CN212441203U - Coal tar coproduction ammonium sulfate reation kettle for production reagent - Google Patents
Coal tar coproduction ammonium sulfate reation kettle for production reagent Download PDFInfo
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- CN212441203U CN212441203U CN202020834016.3U CN202020834016U CN212441203U CN 212441203 U CN212441203 U CN 212441203U CN 202020834016 U CN202020834016 U CN 202020834016U CN 212441203 U CN212441203 U CN 212441203U
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- cauldron body
- ammonium sulfate
- coal tar
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- reagent
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Abstract
The utility model discloses a coal tar attaches produces reation kettle for ammonium sulfate production reagent, including the cauldron body, the top of the cauldron body is provided with feed inlet and inlet, and the bottom of the cauldron body is provided with the liquid outlet, be provided with the solenoid valve in the liquid outlet, the bottom fixedly connected with supporting legs of the cauldron body is provided with the electrical heating board on the inner wall of the cauldron body, and cauldron body center department rotates and is connected with the pivot, through a set of stirring vane of petiole fixedly connected with in the pivot, cauldron body top fixedly connected with mounting panel, fixed mounting motor on the mounting panel, the output shaft and the pivot fixed connection of motor. The utility model discloses a simple structure, the reliability is high, and the coal tar that reaction rate is fast is attached to produce reation kettle for ammonium sulfate production reagent.
Description
Technical Field
The utility model relates to an ammonium sulfate production facility technical field specifically is a coal tar attaches to produce reation kettle for ammonium sulfate production reagent.
Background
The main reason that the coking by-product ammonium sulfate affects the clarity and the burning residue of the reagent ammonium sulfate product is organic substances brought in the coking by-product ammonium sulfate, and a method must be considered for removing the organic substances brought in the ammonium sulfate and eliminating the influence on the quality of the reagent ammonium sulfate product so as to solve the problems of the clarity and the burning residue of the reagent ammonium sulfate production. The coking by-product ammonium sulfate is used as a raw material, organic matters are oxidized by utilizing the strong oxidizing property of ammonium persulfate, and colloidal substances in the solution are adsorbed by utilizing the adsorption capacity of activated carbon, so that the aim of purifying the solution is fulfilled, and a reagent ammonium sulfate product meeting the quality requirement of the reagent is obtained through concentrated crystallization. At present, the existing reaction kettle for producing the reagent by producing ammonium sulfate from the coal tar mostly has the defect of poor stirring effect in the using process, so that the uniformity of the solution is poor, and the quality of a final product is influenced.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a coal tar is attached to produce reation kettle for ammonium sulfate production reagent to solve the problem of proposing in the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme:
the utility model provides a coal tar attaches produces reation kettle for ammonium sulfate production reagent, includes the cauldron body, the top of the cauldron body is provided with feed inlet and inlet, and the bottom of the cauldron body is provided with the liquid outlet, be provided with the solenoid valve in the liquid outlet, the bottom fixedly connected with supporting legs of the cauldron body is provided with the electrical heating board on the inner wall of the cauldron body, and cauldron body center department rotates and is connected with the pivot, through a set of stirring vane of petiole fixedly connected with in the pivot, cauldron body top fixedly connected with mounting panel, fixed mounting motor on the mounting panel, the output shaft and the pivot fixed connection of motor.
Preferably, a material cylinder is arranged below the feeding hole, a buffer device is arranged in the material cylinder, the buffer device comprises a spiral blade, a mounting seat is arranged at the lower end of the material cylinder, and the spiral blade is rotatably connected to the mounting seat.
Preferably, the inner wall of the kettle body is fixedly connected with a fixing rod, the center of the fixing rod is fixedly connected with a shaft sleeve, and the rotating shaft is rotatably connected in the shaft sleeve.
Preferably, the lower extreme fixedly connected with puddler of pivot, the puddler is the arc structure with the laminating of cauldron body bottom.
Preferably, the side wall of the kettle body is provided with a heat insulation layer.
Preferably, the heat insulation layer is filled with perlite.
Compared with the prior art, the beneficial effects of the utility model are that: the utility model discloses the during operation, stirring vane compares in traditional stirring rod, can make the internal solution from bottom to top motion of cauldron, is favorable to making the solute dissolve fast. When the feed inlet feeds in raw material, helical blade is forced to rotate when the material passes through the feed cylinder, can avoid material direct impact stirring vane. The stirring rod can prevent the solute from depositing at the bottom of the kettle body. The heat preservation layer improves the thermal insulation performance of the kettle body and reduces energy consumption. The utility model discloses a simple structure, the reliability is high, and the coal tar that reaction rate is fast is attached to produce reation kettle for ammonium sulfate production reagent.
Drawings
FIG. 1 is a schematic structural diagram of a reaction kettle for producing a reagent by coal tar by-product ammonium sulfate;
fig. 2 is a partially enlarged view of fig. 1 at K.
In the figure: 1-supporting legs, 2-kettle body, 3-insulating layer, 4-electric heating plate, 5-mounting plate, 6-motor, 7-rotating shaft, 8-fixing rod, 9-shaft sleeve, 10-blade handle, 11-stirring blade, 12-liquid inlet, 13-liquid inlet, 14-liquid outlet, 15-stirring rod, 16-electromagnetic valve, 17-material barrel, 18-mounting seat, 19-helical blade and 20-buffer device.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-2, the present invention provides a technical solution:
the utility model provides a coal tar subsidiary product ammonium sulfate reation kettle for reagent, includes the cauldron body 2, the top of the cauldron body 2 is provided with feed inlet 13 and inlet 12, and the bottom of the cauldron body 2 is provided with liquid outlet 14, be provided with solenoid valve 16 in the liquid outlet 14, the bottom fixedly connected with supporting legs 1 of the cauldron body 2 is provided with electrical heating board 4 on the inner wall of the cauldron body 2, and 2 center departments of the cauldron body rotate and are connected with pivot 7, through a set of stirring vane 11 of 10 fixedly connected with of petioles in the pivot 7, 2 top fixedly connected with mounting panel 5 of the cauldron body, fixed mounting motor 6 on mounting panel 5, the output shaft and the 7 fixed connection of pivot of motor 6.
During work, 1000 Kg of pure water and 1500Kg of pure water are added into the kettle body 2, the electric heating plate 4 is heated, the stirring blades 11 are started to stir, 1500Kg of treated ammonium sulfate are added, the pure water is supplemented to dissolve the ammonium sulfate, about 10Kg of ammonium persulfate is added into each kettle to carry out oxidation treatment, the temperature is controlled to be 70-800 ℃, and the specific gravity of the solution is 1.17-1.19. Adjusting pH to 7.0 or more with ammonia water, adding 4-5Kg of ammonium bicarbonate, adjusting pH to 7.0 or more with ammonia water, adding 1-2Kg of activated carbon, and keeping the temperature overnight for use in the next ring segment; compared with a traditional stirring rod, the stirring blade 11 can enable the solution in the kettle body 2 to move from bottom to top, and is favorable for quickly dissolving the solute.
Preferably, a barrel 17 is arranged below the feed inlet 13, a buffer device 20 is arranged in the barrel 17, the buffer device 20 comprises a helical blade 19, a mounting seat 18 is arranged at the lower end of the barrel 17, and the helical blade 19 is rotatably connected to the mounting seat 18.
When the material is fed from the feeding hole 13, the helical blade 19 is forced to rotate when the material passes through the charging barrel 17, so that the material can be prevented from directly colliding with the stirring blade 11.
Preferably, a fixing rod 8 is fixedly connected to the inner wall of the kettle body 2, a shaft sleeve 9 is fixedly connected to the center of the fixing rod 8, and the rotating shaft 7 is rotatably connected to the shaft sleeve 9.
The shaft sleeve 9 is used for mounting the rotating shaft 7.
Preferably, the lower end of the rotating shaft 7 is fixedly connected with a stirring rod 15, and the stirring rod 15 is of a circular arc structure attached to the bottom of the kettle body 2.
The stirring rod 15 prevents the solute from being deposited on the bottom of the vessel body 2.
Preferably, the side wall of the kettle body 2 is provided with an insulating layer 3.
The heat preservation layer 3 improves the heat preservation performance of the kettle body 2 and reduces the energy consumption.
Preferably, the insulating layer 3 is filled with perlite.
The perlite has the advantages of heat preservation, heat resistance and low price.
The utility model discloses a theory of operation is: during work, 1000 Kg of pure water and 1500Kg of pure water are added into the kettle body 2, the electric heating plate 4 is heated, the stirring blades 11 are started to stir, 1500Kg of treated ammonium sulfate are added, the pure water is supplemented to dissolve the ammonium sulfate, about 10Kg of ammonium persulfate is added into each kettle to carry out oxidation treatment, the temperature is controlled to be 70-800 ℃, and the specific gravity of the solution is 1.17-1.19. Adjusting pH to 7.0 or more with ammonia water, adding 4-5Kg of ammonium bicarbonate, adjusting pH to 7.0 or more with ammonia water, adding 1-2Kg of activated carbon, and keeping the temperature overnight for use in the next ring segment; compared with a traditional stirring rod, the stirring blade 11 can enable the solution in the kettle body 2 to move from bottom to top, and is favorable for quickly dissolving the solute. When the material is fed from the feeding hole 13, the helical blade 19 is forced to rotate when the material passes through the charging barrel 17, so that the material can be prevented from directly colliding with the stirring blade 11. The shaft sleeve 9 is used for mounting the rotating shaft 7. The stirring rod 15 prevents the solute from being deposited on the bottom of the vessel body 2. The heat preservation layer 3 improves the heat preservation performance of the kettle body 2 and reduces the energy consumption. The perlite has the advantages of heat preservation, heat resistance and low price.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (6)
1. The utility model provides a coal tar coproduces reation kettle for ammonium sulfate production reagent, includes the cauldron body (2), its characterized in that: the top of the cauldron body (2) is provided with feed inlet (13) and inlet (12), and the bottom of the cauldron body (2) is provided with liquid outlet (14), be provided with solenoid valve (16) in liquid outlet (14), bottom fixedly connected with supporting legs (1) of the cauldron body (2), be provided with electric heating board (4) on the inner wall of the cauldron body (2), cauldron body (2) center department rotates and is connected with pivot (7), go up in pivot (7) through a set of stirring vane (11) of petiole (10) fixedly connected with, cauldron body (2) top fixedly connected with mounting panel (5), fixed mounting motor (6) are gone up in mounting panel (5), the output shaft and pivot (7) fixed connection of motor (6).
2. The reaction kettle for the reagent for producing ammonium sulfate by coal tar according to claim 1, is characterized in that: feed inlet (13) below is provided with feed cylinder (17), be provided with buffer (20) in feed cylinder (17), buffer (20) include helical blade (19), the lower extreme of feed cylinder (17) is provided with mount pad (18), helical blade (19) rotate to be connected on mount pad (18).
3. The reaction kettle for the reagent for producing ammonium sulfate by coal tar according to claim 1, is characterized in that: fixedly connected with dead lever (8) on the inner wall of cauldron body (2), dead lever (8) center department fixedly connected with axle sleeve (9), pivot (7) rotate to be connected in axle sleeve (9).
4. The reaction kettle for the reagent for producing ammonium sulfate by coal tar according to claim 1, is characterized in that: the lower extreme fixedly connected with puddler (15) of pivot (7), puddler (15) are the arc structure with the laminating of cauldron body (2) bottom.
5. The reaction kettle for the reagent for producing ammonium sulfate by coal tar according to claim 1, is characterized in that: and a heat-insulating layer (3) is arranged on the side wall of the kettle body (2).
6. The reaction kettle for the reagent for producing ammonium sulfate by-produced from coal tar as claimed in claim 5, is characterized in that: the heat-insulating layer (3) is filled with perlite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020834016.3U CN212441203U (en) | 2020-05-18 | 2020-05-18 | Coal tar coproduction ammonium sulfate reation kettle for production reagent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020834016.3U CN212441203U (en) | 2020-05-18 | 2020-05-18 | Coal tar coproduction ammonium sulfate reation kettle for production reagent |
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| Publication Number | Publication Date |
|---|---|
| CN212441203U true CN212441203U (en) | 2021-02-02 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202020834016.3U Active CN212441203U (en) | 2020-05-18 | 2020-05-18 | Coal tar coproduction ammonium sulfate reation kettle for production reagent |
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| CN (1) | CN212441203U (en) |
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- 2020-05-18 CN CN202020834016.3U patent/CN212441203U/en active Active
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