron-doped graphene dispersion liquid is used for a period of time, the used gas or liquid in the interlayer 4 can be discharged by opening the liquid discharge pipe at the bottom of the side surface of the outer bottle body 1;
finally, the boron-doped graphene dispersion liquid in the inner bottle body 3 is easy to generate coagulation after being stored for a long time, and before the user uses the boron-doped graphene dispersion liquid again, the rotating wheel 6 is rotated to drive the rotating shaft 7 to rotate, so that the stirring blade 10 at the bottom of the connecting shaft 8 is driven to rotate, and then the boron-doped graphene dispersion liquid in the inner bottle body 3 is stirred and dispersed.
It is to be understood that the above-described embodiments of the present invention are merely illustrative of or explaining the principles of the invention and are not to be construed as limiting the invention. Therefore, any modification, equivalent replacement, improvement and the like made without departing from the spirit and scope of the present invention should be included in the protection scope of the present invention. Further, it is intended that the appended claims cover all such variations and modifications as fall within the scope and boundaries of the appended claims or the equivalents of such scope and boundaries.
Claims (7)
1. A dispersion storage device for electrochemical stripping preparation of double graphite electrodes is characterized by comprising an outer bottle body (1), a bottle cap (2), an inner bottle body (3), an interlayer (4), an injection tube (5) and a stirring mechanism;
the bottle cap (2) is assembled at the top of the outer bottle body (1) in a threaded manner, the inner bottle body (3) is located inside the outer bottle body (1), an interlayer (4) is formed between the inner bottle body (3) and the outer bottle body (1), the injection tube (5) is arranged on the outer side of the outer bottle body (1) and communicated with the interlayer (4), and the stirring mechanism is installed on the bottle cap (2).
2. The device for storing the dispersion liquid for the electrochemical stripping preparation of the double graphite electrodes as claimed in claim 1, wherein the outer wall of the outer bottle body (1) is provided with a rubber ring (111), and the outer wall of the rubber ring (111) is provided with anti-skid lines.
3. The device for storing the dispersion liquid for the electrochemical stripping preparation of the double graphite electrodes as claimed in claim 1, wherein the bottle cap (2) is provided with a sealing head (21) at the middle of the inner side, and the sealing head (21) is in pressing contact with the inner wall of the inner bottle body (3).
4. The dispersion storage device for the electrochemical stripping preparation of the double graphite electrodes as claimed in claim 1, wherein the stirring mechanism comprises a rotating wheel (6), a rotating shaft (7), a connecting shaft (8), a fixing bolt (9), a stirring blade (10) and a sealing ring (11), the rotating shaft (7) is movably assembled in the middle of the bottle cap (2), the rotating wheel (6) is fixedly connected to the top of the rotating shaft (7), the sealing ring (11) sleeved on the periphery of the rotating shaft (7) is arranged in the bottle cap (2), the bottom of the rotating shaft (7) penetrates through the sealing head (21) and extends into the inner bottle body (3) and is fixedly connected with the connecting shaft (8) through the fixing bolt (9), and the stirring blade (10) is arranged at the bottom of the connecting shaft (8).
5. The device for storing the dispersion liquid for the electrochemical stripping preparation of the double graphite electrodes as claimed in claim 1, wherein a drain pipe communicated with the interlayer (4) is arranged at the bottom of one side of the outer bottle body (1).
6. The device for storing the dispersion liquid for the electrochemical stripping preparation of the double graphite electrodes as claimed in claim 3, wherein the sealing head (21) is of a truncated cone-shaped rubber structure, and a groove is formed in the middle of the bottom end of the sealing head (21).
7. The device for storing the dispersion liquid for the electrochemical stripping preparation of the double graphite electrodes as claimed in claim 4, wherein the rotating wheel (6) has four handles in an annular array on the outer wall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021338561.XU CN212980831U (en) | 2020-07-09 | 2020-07-09 | Dispersion storage device for electrochemical stripping preparation of double graphite electrodes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021338561.XU CN212980831U (en) | 2020-07-09 | 2020-07-09 | Dispersion storage device for electrochemical stripping preparation of double graphite electrodes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212980831U true CN212980831U (en) | 2021-04-16 |
Family
ID=75426905
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021338561.XU Active CN212980831U (en) | 2020-07-09 | 2020-07-09 | Dispersion storage device for electrochemical stripping preparation of double graphite electrodes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212980831U (en) |
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2020
- 2020-07-09 CN CN202021338561.XU patent/CN212980831U/en active Active
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20231007 Address after: 653100 Bailong Road Poultry and Egg Comprehensive Market, Liqi Street, Hongta District, Yuxi City, Yunnan Province Patentee after: Yuxi Cesium Rubidium Technology Co.,Ltd. Address before: 723000, Shaanxi City, Hanzhoung province Dongguan small son Patentee before: Shaanxi University of Technology |