CN212491609U - Rectifying still and rectifying tower combined device - Google Patents

Rectifying still and rectifying tower combined device Download PDF

Info

Publication number
CN212491609U
CN212491609U CN202020574957.8U CN202020574957U CN212491609U CN 212491609 U CN212491609 U CN 212491609U CN 202020574957 U CN202020574957 U CN 202020574957U CN 212491609 U CN212491609 U CN 212491609U
Authority
CN
China
Prior art keywords
rectifying
support column
pipe
rectifying still
still
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN202020574957.8U
Other languages
Chinese (zh)
Inventor
夏卫平
陈政权
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HUBEI TEYER PHARMACEUTICAL CO Ltd
Original Assignee
HUBEI TEYER PHARMACEUTICAL CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HUBEI TEYER PHARMACEUTICAL CO Ltd filed Critical HUBEI TEYER PHARMACEUTICAL CO Ltd
Priority to CN202020574957.8U priority Critical patent/CN212491609U/en
Application granted granted Critical
Publication of CN212491609U publication Critical patent/CN212491609U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model discloses a rectifying still and rectifying tower combined device, which relates to the technical field of rectification, and comprises a liquid storage tank, a support column, a rectifying still, a rectifying tower and a connecting pipe, wherein the support column is fixedly arranged on the working ground through a balancing weight arranged at the bottom of the support column, the rectifying still and the rectifying tower are fixedly arranged on the side wall of the support column, and a discharge pipe of the rectifying still is connected with an inlet pipe of the rectifying tower through the connecting pipe, so that the rectifying still and the rectifying tower are two independent working devices, thereby facilitating the replacement and the maintenance, and simultaneously being replaced by rectifying towers with different models, and the added device has practicability; simultaneously rectifying still's inside is provided with the bull stick, drives the bull stick through the motor and rotates to the stirring leaf and the three puddler of installation on the drive bull stick rotate, stir mixed liquid, guarantee to mix and can fully contact between the liquid, improve reaction rate.

Description

Rectifying still and rectifying tower combined device
Technical Field
The utility model relates to a rectification technical field specifically is a rectifying still and rectifying column allies oneself with and uses device.
Background
Rectification is a distillation method for separating a liquid mixture with high purity by utilizing reflux, is the separation operation of the liquid mixture with the widest industrial application, and is widely applied to the departments of petroleum, chemical industry, light industry, food, metallurgy and the like. The existing rectifying still refers to a device for liquid reaction vaporization in the rectifying process, the rectifying tower refers to a device for liquefying gas after reaction, and the rectifying still and the rectifying tower are main devices in the distilling process.
However, the rectifying still and the rectifying tower are generally used together, and the cavity formed by the rectifying still and the rectifying tower is used as a reaction distillation cavity of reactants to form gas outflow, so that the sizes of the rectifying still and the rectifying tower need to be matched with each other, the practicability of the device is low, the replacement is inconvenient, and meanwhile, the joint mode causes the problems of low reaction speed, low distillation efficiency and the like, the production cost of enterprises is increased, and the production efficiency of equipment is reduced.
SUMMERY OF THE UTILITY MODEL
To the problem that exists among the prior art, the utility model aims to provide a rectifying still and rectifying column allies oneself with uses device links together the discharging pipe of rectifying still and the inlet pipe of rectifying column through the connecting pipe for rectifying still and rectifying column are two independent working equipment, have not only made things convenient for change and maintenance, can replace the practicality of the device of increase with the rectifying column of the model of difference simultaneously.
In order to achieve the above object, the utility model provides a following technical scheme: the support column is fixedly arranged on the working ground through a balancing weight arranged at the bottom of the support column, a pair of clamping pieces are fixedly welded on the right side face of the support column, clamping grooves are formed in the side walls of the clamping pieces, connecting blocks with the same size are fixedly welded on the side walls of the rectification column and the rectification column, the diameter of each connecting block corresponds to the clamping groove of the clamping piece, and the connecting blocks are fixedly arranged in the clamping grooves of the clamping pieces through bolts and nuts, so that the rectification column and the rectification column are fixed on the right side face of the support column and are positioned right above the rectification column; the discharging pipe of the rectifying still is connected with the feeding pipe of the rectifying tower through a connecting pipe, the diameter of the connecting pipe is the same as that of the discharging pipe and the feeding pipe, a pair of guide pipes are welded at the two ends of the connecting pipe, the outer diameter of each guide pipe is the same as that of the inner diameter of each connecting pipe, the connecting pipes are connected with the discharging pipe and the feeding pipe through the guide pipes, a first flange is fixedly welded at the joint of each connecting pipe and the corresponding guide pipe, a second flange is welded at the end part of each discharging pipe and the end part of each feeding pipe, the first flange and the second flange are the same in size, the first flange and the second flange are fixedly connected together through connecting bolts, a rubber pad is installed between the first flange and the second flange, a rotating rod is arranged inside the rectifying still and fixedly installed on an output shaft of a motor through a coupler, and the, the shaft coupling is sealed and installed on the lateral wall of rectifying still to the welding has the stirring leaf on the lateral wall of bull stick, and is connected with the puddler at the terminal surface of bull stick.
As a further aspect of the present invention: the subaerial fixed mounting of left side level of support column has the liquid reserve tank, and the inside bottom surface of liquid reserve tank is provided with the water pump, and the delivery port of water pump passes through the inlet tube and links together with the rectifying column to the inlet tube passes from the inside of support column.
As a further aspect of the present invention: the bottom drain department of rectifying column is connected with the outlet pipe to outlet pipe connection is in the waste material case, and waste material case fixed welding is on the lateral wall of support column.
As a further aspect of the present invention: the middle position welding of bull stick has the montant, and the montant is installed about the bull stick symmetry to be connected with the puddler in the both sides of montant equally.
As a further aspect of the present invention: and a gas pressure gauge is fixedly arranged on the left side of the top of the rectifying still and used for observing the gas pressure in the rectifying still and ensuring that the pressure of the rectifying still is ensured to be within a proper temperature.
As a further aspect of the present invention: and a feed valve is arranged on the feed inlet on the right side of the top of the rectifying still in a threaded manner, and the feed inlet is controlled to be opened and closed through the feed valve.
As a further aspect of the present invention: and a one-way vent valve is fixedly arranged in the middle of the connecting pipe, and only the distilled gas in the rectifying kettle is allowed to enter the rectifying tower.
Compared with the prior art, the beneficial effects of the utility model are that: the utility model fixedly installs the rectifying still and the rectifying tower on the supporting column, and the discharging pipe of the rectifying still and the feeding pipe of the rectifying tower are connected together through the connecting pipe, so that the rectifying still and the rectifying tower are two independent working devices, which not only facilitates the replacement and the maintenance, but also can be replaced by rectifying towers with different models, and the practicability of the added device is improved; simultaneously rectifying still's inside is provided with the bull stick, drives the bull stick through the motor and rotates to drive stirring leaf and three puddler and rotate, stir mixed liquid, guarantee to mix and can fully contact between the liquid, improve reaction rate, distillation efficiency is high.
Drawings
Fig. 1 is a front view of the present invention.
Fig. 2 is a schematic diagram of the internal structure of the rectifying still of the present invention.
Fig. 3 is an enlarged schematic view of the detail at a of the present invention.
Fig. 4 is a schematic view of the structure of the connecting pipe of the present invention.
As shown in the figure: 1. liquid reserve tank, 2, the support column, 3, the rectifying still, 4, the rectifying column, 5, the connecting pipe, 501, first flange, 502, the pipe, 6, the dump bin, 7, the fastener, 8, the connecting block, 9, the bolt, 10, the nut, 11, the water pump, 12, the inlet tube, 13, the outlet pipe, 14, the discharging pipe, 15, the inlet pipe, 16, the one-way vent valve, 17, the second flange, 18, the rubber pad, 19, connecting bolt, 20, the motor, 21, the bull stick, 22, the stirring leaf, 23, the puddler, 24, the montant, 25, the barometer, 26, the feed valve.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted", "provided", "sleeved/connected", "connected", and the like are to be understood in a broad sense, such as "connected", which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-4, in the embodiment of the present invention, a rectifying still and rectifying tower combined device comprises a liquid storage tank 1, a supporting column 2, a rectifying still 3, a rectifying tower 4 and a connecting pipe 5, wherein the supporting column 2 is fixedly installed on the working ground through a balancing weight arranged at the bottom, a pair of fasteners 7 is fixedly welded on the right side surface of the supporting column 2, a clamping groove is formed on the side wall of each fastener 7, a connecting block 8 with the same size is fixedly welded on the side walls of the rectifying still 3 and the rectifying tower 4, the diameter of the connecting block 8 corresponds to the clamping groove of the fastener 7, the connecting block 8 is fixedly installed in the clamping groove of the fastener 7 through a bolt 9 and a nut 10, so that the rectifying still 3 and the rectifying tower 4 are fixed on the right side surface of the supporting column 2, the rectifying tower 4 is positioned right above the rectifying still 3, and the liquid storage tank 1 is fixedly installed on the left horizontal ground of the, the inside bottom surface of liquid reserve tank 1 is provided with water pump 11, water pump 11's delivery port links together through inlet tube 12 and rectifying column 4, and inlet tube 12 passes from the inside of support column 2, make inlet tube 12 safer, provide mixed liquid for rectifying column 4 through liquid reserve tank 1, be connected with outlet pipe 13 in rectifying column 4's bottom discharge outlet department simultaneously, and outlet pipe 13 connects in dump bin 6, 6 fixed welding of dump bin are on the lateral wall of support column 2, collect rectifying column 4 exhaust waste liquid through dump bin 6, convenient recycle.
Wherein, the discharging pipe 14 of the rectifying still 3 and the feeding pipe 15 of the rectifying tower 4 are connected together through a connecting pipe 5, meanwhile, the diameter of the connecting pipe 5 is the same as the diameter of the discharging pipe 14 and the feeding pipe 15, a pair of guide pipes 502 are welded at two ends of the connecting pipe 5, the outer diameter of each guide pipe 502 is the same as the inner diameter of the connecting pipe 5, the connecting pipe 5 is connected with the discharging pipe 14 and the feeding pipe 15 through the guide pipe 502, meanwhile, a first flange 501 is fixedly welded at the joint of the connecting pipe 5 and the guide pipe 502, a second flange 17 is also welded at the end of the discharging pipe 14 and the feeding pipe 15, the first flange 501 and the second flange 17 have corresponding sizes, meanwhile, the first flange 501 and the second flange 17 are fixedly connected together through a connecting bolt 19, a rubber gasket 18 is arranged between the first flange 501 and the second flange 17, and the first flange 501 and the second flange 17 can be meshed together in a sealing, the gas leakage pollution environment caused by the fine gap at the joint of the first flange 501 and the second flange 17 is prevented.
Wherein, rectifying still 3's inside is provided with bull stick 21, bull stick 21 passes through shaft coupling fixed mounting on motor 20's output shaft, motor 20 fixed mounting is on the lateral wall of support column 2, shaft coupling seal installation is on rectifying still 3's lateral wall, the welding has the stirring leaf on the lateral wall of bull stick 21 simultaneously, and the terminal surface at bull stick 21 is connected with puddler 23, there is montant 24 simultaneously in the welding of the intermediate position of bull stick 21, montant 24 is about 21 symmetrical installation of bull stick, and be connected with puddler 23 equally in montant 24's both sides, it rotates to drive bull stick 21 through the motor, thereby drive stirring leaf 22 and three puddler 23 and rotate, stir mixed liquid, guarantee to mix and can fully contact between the liquid, improve reaction rate.
Preferably, a barometer 25 is fixedly installed on the left side of the top of the rectifying still 3 and used for observing the air pressure in the rectifying still 3, so that the pressure of the rectifying still 3 is ensured to be within a proper temperature, meanwhile, a feed valve 26 is installed on a feed port on the right side of the top of the rectifying still 3 in a threaded manner, and the opening and closing of the feed port are controlled through the feed valve 26, so that the situation that evaporated gas overflows from the feed port is avoided.
Preferably, a one-way vent valve 16 is fixedly installed in the middle of the connecting pipe 5, only the distilled gas in the rectifying still 3 is allowed to enter the rectifying tower 4, and the gas in the rectifying tower 4 is effectively prevented from flowing back to enter the rectifying still 3 to pollute the reaction liquid and influence the normal operation of the reaction.
It should be noted that the working principle and the installation manner of the internal structure of the rectifying still 3 and the rectifying tower 4 both adopt the prior art, which is common knowledge of those skilled in the art and will not be described herein again.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention, and the following claims are therefore to be read in this light of the appended claims.

Claims (7)

1. The utility model provides a rectifying still and rectifying column allies oneself with uses device, includes liquid reserve tank (1), support column (2), rectifying still (3), rectifying column (4) and connecting pipe (5), its characterized in that: the support column (2) is fixedly installed on the working ground through a balancing weight arranged at the bottom of the support column (2), a pair of clamping pieces (7) is fixedly welded on the right side face of the support column (2), a clamping groove is formed in the side wall of each clamping piece (7), meanwhile, connecting blocks (8) with the same size are fixedly welded on the side walls of the rectifying still (3) and the rectifying tower (4), the diameter of each connecting block (8) corresponds to the clamping groove of each clamping piece (7), the connecting blocks (8) are fixedly installed in the clamping grooves of the clamping pieces (7) through bolts (9) and nuts (10), so that the rectifying still (3) and the rectifying tower (4) are fixed on the right side face of the support column (2), and the rectifying tower (4) is located right above the rectifying still (3); the discharge pipe (14) of the rectifying still (3) is connected with the feed pipe (15) of the rectifying tower (4) through a connecting pipe (5), meanwhile, the diameter of the connecting pipe (5) is the same as that of the discharge pipe (14) and the feed pipe (15), a pair of guide pipes (502) are welded at two ends of the connecting pipe (5), the outer diameter of each guide pipe (502) is the same as that of the connecting pipe (5), a first flange (501) is fixedly welded at the joint of the connecting pipe (5) and the guide pipes (502), a second flange (17) is also welded at the end parts of the discharge pipe (14) and the feed pipe (15), the first flange (501) and the second flange (17) are the same in size, meanwhile, the first flange (501) and the second flange (17) are fixedly connected together through a connecting bolt (19), and a rubber gasket (18) is arranged between the first flange (501) and the second flange (17), simultaneously the inside of rectifying still (3) is provided with bull stick (21), and bull stick (21) pass through shaft coupling fixed mounting on the output shaft of motor (20), and motor (20) fixed mounting is on the lateral wall of support column (2), and shaft coupling seal installation is on the lateral wall of rectifying still (3) to the welding has the stirring leaf on the lateral wall of bull stick (21), and the terminal surface of bull stick (21) is connected with puddler (23) simultaneously.
2. The apparatus of claim 1, wherein the apparatus comprises: the utility model discloses a rectification tower, including support column (2), the subaerial fixed mounting of left side level of support column (2) has liquid reserve tank (1), and the inside bottom surface of liquid reserve tank (1) is provided with water pump (11), and the delivery port of water pump (11) passes through inlet tube (12) and rectifying column (4) links together to inlet tube (12) are passed from the inside of support column (2).
3. The apparatus of claim 1 or 2, wherein the apparatus comprises: the bottom drain department of rectifying column (4) is connected with outlet pipe (13) to outlet pipe (13) are connected in waste bin (6), and waste bin (6) fixed welding is on the lateral wall of support column (2).
4. The apparatus of claim 1, wherein the apparatus comprises: the middle position welding of bull stick (21) has montant (24), and montant (24) are installed about bull stick (21) symmetry to be connected with puddler (23) in the both sides of montant (24) equally.
5. The apparatus of claim 1, wherein the apparatus comprises: and a barometer (25) is fixedly arranged on the left side of the top of the rectifying still (3).
6. The apparatus of claim 1 or 5, wherein: and a feed valve (26) is installed on the feed inlet on the right side of the top of the rectifying still (3) in a threaded manner.
7. The apparatus of claim 1, wherein the apparatus comprises: a one-way vent valve (16) is fixedly arranged in the middle of the connecting pipe (5) and only allows the distilled gas in the rectifying still (3) to enter the rectifying tower (4).
CN202020574957.8U 2020-04-17 2020-04-17 Rectifying still and rectifying tower combined device Expired - Fee Related CN212491609U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202020574957.8U CN212491609U (en) 2020-04-17 2020-04-17 Rectifying still and rectifying tower combined device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202020574957.8U CN212491609U (en) 2020-04-17 2020-04-17 Rectifying still and rectifying tower combined device

Publications (1)

Publication Number Publication Date
CN212491609U true CN212491609U (en) 2021-02-09

Family

ID=74431740

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202020574957.8U Expired - Fee Related CN212491609U (en) 2020-04-17 2020-04-17 Rectifying still and rectifying tower combined device

Country Status (1)

Country Link
CN (1) CN212491609U (en)

Similar Documents

Publication Publication Date Title
CN207605634U (en) With sampling and the chemical industry solutions mixed stirring device being quickly cooled down
CN212491609U (en) Rectifying still and rectifying tower combined device
WO2022252604A1 (en) Safe reactor for leaching of waste battery powder and capable of controlling hydrogen concentration
CN107899462A (en) With sampling and the chemical industry solutions mixed stirring device quickly cooled down
CN112121457A (en) Crystallization container for high-temperature crystallization of manganese sulfate
CN211997855U (en) Device for filling pearlife on air separation cold box
CN209130369U (en) A kind of oil pipeline receiving ball tube automatic exhaust device
CN212717966U (en) Easy-to-clean liquid seal device for chloroprene rubber degasser
CN208229881U (en) A kind of production of chloroacetic acid reaction kettle of easy access
CN214183008U (en) Low freezing point toluene apparatus for producing
CN221048850U (en) Nitrogen reflux box with uniform cooling
CN214232838U (en) Crystallization container for high-temperature crystallization of manganese sulfate
CN2549236Y (en) Integrated separating and cooling liquid circulating pump
CN217583253U (en) Solid impurity collecting device for low-temperature slurry material
CN213865495U (en) Multilayer baffling type oil-water separator
CN206156732U (en) Filling device is stored in ultrapure coolant liquid filling of water -cooled frequency converter
CN219994688U (en) Be used for flowmeter flange antiseep sealing mechanism
CN219502602U (en) Dispersing device for rust remover allocation
CN220194819U (en) Sealing structure of chemical production reaction kettle
CN214389673U (en) Stainless steel bucket with mixing function
CN211358824U (en) Pump capable of improving chemical raw material reaction efficiency
CN202383153U (en) Liquid flow indicator
CN211837858U (en) Novel reaction kettle
CN220945966U (en) Self-leveling cement mixing device
CN211913763U (en) Visual cauldron

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20210209