CN212269478U - Apparatus for producing of high-purity manganese sulfate - Google Patents
Apparatus for producing of high-purity manganese sulfate Download PDFInfo
- Publication number
- CN212269478U CN212269478U CN202020511006.6U CN202020511006U CN212269478U CN 212269478 U CN212269478 U CN 212269478U CN 202020511006 U CN202020511006 U CN 202020511006U CN 212269478 U CN212269478 U CN 212269478U
- Authority
- CN
- China
- Prior art keywords
- wall
- manganese sulfate
- tank
- purity manganese
- rotating rod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
The utility model discloses a apparatus for producing of high-purity manganese sulfate, comprising a base plate, the top outer wall of bottom plate is provided with retort, collecting box and gunbarrel, and the top outer wall both sides of collecting box all are provided with the supporting leg, the top outer wall of supporting leg is provided with the extraction jar, and the top outer wall of retort, extraction jar and gunbarrel is provided with first rabbling mechanism, second rabbling mechanism and third rabbling mechanism respectively, one side outer wall of extraction jar is provided with transparent observation window, and the bottom inner wall of extraction jar and the top inner wall of collecting box set up same third pipe, and one side outer wall of third pipe is provided with the capacity solenoid valve. The utility model discloses a be provided with extraction jar, transparent observation window, third pipe, capacity solenoid valve, fourth pipe and fourth solenoid valve, when extracting, observe the boundary through transparent observation window, the accessible is opened capacity solenoid valve and fourth solenoid valve and is carried out the ejection of compact respectively, can effectual improvement device extraction efficiency.
Description
Technical Field
The utility model relates to a high-purity manganese sulfate technical field especially relates to a apparatus for producing of high-purity manganese sulfate.
Background
Manganese sulfate (chemical formula is MnSO4, formula weight 151.00), monohydrate of which is reddish orthorhombic crystal, has relative density of 3.50 and melting point of 700 ℃, is easily soluble in water and insoluble in ethanol. It exists in the form of various hydrates.
When manganese sulfate produced, at first need add raw materials manganese dioxide and sulphuric acid respectively and carry out abundant mixture and reaction in the retort, and then can produce the manganese sulfate product, the manganese sulfate product of production can obtain high-purity manganese sulfate through extraction and precipitation many times, but when extracting at present, need the staff to extract and separate it manually, need consume a large amount of time, reduced work efficiency, lead to the practicality of device lower.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects existing in the prior art and providing a production device of high-purity manganese sulfate.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
the utility model provides a apparatus for producing of high-purity manganese sulfate, includes the bottom plate, the top outer wall of bottom plate is provided with retort, collecting box and gunbarrel, and the top outer wall both sides of collecting box all are provided with the supporting leg, the top outer wall of supporting leg is provided with the extraction jar, and the top outer wall of retort, extraction jar and gunbarrel is provided with first rabbling mechanism, second rabbling mechanism and third rabbling mechanism respectively, one side outer wall of extraction jar is provided with transparent observation window, and the bottom inner wall of extraction jar and the top inner wall of collecting box set up same third pipe, and one side outer wall of third pipe is provided with the capacity solenoid valve, one side inner wall of extraction jar and one side inner wall of gunbarrel set up same fourth pipe, and one side outer wall of fourth pipe is provided with the fourth solenoid valve.
Furthermore, first rabbling mechanism is including first motor, and the output shaft of first motor has first bull stick through the coupling joint, and the outer wall of first bull stick is provided with the first puddler that the equidistance distributes.
Furthermore, the second stirring mechanism comprises a second motor, an output shaft of the second motor is connected with a second rotating rod through a coupler, and second stirring rods distributed at equal intervals are arranged on the outer wall of the second rotating rod.
Furthermore, the third stirring mechanism comprises a third motor, an output shaft of the third motor is connected with a third rotating rod through a coupler, and third stirring rods distributed at equal intervals are arranged on the outer wall of the third rotating rod.
Furthermore, the outer wall of the reaction tank is provided with a heat insulation sleeve, the outer wall of one side of the heat insulation sleeve is provided with an absorption box, and the inner wall of the top of the absorption box and the inner wall of one side of the reaction tank are provided with the same first guide pipe.
Furthermore, the top outer wall of retort is provided with the pump body, and the input of the pump body and the top inner wall of retort set up same second pipe, and the output of the pump body and the top inner wall of extraction jar set up same fifth pipe.
Further, the inner wall both sides of gunbarrel all are provided with the slot, and the inner wall of slot is pegged graft and is had the inserted block, and the top outer wall of inserted block is provided with the pull ring, and one side outer wall of inserted block is provided with the filter.
Furthermore, still including setting up in the down tube of first bull stick outer wall both sides, one side of down tube is provided with the connecting rod that the equidistance distributes, and the specification variation in size of connecting rod.
Compared with the prior art, the utility model provides a device for producing of high-purity manganese sulfate possesses following beneficial effect:
1. this apparatus for producing of high-purity manganese sulfate through being provided with extraction jar, transparent observation window, third pipe, capacity solenoid valve, fourth pipe and fourth solenoid valve, when extracting, observes the boundary through transparent observation window, and the accessible is opened capacity solenoid valve and fourth solenoid valve and is carried out the ejection of compact respectively, can the effectual efficiency that improves the device extraction.
2. This apparatus for producing of high-purity manganese sulfate through being provided with insulation cover, first pipe and absorption box, when reacting to manganese dioxide and sulphuric acid, can produce oxygen and few vapor, and the first pipe of accessible is absorbed in leading-in the absorption box with it, has improved the practicality of device.
3. This apparatus for producing of high-purity manganese sulfate through being provided with slot, inserted block, pull ring and filter, when the gunbarrel carries out the precipitation reaction, the filter can separate the precipitate to the speed, can be quick through the mode of the mutual grafting of slot and inserted block install the filter.
4. This apparatus for producing of high-purity manganese sulfate, through being provided with down tube and connecting rod, the different whirlpools that all can produce the difference when stirring of the angle difference of down tube and the length difference of connecting rod can improve the mixed effect of retort, has improved the practicality of device.
The parts of the device not involved are the same as or can be implemented using prior art.
Drawings
FIG. 1 is a schematic structural diagram of a production apparatus for high-purity manganese sulfate according to embodiment 1 of the present invention;
FIG. 2 is a schematic structural view of a filter plate of a high purity manganese sulfate production apparatus according to example 1 of the present invention;
FIG. 3 is a schematic structural view of a transparent observation window of a high-purity manganese sulfate production apparatus according to embodiment 1 of the present invention;
fig. 4 is a schematic structural diagram of an inclined rod of a production device for high-purity manganese sulfate according to embodiment 2 of the present invention.
In the figure: 1-bottom plate, 2-insulating sleeve, 3-absorption box, 4-first conduit, 5-reaction tank, 6-first motor, 7-first rotating rod, 8-pump body, 9-second conduit, 10-first stirring rod, 11-collecting box, 12-third conduit, 13-capacity electromagnetic valve, 14-fourth conduit, 15-fourth electromagnetic valve, 16-fifth conduit, 17-second motor, 18-extraction tank, 19-second stirring rod, 20-third motor, 21-third rotating rod, 22-filter plate, 23-settling tank, 24-slot, 25-insert block, 26-pull ring, 27-transparent observation window, 28-oblique rod and 29-connecting rod.
Detailed Description
The technical solution of the present patent will be described in further detail with reference to the following embodiments.
Reference will now be made in detail to embodiments of the present patent, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are exemplary only for the purpose of explaining the present patent and are not to be construed as limiting the present patent.
In the description of this patent, it is to be understood that the terms "center," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in the orientations and positional relationships indicated in the drawings for the convenience of describing the patent and for the simplicity of description, and are not intended to indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and are not to be considered limiting of the patent.
In the description of this patent, it is noted that unless otherwise specifically stated or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly and can include, for example, fixedly connected, disposed, detachably connected, disposed, or integrally connected and disposed. The specific meaning of the above terms in this patent may be understood by those of ordinary skill in the art as appropriate.
Example 1
Referring to fig. 1-3, a production device of high-purity manganese sulfate comprises a bottom plate 1, a reaction tank 5, a collection tank 11 and a precipitation tank 23 are fixed on the outer wall of the top of the bottom plate 1 through screws, supporting legs are welded on two sides of the outer wall of the top of the collection tank 11, an extraction tank 18 is welded on the outer wall of the top of the supporting legs, a first stirring mechanism, a second stirring mechanism and a third stirring mechanism are respectively fixed on the outer walls of the top of the reaction tank 5, the extraction tank 18 and the precipitation tank 23 through screws, a transparent observation window 27 is arranged on the outer wall of one side of the extraction tank 18, the inner wall of the bottom of the extraction tank 18 and the inner wall of the top of the collection tank 11 are connected with a same third guide pipe 12 through flanges, a capacity electromagnetic valve 13 is connected on the outer wall of one side of the third guide pipe 12 through threads, and a fourth solenoid valve 15 is threadedly connected to an outer wall of one side of the fourth guide duct 14.
In the utility model, the first stirring mechanism comprises a first motor 6, the output shaft of the first motor 6 is connected with a first rotating rod 7 through a coupling joint, the outer wall of the first rotating rod 7 is welded with first stirring rods 10 which are distributed equidistantly, the second stirring mechanism comprises a second motor 17, the output shaft of the second motor 17 is connected with a second rotating rod through a coupling joint, the outer wall of the second rotating rod is welded with second stirring rods 19 which are distributed equidistantly, the third stirring mechanism comprises a third motor 20, the output shaft of the third motor 20 is connected with a third rotating rod 21 through a coupling joint, the outer wall of the third rotating rod 21 is welded with third stirring rods which are distributed equidistantly, the outer wall of the reaction tank 5 is welded with a heat-insulating sleeve 2, the outer wall of one side of the heat-insulating sleeve 2 is fixed with an absorption tank 3 through screws, the inner wall of the top of the absorption tank 3 and the inner wall of one side of the reaction tank 5 are connected with a same first conduit, the top outer wall of retort 5 has the pump body 8 through the fix with screw, and there is same second pipe 9 at the input of the pump body 8 and the top inner wall of retort 5 through flange joint, there is same fifth pipe 16 at the output of the pump body 8 and the top inner wall of extraction jar 18 through flange joint, slot 24 has all been welded to the inner wall both sides of gunbarrel 23, and the inner wall of slot 24 is pegged graft and is had inserted block 25, the top outer wall of inserted block 25 has pull ring 26 through the fix with screw, one side outer wall of inserted block 25 has filter 22 through the fix with screw.
The working principle is as follows: connecting the equipment with a power supply, firstly adding reactants into a reaction tank 5, turning on a first motor 6, driving a rotating rod 7 and a first stirring rod 10 by the first motor 6 to fully mix the reactants, after the reaction is finished, opening a pump body 8, guiding a product into an extraction tank 18 through a second conduit 9 and a fifth conduit 16, adding an extraction liquid into the extraction tank 18, turning on a second motor 17, driving a second rotating rod and a second stirring rod 19 by the second motor 17 to fully mix, standing for a period of time after uniform mixing, adjusting the opening degree of a capacity electromagnetic valve 13 when an obvious boundary is observed from a transparent observation window 27, slowly discharging, finally turning on a fourth electromagnetic valve 15, guiding an upper-layer solution into a precipitation tank 23, and adding a precipitator for precipitation.
Example 2
Referring to fig. 4, in the present embodiment, compared with embodiment 1, the apparatus for producing high-purity manganese sulfate further includes inclined rods 28 welded to two sides of the outer wall of the first rotating rod 7, connecting rods 29 are welded to one side of the inclined rods 28, and the connecting rods 29 have different specifications.
The working principle is as follows: connecting the equipment with a power supply, firstly adding reactants into a reaction tank 5, opening a first motor 6, driving a rotating rod 7 and a first stirring rod 10 by the first motor 6 to fully mix the reactants, after the reaction is finished, opening a pump body 8, guiding a product into an extraction tank 18 through a second guide pipe 9 and a fifth guide pipe 16, adding an extraction liquid into the extraction tank 18, opening a second motor 17, driving a second rotating rod and a second stirring rod 19 by the second motor 17 to fully mix, standing for a period of time after uniform mixing, adjusting the opening degree of a capacity electromagnetic valve 13 when an obvious boundary is observed from a transparent observation window 27, slowly discharging, finally opening a fourth electromagnetic valve 15, guiding an upper-layer solution into a precipitation tank 23, adding a precipitator for precipitation, and generating different vortexes when stirring is carried out due to different angles of an inclined rod 28 and different lengths of a connecting rod 29, the mixing effect of the reaction tank 5 can be improved.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (8)
1. A production device of high-purity manganese sulfate comprises a bottom plate (1) and is characterized in that a reaction tank (5), a collection tank (11) and a precipitation tank (23) are arranged on the outer wall of the top of the bottom plate (1), supporting legs are arranged on two sides of the outer wall of the top of the collection tank (11), an extraction tank (18) is arranged on the outer wall of the top of each supporting leg, a first stirring mechanism, a second stirring mechanism and a third stirring mechanism are respectively arranged on the outer walls of the top of the reaction tank (5), the extraction tank (18) and the precipitation tank (23), a transparent observation window (27) is arranged on the outer wall of one side of the extraction tank (18), the inner wall of the bottom of the extraction tank (18) and the inner wall of the top of the collection tank (11) are provided with a same third guide pipe (12), a capacity electromagnetic valve (13) is arranged on the outer wall of one side of the third guide pipe (12), and a fourth guide pipe (14) is, and a fourth electromagnetic valve (15) is arranged on the outer wall of one side of the fourth conduit (14).
2. The production device of high-purity manganese sulfate according to claim 1, wherein the first stirring mechanism comprises a first motor (6), an output shaft of the first motor (6) is connected with a first rotating rod (7) through a coupling, and the outer wall of the first rotating rod (7) is provided with first stirring rods (10) which are distributed equidistantly.
3. The production device of high-purity manganese sulfate according to claim 2, wherein the second stirring mechanism comprises a second motor (17), an output shaft of the second motor (17) is connected with a second rotating rod through a coupling, and second stirring rods (19) are arranged on the outer wall of the second rotating rod and distributed at equal intervals.
4. The production device of high-purity manganese sulfate according to claim 3, wherein the third stirring mechanism comprises a third motor (20), an output shaft of the third motor (20) is connected with a third rotating rod (21) through a coupling, and the outer wall of the third rotating rod (21) is provided with third stirring rods distributed at equal intervals.
5. The production device of high-purity manganese sulfate according to claim 1, wherein the outer wall of the reaction tank (5) is provided with a heat insulating sleeve (2), the outer wall of one side of the heat insulating sleeve (2) is provided with an absorption box (3), and the inner wall of the top of the absorption box (3) and the inner wall of one side of the reaction tank (5) are provided with the same first conduit (4).
6. The production device of high-purity manganese sulfate according to claim 5, wherein the top outer wall of the reaction tank (5) is provided with a pump body (8), the input end of the pump body (8) and the top inner wall of the reaction tank (5) are provided with the same second conduit (9), and the output end of the pump body (8) and the top inner wall of the extraction tank (18) are provided with the same fifth conduit (16).
7. The production device of high-purity manganese sulfate according to claim 6, wherein slots (24) are formed in both sides of the inner wall of the precipitation tank (23), insertion blocks (25) are inserted into the inner walls of the slots (24), pull rings (26) are arranged on the outer walls of the tops of the insertion blocks (25), and filter plates (22) are arranged on the outer walls of one sides of the insertion blocks (25).
8. The production device of high-purity manganese sulfate according to claim 1, further comprising inclined rods (28) arranged on two sides of the outer wall of the first rotating rod (7), wherein connecting rods (29) are arranged on one side of each inclined rod (28) and are distributed equidistantly, and the connecting rods (29) are different in size.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020511006.6U CN212269478U (en) | 2020-04-09 | 2020-04-09 | Apparatus for producing of high-purity manganese sulfate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020511006.6U CN212269478U (en) | 2020-04-09 | 2020-04-09 | Apparatus for producing of high-purity manganese sulfate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212269478U true CN212269478U (en) | 2021-01-01 |
Family
ID=73876973
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202020511006.6U Active CN212269478U (en) | 2020-04-09 | 2020-04-09 | Apparatus for producing of high-purity manganese sulfate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212269478U (en) |
-
2020
- 2020-04-09 CN CN202020511006.6U patent/CN212269478U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN212269478U (en) | Apparatus for producing of high-purity manganese sulfate | |
| CN219513121U (en) | Diffusion furnace for producing topcon battery piece with uniform diffusion | |
| CN207845504U (en) | Ardealite pretreatment unit | |
| CN211988443U (en) | Continuous mixing device for acidizing fracturing fluid | |
| CN112408566A (en) | Environment-friendly sewage treatment equipment based on convection impact principle | |
| CN112279975A (en) | Efficient polycarboxylic acid composite additive and preparation equipment | |
| CN108144479A (en) | A kind of material stirring mixing arrangement that can be carried out at the same time different proportion mixing | |
| CN215586080U (en) | Automatic proportioning and mixing device for herbicide production | |
| CN216260770U (en) | Polyester polyol continuous production device | |
| CN210384926U (en) | Mixed reaction device for dilute alkali extraction process of cartilage sulfate | |
| CN210186999U (en) | Raw materials dual cycle stirring mixing apparatus of compound fertilizer production usefulness | |
| CN209832152U (en) | Mixing arrangement is used in concrete processing | |
| CN214438605U (en) | Premixing system for sulfuric acid method titanium dioxide production process | |
| CN207827873U (en) | A kind of potassium sulfate Mannheim reburner with netted divider | |
| CN209161989U (en) | A kind of biodiesel is efficiently acidified reaction system | |
| CN202155162U (en) | Double-helix consecutive mixing machine for preparing lithium battery cathode material | |
| CN208836829U (en) | A kind of charger for Terrapin raising | |
| CN208378426U (en) | A kind of energy conservation and environmental protection prepares the device of LiFePO4 | |
| CN206591062U (en) | A kind of efficient slump retaining agent synthesis device | |
| CN106892461A (en) | A kind of catalyst preparation device | |
| CN207432470U (en) | A kind of concrete central mix plant | |
| CN217747006U (en) | Continuous feeding structure for preparing ethylene sulfite | |
| CN213790012U (en) | A mix liquid purification device for chemical production | |
| CN213078167U (en) | Agricultural fertilizer raw materials proportioning device | |
| CN206415116U (en) | Rare earth oxide automatic producing device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A production device of high purity manganese sulfate Effective date of registration: 20220119 Granted publication date: 20210101 Pledgee: Bank of Guilin Co.,Ltd. Qinzhou branch Pledgor: Qinzhou Nanhai Chemical Co.,Ltd. Registration number: Y2022450000011 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20230221 Granted publication date: 20210101 Pledgee: Bank of Guilin Co.,Ltd. Qinzhou branch Pledgor: Qinzhou Nanhai Chemical Co.,Ltd. Registration number: Y2022450000011 |
|
| PC01 | Cancellation of the registration of the contract for pledge of patent right |