CN212807791U - Small-size device for collecting volatile components in enzymatic hydrolysate in real time - Google Patents
Small-size device for collecting volatile components in enzymatic hydrolysate in real time Download PDFInfo
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- CN212807791U CN212807791U CN202021560070.XU CN202021560070U CN212807791U CN 212807791 U CN212807791 U CN 212807791U CN 202021560070 U CN202021560070 U CN 202021560070U CN 212807791 U CN212807791 U CN 212807791U
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- Prior art keywords
- bottle
- conduit
- collecting
- collecting bottle
- collection
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- 230000002255 enzymatic effect Effects 0.000 title claims description 8
- 239000000413 hydrolysate Substances 0.000 title claims description 8
- 239000007788 liquid Substances 0.000 claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000010410 layer Substances 0.000 claims description 9
- 239000011229 interlayer Substances 0.000 claims description 6
- 239000004033 plastic Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 abstract description 4
- 238000001514 detection method Methods 0.000 abstract description 3
- 238000009835 boiling Methods 0.000 description 6
- 238000009833 condensation Methods 0.000 description 6
- 230000005494 condensation Effects 0.000 description 6
- 238000000605 extraction Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 2
- 238000001319 headspace solid-phase micro-extraction Methods 0.000 description 2
- DNHVXYDGZKWYNU-UHFFFAOYSA-N lead;hydrate Chemical compound O.[Pb] DNHVXYDGZKWYNU-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Apparatus Associated With Microorganisms And Enzymes (AREA)
Abstract
The utility model discloses a small-size device of collecting enzymolysis liquid volatile component in real time, include: a reaction bottle; the collecting device comprises a first collecting bottle, a second collecting bottle and a third collecting bottle, wherein the second collecting bottle and the third collecting bottle are of a double-layer structure; the communication device comprises a first conduit, a second conduit, a third conduit and a fourth conduit, wherein the first conduit is communicated with the reaction bottle and the first collecting bottle, the second conduit is communicated with the first collecting bottle and the second collecting bottle, the third conduit is communicated with the second collecting bottle and the third collecting bottle, and the fourth conduit is arranged in the third collecting bottle; and the valve bodies are respectively arranged on the first guide pipe and the fifth and fourth guide pipe, and the bottoms of the first collecting bottle, the second collecting bottle and the third collecting bottle. The utility model discloses can collect the volatile composition of enzymolysis liquid in real time to tentatively separate the composition, the liquid of collection can direct detection, and more convenient laborsaving.
Description
Technical Field
The utility model discloses volatile components collection device technical field especially relates to a device of small-size real-time collection enzymolysis liquid volatile components.
Background
The collection of current enzymolysis liquid volatile component is mainly through headspace solid phase microextraction, and headspace solid phase microextraction collects the adsorption and sampling, the extraction, it is concentrated, advance a kind in an organic whole, but the volatile substance in the high efficiency extraction sample, this processing mode has the operation swiftly, the extraction is complete, advantages such as with low costs, the volatile component enrichment in the enzymolysis liquid, but the liquid of collection is preliminary and not separated, can't directly detect, a device is provided, can collect the volatile component of enzymolysis liquid in real time, and tentatively separate the composition, the liquid of collection can direct detection be very necessary.
SUMMERY OF THE UTILITY MODEL
It is an object of the present invention to solve at least the above problems and to provide at least the advantages which will be described later.
The utility model discloses it is still another purpose to provide a small-size device of collecting enzymolysis liquid volatile component in real time, but its volatile component of real-time collection enzymolysis liquid to tentatively separate the composition, the liquid of collection can direct detection, more convenient laborsaving.
To achieve these objects and other advantages in accordance with the purpose of the invention, there is provided a small apparatus for collecting volatile components of an enzymatic hydrolysate in real time, comprising:
a reaction bottle; the collecting device comprises a first collecting bottle, a second collecting bottle and a third collecting bottle, wherein the second collecting bottle and the third collecting bottle are of a double-layer structure, and condensed water is arranged in a structural interlayer.
And the communication device comprises a first conduit, a second conduit, a third conduit and a fourth conduit, wherein the first conduit is communicated with the reaction bottle and the first collecting bottle, the second conduit is communicated with the first collecting bottle and the second collecting bottle, the third conduit is communicated with the second collecting bottle and the third collecting bottle, and the fourth conduit is arranged in the third collecting bottle.
The valve body comprises a first valve arranged on the first guide pipe, a second valve arranged at the bottom of the first collecting bottle, a third valve arranged at the bottom of the second collecting bottle, a fourth valve arranged at the bottom of the third collecting bottle and a fifth valve arranged on the fourth guide pipe.
Preferably, two ends of the first conduit are respectively arranged at the opening of the reaction bottle and the opening of the first collection bottle; the first end of the second conduit is arranged at the opening of the first collecting bottle, and the second end of the second conduit extends into the bottom of the second collecting bottle; the first end of the third conduit is arranged at the opening of the second collecting bottle, and the second end of the third conduit extends into the bottom of the third collecting bottle; one end of the fourth conduit is disposed at the opening of the third collection port.
Preferably, the reaction bottle, the first collecting bottle, the second collecting bottle and the third collecting bottle are provided with detachable covers at the openings
Preferably, the second collecting bottle and the third collecting bottle have the same structure, condensed water is filled in an interlayer between the double-layer structures of the second collecting bottle, and a condensed water outlet and a condensed water inlet are formed in the right side of the second collecting bottle from top to bottom.
Preferably, the first conduit and the second conduit are both rubber hoses, and the third conduit is a plastic hose.
The utility model discloses at least, include following beneficial effect:
the utility model discloses first receiving flask is connected with the reaction flask through first pipe, collects enzymolysis liquid volatile component in the reaction flask in first receiving flask, and the effect of first receiving flask, second receiving flask and third receiving flask all is with the gaseous condensation liquid of enzymolysis liquid volatility, and wherein the volatile component of low boiling point of first receiving flask condensation, the volatile component of boiling point in the second receiving flask condensation and the volatile component of high boiling point of third receiving flask condensation; the communication between the reaction bottle and the first collecting bottle is controlled by screwing or loosening the first valve; the liquid in the first collecting bottle, the second collecting bottle and the third collecting bottle can be controlled to flow out through the opening and closing of a second valve, a third valve and a fourth valve which are respectively arranged at the bottom, so that the convenience and labor saving are realized; through setting up second receiving flask and third receiving flask into bilayer structure, be convenient for fill into the comdenstion water in the structure intermediate layer, make the comdenstion water lead to the top export from the below entry, cool off volatile component, be convenient for make the gas that produces and comdenstion water contact fully the condensation to become liquid against the current. Therefore, the volatile components of the enzymolysis liquid can be collected in real time, the components are preliminarily separated, the collected liquid can be directly detected, and the convenience and labor saving are realized.
Additional advantages, objects, and features of the invention will be set forth in part in the description which follows and in part will become apparent to those having ordinary skill in the art upon examination of the following or may be learned from practice of the invention.
Drawings
Fig. 1 is a schematic structural diagram of a small-sized device for collecting volatile components of an enzymatic hydrolysate in real time.
Detailed Description
The present invention is further described in detail below with reference to the drawings so that those skilled in the art can implement the invention with reference to the description.
It will be understood that terms such as "having," "including," and "comprising," as used herein, do not preclude the presence or addition of one or more other elements or groups thereof.
As shown in fig. 1, the utility model provides a small-size device of collecting enzymolysis liquid volatile component in real time, include:
a reaction bottle 1; the collecting device comprises a first collecting bottle 2, a second collecting bottle 3 and a third collecting bottle 4, wherein the second collecting bottle 3 and the third collecting bottle 4 are both of a double-layer structure, and condensed water is arranged in a structural interlayer 31.
A communication device which comprises a first conduit 10, a second conduit 20, a third conduit 30 and a fourth conduit 40, wherein the first conduit 10 is communicated with the reaction bottle 1 and the first collection bottle 2, the second conduit 20 is communicated with the first collection bottle 2 and the second collection bottle 3, the third conduit 30 is communicated with the second collection bottle 3 and the third collection bottle 4, and the fourth conduit 40 is arranged in the third collection bottle 4.
A valve body including a first valve 11 disposed on the first conduit 10, a second valve 12 disposed at the bottom of the first receiving flask 2, a third valve 13 disposed at the bottom of the second receiving flask 3, a fourth valve 14 disposed at the bottom of the third receiving flask 4, and a fifth valve 15 disposed on the fourth conduit 40.
In a preferred scheme, two ends of the first conduit 10 are respectively arranged at the opening of the reaction bottle 1 and the opening of the first collection bottle 2; the first end of the second conduit 20 is arranged at the opening of the first collecting bottle 2, and the second end of the second conduit 20 is inserted into the bottom of the second collecting bottle 3; the first end of the third conduit 30 is arranged at the opening of the second collecting bottle 3, and the second end of the third conduit 30 extends into the bottom of the third collecting bottle 4; one end of the fourth guide duct 40 is disposed at the third collecting opening.
In a preferred embodiment, the openings of the reaction flask 1, the first collection flask 2, the second collection flask 3 and the third collection flask 4 are all provided with a detachable cover 5.
In a preferred embodiment, the second collection bottle 3 and the third collection bottle 4 have the same structure, the interlayer 31 between the two layers of the second collection bottle 3 is filled with condensed water, and the right side of the second collection bottle 3 is provided with a condensed water outlet 32 and a condensed water inlet 33 from top to bottom.
In a preferred embodiment, the first conduit 10 and the second conduit 20 are both rubber hoses, and the third conduit 30 is a plastic hose.
In the scheme, the first collecting bottle 2 is connected with the reaction bottle 1 through the first conduit 10, the volatile components of the enzymatic hydrolysate in the reaction bottle 1 are collected in the first collecting bottle 2, and the first collecting bottle 2, the second collecting bottle 3 and the third collecting bottle 4 are all used for condensing the volatile gas of the enzymatic hydrolysate into liquid, wherein the first collecting bottle 2 condenses the volatile components with low boiling point, the volatile components with medium boiling point condensed by the second collecting bottle 3 and the volatile components with high boiling point condensed by the third collecting bottle 4; the communication between the reaction bottle 1 and the first collection bottle 2 is controlled by screwing or unscrewing the first valve 11; the liquid in the first collecting bottle 2, the second collecting bottle 3 and the third collecting bottle 4 can be controlled to flow out through the opening and closing of a second valve 12, a third valve 13 and a fourth valve 14 which are respectively arranged at the bottom, so that the convenience and labor saving are realized; through setting up second receiving flask 3 and third receiving flask 4 to bilayer structure, be convenient for fill into the comdenstion water in structure intermediate layer 31, make the comdenstion water lead to the top export from the below entry, cool off volatile component, be convenient for make the gas that produces and comdenstion water contact the abundant condensation of flowing backwards into liquid. Therefore, the volatile components of the enzymolysis liquid can be collected in real time, the components are preliminarily separated, the collected liquid can be directly detected, and the convenience and labor saving are realized.
Wherein, the first collecting bottle 2 adopts plastic or glass bottle, and the second collecting bottle 3 and the third collecting bottle 4 adopt double-layer plastic or glass bottle.
While the embodiments of the invention have been described above, it is not intended to be limited to the details shown, or described, but rather to cover all modifications, which would come within the scope of the appended claims, and all changes which come within the meaning and range of equivalency of the art are therefore intended to be embraced therein.
Claims (5)
1. A small-size device for collecting volatile components in enzymolysis liquid in real time is characterized by comprising:
a reaction bottle;
the collecting device comprises a first collecting bottle, a second collecting bottle and a third collecting bottle, wherein the second collecting bottle and the third collecting bottle are of a double-layer structure, and condensed water is arranged in an interlayer of the structure;
a communication device comprising a first conduit, a second conduit, a third conduit and a fourth conduit, wherein the first conduit is communicated with the reaction bottle and the first collection bottle, the second conduit is communicated with the first collection bottle and the second collection bottle, the third conduit is communicated with the second collection bottle and the third collection bottle, and the fourth conduit is arranged in the third collection bottle;
the valve body comprises a first valve arranged on the first guide pipe, a second valve arranged at the bottom of the first collecting bottle, a third valve arranged at the bottom of the second collecting bottle, a fourth valve arranged at the bottom of the third collecting bottle and a fifth valve arranged on the fourth guide pipe.
2. The miniature apparatus for collecting volatile components in real time of enzymolysis liquid as claimed in claim 1, wherein two ends of said first conduit are respectively disposed at the opening of said reaction bottle and the opening of said first collection bottle; the first end of the second conduit is arranged at the opening of the first collecting bottle, and the second end of the second conduit extends into the bottom of the second collecting bottle; the first end of the third conduit is arranged at the opening of the second collecting bottle, and the second end of the third conduit extends into the bottom of the third collecting bottle; one end of the fourth conduit is disposed at the opening of the third collection port.
3. The device for collecting the volatile components of the enzymatic hydrolysate in real time in small size as claimed in claim 1, wherein the openings of the reaction bottle, the first collection bottle, the second collection bottle and the third collection bottle are all provided with detachable covers.
4. The device for collecting the volatile components of the enzymatic hydrolysate in real time in a small scale as claimed in claim 1, wherein the second collection bottle has the same structure as the third collection bottle, condensed water is filled in the interlayer between the double-layer structure of the second collection bottle, and a condensed water outlet and a condensed water inlet are arranged from top to bottom on the right side of the second collection bottle.
5. The device for collecting volatile components in enzymolysis liquid in real time as claimed in claim 1, wherein the first conduit and the second conduit are both rubber hoses, and the third conduit is a plastic hose.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021560070.XU CN212807791U (en) | 2020-07-31 | 2020-07-31 | Small-size device for collecting volatile components in enzymatic hydrolysate in real time |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021560070.XU CN212807791U (en) | 2020-07-31 | 2020-07-31 | Small-size device for collecting volatile components in enzymatic hydrolysate in real time |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212807791U true CN212807791U (en) | 2021-03-26 |
Family
ID=75106775
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021560070.XU Expired - Fee Related CN212807791U (en) | 2020-07-31 | 2020-07-31 | Small-size device for collecting volatile components in enzymatic hydrolysate in real time |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212807791U (en) |
-
2020
- 2020-07-31 CN CN202021560070.XU patent/CN212807791U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210326 |