CN212854739U - Continuous liquid separating device - Google Patents
Continuous liquid separating device Download PDFInfo
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- CN212854739U CN212854739U CN202021410652.XU CN202021410652U CN212854739U CN 212854739 U CN212854739 U CN 212854739U CN 202021410652 U CN202021410652 U CN 202021410652U CN 212854739 U CN212854739 U CN 212854739U
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- 239000007788 liquid Substances 0.000 title claims abstract description 113
- 238000000926 separation method Methods 0.000 claims description 72
- 239000000376 reactant Substances 0.000 claims description 15
- 239000003960 organic solvent Substances 0.000 claims description 13
- 238000011084 recovery Methods 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 230000002378 acidificating effect Effects 0.000 claims description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 24
- 239000012071 phase Substances 0.000 description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 238000010586 diagram Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000012074 organic phase Substances 0.000 description 4
- 238000005265 energy consumption Methods 0.000 description 3
- 238000005191 phase separation Methods 0.000 description 3
- 238000004064 recycling Methods 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000010815 organic waste Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000013076 target substance Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The application relates to a continuous liquid separating device, which is characterized by comprising at least one liquid separating tank, wherein a flow guide pipe extending into the middle lower part of the tank is arranged in the liquid separating tank, an overflow port and a vent port are arranged at the upper part of the tank, and a bottom valve is arranged at the bottom of the tank; the pipe diameter of the flow guide pipe is more than 1.2 times of the pipe diameter of the pipeline before entering the tank; the outlet of the draft tube is positioned in the light phase.
Description
Technical Field
The application relates to a continuous liquid distribution device.
Background
With the rapid development of the chemical industry, the national requirements on the environmental protection of the chemical industry are increasingly strict, the recycling treatment difficulty of chemical organic waste liquid is increasingly high, most of the organic solvent is recycled at present through alkali washing or acid washing, then neutral organic solvent is obtained through separation treatment, and then pure organic solvent is obtained through recycling of a rectifying tower. However, the recovery mode produces a large amount of wastewater containing organic impurities and salts, the environmental protection pressure is large, and the energy consumption is large, the time and the labor are wasted, and the production cost is increased due to the fact that rectification is needed.
Disclosure of Invention
The invention aims to provide a continuous liquid separating device, which can conveniently and efficiently recover an organic solvent or carry out phase separation on reactants, has low energy consumption, is energy-saving and environment-friendly, and can continuously operate, thereby improving the production efficiency.
Specifically, the present invention relates to:
(1) the continuous liquid separation device is characterized by comprising at least one liquid separation tank, wherein a guide pipe extending into the middle lower part of the tank is arranged in the liquid separation tank, an overflow port and a vent port are arranged at the upper part of the tank, and a bottom valve is arranged at the bottom of the tank; the pipe diameter of the draft tube is more than 1.2 times, preferably more than 1.5 times of the pipe diameter of the pipeline before entering the tank; the outlet of the draft tube is positioned in the light phase.
(2) The continuous liquid separation device in the above (1), wherein the number of the liquid separation tanks is 2-3, preferably 2.
(3) The continuous liquid separation device in the (2), wherein the liquid separation tanks are connected in series, and the height difference of overflow ports of adjacent liquid separation tanks is not less than 30 cm.
(4) The continuous liquid separation device according to any one of the above (1) to (3), which is used for recovering an organic solvent without containing an acidic or basic substance, wherein the target organic solvent to be obtained is a light phase, the first liquid separation tank is connected with the recovery kettle, and a condenser is arranged between the first liquid separation tank and the recovery kettle.
(5) The continuous liquid separation device according to any one of the above (1) to (3), which is used for separating the phases of reactants, wherein the target phase to be obtained is a light phase, wherein the first liquid separation tank is connected with a clarifying tank or a reaction tank.
(6) The continuous liquid separation device according to the above (5), wherein the height of the overflow port of the clarifying tank is at least 30cm greater than the height of the overflow port of the first liquid separation tank.
(7) The continuous liquid separation device according to any one of the above (1) to (6), wherein an interface meter is provided on the liquid separation tank.
Drawings
Fig. 1 is a schematic structural diagram of a preferred embodiment of the continuous liquid separation device of the present application.
Fig. 2 is a schematic structural diagram of a preferred embodiment of the continuous liquid separation device for recovering an organic solvent without containing an acidic or basic substance.
FIG. 3 is a schematic structural diagram of a preferred embodiment of the continuous liquid separation device for separating the phases of the reactants according to the present application.
FIG. 4 is a schematic structural diagram of another preferred embodiment of the continuous liquid separation device for separating the phases of the reactants according to the present application.
Description of reference numerals:
1: liquid separating tank;
2: a flow guide pipe;
3: an overflow port;
4: a vent port;
5: a bottom valve;
6: an interface meter;
7: a pipeline before tank entry;
8: a recovery kettle;
9: a condenser;
10: a clarifying tank;
11: and (4) a reaction tank.
Detailed Description
As shown in figure 1, the liquid separating device comprises at least one liquid separating tank 1, a guide pipe 2 extending into the middle lower part of the tank is arranged inside the liquid separating tank 1, an overflow port 3 and a vent port 4 are arranged on the upper part of the tank, and a bottom valve 5 is arranged on the bottom of the tank.
The liquid separating device can be used for different purposes, including but not limited to recovering organic solvents without acidic or basic substances, separating reactants and the like. When the organic solvent is recovered, as shown in fig. 2, the first liquid separation tank 1 is connected with a recovery kettle 8 through a condenser 9; for the separation of the reactants, as shown in FIG. 3, the first separation tank 1 is connected to a clarifying tank 10 or a reaction tank 11.
The liquid separating device is suitable for being used in liquid separation of a light phase serving as a target phase to be obtained.
The number of the liquid separation tanks 1 may be determined depending on the properties of the liquid to be separated, and is preferably 2 or more from the viewpoint of ensuring sufficient liquid separation, but is generally preferably not more than 3, and preferably 2 from the viewpoint of time.
When more than two liquid separation tanks 1 are arranged, the tanks are connected in series, and a certain height difference is arranged between the adjacent tanks, so that liquid can flow from the previous tank to the next tank by means of a potential difference without pumping. The height difference is determined according to factors influencing the pipe resistance, such as the viscosity of the liquid, the distance between the tanks, the size of the connecting pipeline and the like. The height difference is typically not less than 30cm, measured as the height difference between the overflow ports 3 on each tank.
When the liquid separating device is used for separating the reactants, the appropriate height difference is also preferably arranged between the clarifying tank 10 and the liquid separating tank 1, so that the liquid automatically overflows through the height difference without pumping.
The residence time of the liquid in the liquid separation tank 1 is determined according to the time required for the liquid to be fully layered, and the volume of the tank is reasonably determined according to the residence time and the feeding speed of the liquid.
The continuous liquid separation device is characterized in that a liquid separation tank 1 is internally provided with a guide pipe 2 extending into the middle lower part of the tank, and the distance between the outlet of the guide pipe 2 and the bottom of the tank is preferably 20-50 cm.
If the liquid to be separated continuously falls into the separating tank 1 from the upper part thereof, the upper layer light phase is always in a state of disturbance of the liquid level, and in this state, if the upper layer light phase is caused to flow out from the overflow port 3, a certain amount of moisture is still contained therein. Therefore, the feeding is stopped for a certain time after the liquid tank is fully stored, and the light phase can flow out from the overflow port 3 after the liquid tank is fully kept standing and layered, so that the continuous operation cannot be carried out.
This application is through the setting of honeycomb duct 2 as above, and the liquid of waiting to divide the liquid is by the well lower part of water conservancy diversion to divide liquid jar 1, has avoided liquid to fall into above the liquid level of jar upper portion and has caused the continuous disturbance of liquid level, consequently lies in the light phase layer near overflow mouth 3 on jar upper portion and keeps static always, can keep light phase constantly flowing out from overflow mouth 3 on one side of the feeding, can realize continuous operation from this.
Further, the flow velocity of the liquid can be reduced by increasing the pipe diameter of the draft tube 2, thereby reducing the impact force thereof. Therefore, the upper layer of the light phase near the overflow port 3 is kept static as much as possible, and the disturbance of the liquid outflow of the draft tube 2 to the heavy phase at the bottom of the tank can be reduced as much as possible. The pipe diameter of the draft tube 2 is preferably more than 1.2 times, preferably more than 1.5 times of the pipe diameter of the pipeline 7 (i.e. the transmission pipeline) before entering the tank.
The outlet of the draft tube 2 is in the light phase.
When the liquid separating device is used for separating the phases of the reactants, if the amounts of both phases of the reactants are large, the reactants are preferably introduced into the clarifying tank 10 for preliminary liquid separation and then introduced into the liquid separating device of the present invention for further liquid separation and purification. If the reactant is substantially a single phase and contains only a small amount of undesired impurities, the reactant can be directly fed from the reaction tank 11 to the liquid separation device of the present invention to be subjected to liquid separation purification.
The vent 4 is used to maintain pressure in the separation tank 1 and is preferably connected to a tail gas absorption unit to reduce inorganical emissions.
Preferably, the liquid separation tank 1 is further provided with an interface meter 6, and a bottom valve 5 at the bottom of the tank is opened according to the liquid level display of the interface meter 6 to discharge the heavy phase.
The continuous liquid separating device is preferably made of acid and alkali resistant materials, such as glass, enamel and lining plastic materials.
When the continuous liquid separating device is used for recovering the organic solvent, the continuous liquid separating device can replace a rectifying device, and is energy-saving and environment-friendly. Furthermore, the continuous liquid distribution device can continuously work, and the production efficiency is improved.
The continuous liquid separation device of the present application is described below by way of specific examples, but the present application is not limited to these examples, and any modification or change within the scope of the present application is within the scope of the present application.
Examples
EXAMPLE 1 recovery of toluene from aqueous waste toluene
The water-containing waste toluene is pumped into a recovery kettle 8, heated to boiling, toluene vapor is condensed into liquid through a condenser 9, the liquid enters a liquid separation tank 1 through a guide pipe 2, and after automatic layering, the upper-layer toluene enters a second liquid separation tank 1 through an overflow port 3. After the liquid separation treatment in the two liquid separation tanks 1 connected in series, the water content in the toluene is less than 0.03 percent and reaches the qualified standard by a Fischer-Tropsch type water content determination method. Qualified toluene enters the storage tank from an overflow port 3 of the second liquid separation tank 1, the layered water phase is deposited at the bottoms of the two liquid separation tanks 1, and the toluene is discharged into a sewage treatment system through a bottom valve 9 at the bottom when an interface meter 6 observes that the water layer reaches a specified height.
In the embodiment, the pipeline 7 before entering the tank adopts DN50 pipes, and the guide pipe 2 adopts DN80 pipes.
EXAMPLE 2 phase separation of reactants
The reaction mixture is introduced into a clarifying tank 10, after preliminary phase separation is carried out in the clarifying tank 10, the upper organic phase containing the target substance automatically overflows into a liquid separation tank 1 through a guide pipe 2 by the difference of the phases. After automatic layering, the upper organic phase enters the next liquid separation tank 1 through an overflow port 3, and two liquid separation tanks 1 connected in series are arranged. After the liquid separation treatment in the two liquid separation tanks 1, the upper organic phase is measured by a Fischer-Tropsch type moisture measurement method, after the process indexes are confirmed to be met, the qualified upper organic phase enters a storage tank or a reaction container in the next step from an overflow port 3 of the second liquid separation tank 1, the layered lower aqueous phase is deposited at the bottoms of the two liquid separation tanks 1, and is discharged through a bottom valve 9 at the bottom when the layered lower aqueous phase reaches the specified height through observation of an interface meter 6.
In the embodiment, the pipeline 7 before entering the tank adopts DN50 pipes, and the guide pipe 2 adopts DN80 pipes.
Industrial applicability
The continuous liquid separation device can be widely used for recycling organic solvents or separating reactants, can replace a rectification device with high energy consumption, and is energy-saving and environment-friendly. Further, can also carry out the separation of dividing continuously through the device that divides of this application, improve production efficiency.
Claims (9)
1. The continuous liquid separation device is characterized by comprising at least one liquid separation tank, wherein a guide pipe extending into the middle lower part of the tank is arranged in the liquid separation tank, an overflow port and a vent port are arranged at the upper part of the tank, and a bottom valve is arranged at the bottom of the tank;
the pipe diameter of the flow guide pipe is more than 1.2 times of the pipe diameter of the pipeline before entering the tank;
the outlet of the draft tube is positioned in the light phase.
2. The continuous liquid separation device according to claim 1, wherein the number of the liquid separation tanks is 2-3.
3. The continuous liquid separation device according to claim 1, wherein the number of the liquid separation tanks is 2.
4. The continuous liquid separation device according to claim 2 or 3, wherein the liquid separation tanks are connected in series, and the height difference of overflow ports of adjacent liquid separation tanks is not less than 30 cm.
5. The continuous liquid separation device according to claim 1 or 2, wherein the diameter of the flow guide pipe is more than 1.5 times of the diameter of the pipe before entering the tank.
6. The continuous liquid separation device according to claim 1 or 2, wherein the device is used for recovering an organic solvent without acidic or basic substances, the target organic solvent to be obtained is a light phase, the first liquid separation tank is connected with the recovery kettle, and a condenser is arranged between the first liquid separation tank and the recovery kettle.
7. A continuous liquid separating device according to claim 1 or 2, characterized in that it is used for separating the phases of the reactants, the target phase to be obtained being the light phase, the first liquid separating tank being connected to the clarifying tank or the reaction tank.
8. The continuous liquid separation device according to claim 7, wherein the height of the overflow port of the clarifying tank is at least 30cm greater than that of the overflow port of the first liquid separation tank.
9. The continuous liquid separation device according to claim 1 or 2, wherein an interface meter is arranged on the liquid separation tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021410652.XU CN212854739U (en) | 2020-07-17 | 2020-07-17 | Continuous liquid separating device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021410652.XU CN212854739U (en) | 2020-07-17 | 2020-07-17 | Continuous liquid separating device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212854739U true CN212854739U (en) | 2021-04-02 |
Family
ID=75216160
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021410652.XU Active CN212854739U (en) | 2020-07-17 | 2020-07-17 | Continuous liquid separating device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212854739U (en) |
-
2020
- 2020-07-17 CN CN202021410652.XU patent/CN212854739U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 052260 No.1, Hongsheng Road West, Mayu Village, Mayu Township, Jinzhou City, Shijiazhuang City, Hebei Province Patentee after: Lansheng Biotechnology Group Co.,Ltd. Patentee after: Hebei lanrun Plant Protection Technology Co.,Ltd. Address before: 052260 Mayu village, Jinzhou City, Shijiazhuang City, Hebei Province Patentee before: HEBEI LANSHENG BIOTECH Co.,Ltd. Patentee before: Hebei lanrun Plant Protection Technology Co.,Ltd. |
|
| CP03 | Change of name, title or address |