CN212790957U - Laboratory emulsification reaction kettle - Google Patents
Laboratory emulsification reaction kettle Download PDFInfo
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- CN212790957U CN212790957U CN202021187082.2U CN202021187082U CN212790957U CN 212790957 U CN212790957 U CN 212790957U CN 202021187082 U CN202021187082 U CN 202021187082U CN 212790957 U CN212790957 U CN 212790957U
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Abstract
The utility model relates to a laboratory emulsion reaction cauldron relates to emulsion reaction equipment's technical field, and it includes the reation kettle body, and sealing connection can be dismantled to the open end of reation kettle body has the lid, and the lid runs through and is provided with agitator motor and digital display stepless speed regulation agitator, still sets up feed inlet, temperature control table and manometer on the lid, and the feed inlet is provided with the feed valve. The utility model discloses a sealing connection's lid, the stepless speed regulation agitator of digital display, the setting such as temperature control table and manometer, guarantee the leakproofness of stirring environment, the stepless speed regulation agitator of digital display is convenient for the staff and is controlled the stirring speed, different stirring speed is used according to the stirring demand of difference, this internal pressure of temperature control table and manometer real-time supervision reation kettle, the temperature, ensure experimental normal clear, make reation kettle have high rotational speed, easy operation, the wide range, strong adaptability's characteristics, the effect that the laboratory that is fit for small batch chooseed for use.
Description
Technical Field
The utility model belongs to the technical field of emulsion reaction equipment's technique and specifically relates to a laboratory emulsion reation kettle is related to.
Background
At present, various types of homogeneous mixing varieties are wide at home and abroad, and for a homogeneous stirring device for a small laboratory, a barrel body is usually open, and a homogenizing head consists of a conical stator and a conical rotor.
When the device is used for manufacturing emulsified liquid, bubbles are easily generated and are not easy to disappear, the emulsifying effect is influenced, the product is easy to be polluted and mixed, the dissolving speed of the product is low, the emulsifying quality is poor, and the experimental efficiency is low; meanwhile, if the method is used for reaction, the method is only suitable for normal-pressure open reaction and has a narrow application range.
Because the external stirring device is not matched with the fixed container, the materials on the peripheral wall of the reaction container can be emulsified only by manual rotation stirring only by a high-speed emulsification mode provided with an outer cover, the labor intensity is high, the automation degree is low, the quality of product emulsification is poor, and the product emulsification is easy to deteriorate.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a laboratory emulsification reaction kettle with higher automation degree and better product emulsification quality.
The above utility model discloses an above-mentioned utility model purpose can realize through following technical scheme:
the utility model provides a laboratory emulsification reation kettle, includes the reation kettle body, sealing connection can be dismantled to the open end of reation kettle body has the lid, the lid runs through and is provided with agitator motor and the electrodeless speed governing agitator of digital display, still set up feed inlet, temperature control table and manometer on the lid, the feed inlet is provided with the feed valve.
By adopting the technical scheme, a worker firstly opens the cover, adds materials into the reaction kettle, then rotates the cover, starts stirring, sets the rotating speed of the digital display stepless speed regulation stirrer and the stirring motor, adds small materials from the feed inlet, and stops the stirring motor or the digital display stepless speed regulation stirrer to discharge materials when the stirring time is up, wherein the digital display stepless speed regulation stirrer is used for homogenizing and emulsifying, and the stirring motor is used for stirring; in this in-process, this internal pressure of reation kettle, temperature are monitored through temperature control table and manometer real-time supervision reation kettle, ensure experimental normal clear for reation kettle has high rotational speed, easy operation, and the wide range, strong adaptability's characteristics are fit for the laboratory of small batch to choose for use.
The present invention may be further configured in a preferred embodiment as: the reaction kettle body is provided with a jacket, and one end of the jacket, which is close to the cover, is provided with a feeding port.
By adopting the technical scheme, after materials are added, a heating medium is introduced into the jacket, the heating medium is steam or hot oil, the heat transfer efficiency is high, and stirring is started after the temperature is stable; and turning off the heating medium while turning off the digital display stepless speed regulation stirrer.
The present invention may be further configured in a preferred embodiment as: the bottom of reation kettle body is provided with the bin outlet, the bin outlet can be dismantled to seal and be provided with the relief valve.
Through adopting above-mentioned technical scheme, the staff can be through the bin outlet blowing, perhaps directly overturn the blowing.
The present invention may be further configured in a preferred embodiment as: the stirring motor is electrically connected with a rotating speed display, and the digital display stepless speed regulation stirrer is electrically connected with an electronic display.
By adopting the technical scheme, the rotating speed display is used for displaying the rotating speed of the stirring motor, so that a worker can adjust the rotating speed of the stirring motor in time according to the stirring requirement; the electronic display is used for displaying the rotating speed of the digital display stepless speed regulation stirrer.
The present invention may be further configured in a preferred embodiment as: the output end of the stirring motor is provided with stirring blades, and the stirring blades are anchor type wall scraping stirring paddles.
Through adopting above-mentioned technical scheme, the anchor type is scraped the wall stirring rake and is convenient for handle high viscosity material when the low speed, and application range is wide, and handles the material of reation kettle body inside wall easily.
The present invention may be further configured in a preferred embodiment as: the digital display stepless speed regulation stirrer is detachably connected with the working head thereof.
By adopting the technical scheme, when workers need to select different working heads according to homogenized and emulsified materials and requirements, the workers only need to disassemble the working heads.
The present invention may be further configured in a preferred embodiment as: the reaction kettle body is detachably connected with a support frame, and the rotating speed displayer is connected with the support frame in a sliding mode.
Through adopting above-mentioned technical scheme, the support frame is convenient for support the reation kettle body for the arrangement that the reation kettle body can be stable in the experimentation is on the laboratory bench.
The present invention may be further configured in a preferred embodiment as: a vacuum interface and a standby buckle are reserved on the cover.
By adopting the technical scheme, the requirement of subsequent treatment process increasing is conveniently met.
To sum up, the utility model discloses a following at least one useful technological effect:
1. the sealing performance of a stirring environment is ensured through the arrangement of a cover, a digital display stepless speed regulation stirrer, a temperature control meter, a pressure gauge and the like which are in sealing connection, the digital display stepless speed regulation stirrer is convenient for workers to control the stirring speed, different stirring speeds are used according to different stirring requirements, the temperature control meter and the pressure gauge monitor the pressure and the temperature in the reaction kettle body in real time, the normal running of a test is ensured, and the reaction kettle has the characteristics of high rotating speed, easiness in operation, wide range and strong adaptability, and is suitable for being selected in a small-batch laboratory;
2. furthermore, the vacuum interface and the standby buckle are arranged, so that the requirement of a subsequent additional treatment process is met conveniently.
Drawings
Fig. 1 is a schematic view of the overall structure of the first embodiment.
Fig. 2 is a schematic view of the overall structure of the present embodiment.
FIG. 3 is a sectional view showing the jacket of the present embodiment (shown when the stirring blade is attached).
In the figure, 1, a reaction kettle body; 11. a jacket; 12. a discharge outlet; 121. a discharge valve; 2. a cover; 21. a vacuum interface; 22. a standby buckle; 3. a stirring motor; 31. a rotational speed display; 32. a stirring blade; 4. a digital display stepless speed regulation stirrer; 41. an electronic display; 5. a feed inlet; 51. a feed valve; 6. a temperature control meter; 7. a pressure gauge; 8. a feeding port; 9. a support frame.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings.
Referring to fig. 1 and 2, the laboratory emulsification reaction kettle disclosed by the utility model comprises a reaction kettle body 1, wherein the open end of the reaction kettle body 1 is detachably and hermetically connected with a cover 2, the sealing connection can adopt an inlet silicon rubber ring, the cover 2 is provided with a stirring motor 3 and a digital display stepless speed regulation stirrer 4 in a penetrating way, and the working head of the digital display stepless speed regulation stirrer 4 and the output shaft of the stirring motor 3 both extend into the reaction kettle body 1; the cover 2 is also provided with a feed port 5, a temperature control meter 6 and a pressure gauge 7, the feed port 5 is provided with a feed valve 51, and the cover 2 is reserved with a vacuum interface 21 and a spare buckle 22.
Referring to fig. 1 and 3, the reactor body 1 is provided with a jacket 11, the jacket 11 is made of stainless steel material, and the inner volume: 12000ml, working volume: 10000ml, material thickness: 7mm, minimum allowed stirring: 1L, minimum allowed emulsification amount: 4L maximum allowable stirring amount: 10L; one end of the jacket 11 close to the cover 2 is provided with a feeding port 8, and a worker introduces a heating medium into the jacket 11, wherein the heating medium is steam or hot oil, preferably steam is introduced in the embodiment, and the heat transfer efficiency is high.
The bottom of reation kettle body 1 is provided with bin outlet 12, and bin outlet 12 can be dismantled and sealed and be provided with relief valve 121, and the staff selects the mode of falling the material of blowing or upset pouring down according to actual demand.
The stirring motor 3 is electrically connected with a rotating speed display 31, a power supply: 220V/50Hz, power: 700W, rotating speed range: 0-200 revolutions and a torque enhancement module; the output end of the stirring motor 3 is provided with a stirring blade 32, the stirring blade 32 is made of 316L stainless steel, the stirring blade 32 is provided with an anchor type wall scraping stirring paddle, a helical ribbon is attached, and the viscosity of 100 ten thousand CP can be realized at low speed.
The digital display stepless speed regulation stirrer 4 and the working head thereof adopt a detachable connection mode, and the power supply comprises: 220V/50Hz, power: 1.5KKw, no load speed range: 00-6000 rpm; the digital display stepless speed regulation stirrer 4 is electrically connected with an electronic display 41, and the electronic display 41 is positioned on the cover 2.
When the staff need disperse emulsification, can replace digital display electrodeless speed governing agitator 4 with fly knife formula high viscosity disperse emulsification system, the power: 220V/50Hz, power: 370w, no load speed range: 30 to 2000 rpm.
The support frame 9 can be dismantled to reation kettle body 1 and be connected with, and support frame 9 can set up to electric crane, and the staff of being convenient for adjusts reation kettle body 1's height, and the joint support frame 9 that slides of rotational speed display 31.
The implementation principle of the embodiment is as follows: firstly, a worker opens a cover 2, materials are added into a reaction kettle, then the cover 2 rotates, stirring is started, the rotating speeds of a digital display stepless speed regulation stirrer 4 and a stirring motor 3 are set, whether the digital display stepless speed regulation stirrer 4 or the stirring motor 3 is started is determined according to experimental requirements, small materials are added from a feeding hole 5, the stirring time is up, the stirring motor 3 or the digital display stepless speed regulation stirrer 4 is closed to discharge materials, the digital display stepless speed regulation stirrer 4 is used for homogenizing and emulsifying, and the stirring motor 3 is used for stirring; in the process, the pressure and the temperature in the reaction kettle body 1 are monitored in real time through the temperature control meter 6 and the pressure gauge 7, so that the normal operation of the test is ensured.
The embodiment of this specific implementation mode is the preferred embodiment of the present invention, not limit according to this the utility model discloses a protection scope, so: all equivalent changes made according to the structure, shape and principle of the utility model are covered within the protection scope of the utility model.
Claims (8)
1. The utility model provides a laboratory emulsification reation kettle, includes reation kettle body (1), its characterized in that: the open end of reation kettle body (1) can be dismantled sealing connection and have lid (2), lid (2) run through and are provided with agitator motor (3) and digital display electrodeless speed governing agitator (4), still set up feed inlet (5), control by temperature change table (6) and manometer (7) on lid (2), feed inlet (5) are provided with feed valve (51).
2. The laboratory emulsification reaction vessel of claim 1, wherein: the reaction kettle body (1) is provided with a jacket (11), and one end, close to the cover (2), of the jacket (11) is provided with a feeding port (8).
3. The laboratory emulsification reaction vessel of claim 2, wherein: the bottom of reation kettle body (1) is provided with bin outlet (12), bin outlet (12) can be dismantled the sealed relief valve (121) that is provided with.
4. The laboratory emulsification reaction kettle of claim 3, wherein: the stirring motor (3) is electrically connected with a rotating speed display (31), and the digital display stepless speed regulation stirrer (4) is electrically connected with an electronic display (41).
5. The laboratory emulsification reaction kettle of claim 4, wherein: the output of agitator motor (3) is provided with stirring vane (32), stirring vane (32) set up to the anchor wall stirring rake of scraping.
6. The laboratory emulsification reaction vessel of claim 1, wherein: the digital display stepless speed regulation stirrer (4) is detachably connected with the working head thereof.
7. The laboratory emulsification reaction kettle of claim 4, wherein: the reaction kettle body (1) is detachably connected with a support frame (9), and the rotating speed displayer (31) is connected with the support frame (9) in a sliding mode.
8. The laboratory emulsification reaction vessel of claim 1, wherein: a vacuum interface (21) and a standby buckle (22) are reserved on the cover (2).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202021187082.2U CN212790957U (en) | 2020-06-23 | 2020-06-23 | Laboratory emulsification reaction kettle |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN202021187082.2U CN212790957U (en) | 2020-06-23 | 2020-06-23 | Laboratory emulsification reaction kettle |
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CN212790957U true CN212790957U (en) | 2021-03-26 |
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CN202021187082.2U Active CN212790957U (en) | 2020-06-23 | 2020-06-23 | Laboratory emulsification reaction kettle |
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CN (1) | CN212790957U (en) |
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2020
- 2020-06-23 CN CN202021187082.2U patent/CN212790957U/en active Active
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