CN212167228U - Vacuum stirring refining system - Google Patents

Vacuum stirring refining system Download PDF

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Publication number
CN212167228U
CN212167228U CN202020591253.1U CN202020591253U CN212167228U CN 212167228 U CN212167228 U CN 212167228U CN 202020591253 U CN202020591253 U CN 202020591253U CN 212167228 U CN212167228 U CN 212167228U
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supporting plate
container
inclination
vacuum
casing
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CN202020591253.1U
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Chinese (zh)
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宋晶尧
谭洁仪
李涛
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Guangzhou Chinaray Optoelectronic Materials Ltd
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Guangzhou Chinaray Optoelectronic Materials Ltd
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Abstract

The utility model relates to a vacuum stirring refining system, include: container, cavity, heating member, casing, vacuum pump, agitating unit and drive arrangement. The container is used for containing materials. The heating element is used for heating the chamber. The container, the chamber and the heating member are all arranged in the machine shell. The vacuum pump is communicated with the chamber of the container through a pipeline. The stirring device is used for stirring the materials in the container. The driving device is used for driving the machine shell to act so that the material heated and melted in the container can infiltrate the inner side wall of the container. The driving device can drive the machine shell to act, the material in a melting state in the container infiltrates the inner side wall of the container when the machine shell acts, the material attached to the inner side wall of the container is fully mixed with other materials when the material in the melting state infiltrates the inner side wall of the container, the deviation of the mass proportion of each material in the finally obtained mixed product to the preset mass proportion is small, and the qualified rate of the mixed product is high.

Description

Vacuum stirring refining system
Technical Field
The utility model relates to a vacuum stirring refining technical field especially relates to a vacuum stirring refining system.
Background
With the development of new material technology, a vacuum stirring and homogenizing system is developed, which is a system for stirring and homogenizing materials (specifically, organic small molecular materials) with various specific mass ratios in a vacuum environment by heating the materials to a molten state.
The traditional vacuum stirring and refining system comprises a crucible, a heating body for heating the crucible, a closed cavity for placing the crucible, a vacuum pump for vacuumizing the closed cavity, and a stirring device for uniformly stirring materials in the crucible. During specific work, materials with various specific mass ratios are filled into the crucible, the amount of the filled materials in the crucible is not more than the volume of a cavity of the crucible, then the crucible is placed into the cavity and fixed, the stirring device is placed and the furnace cover is covered, the vacuum pump is adopted to carry out vacuumizing treatment on the cavity, then the crucible is heated, so that the materials in the crucible are heated to a melting state and are uniformly mixed under the stirring effect of the stirring device, and finally, a mixed product can be obtained by cooling the uniformly mixed materials. However, the deviation between the mass ratio of each material in the finally obtained mixed product and the preset mass ratio is large, and the qualified rate of the mixed product is low.
SUMMERY OF THE UTILITY MODEL
Based on this, it is necessary to provide a vacuum stirring and homogenizing system for solving the problems of the prior art that the deviation between the mass ratio of each material in the finally obtained mixed product and the preset mass ratio is large and the qualified rate of the mixed product is low.
The technical scheme is as follows: a vacuum stirred blending system, the vacuum stirred blending system comprising: a container for holding a material; the chamber is a vacuum chamber and is used for placing a container; a heating member for heating the container; the chamber and the heating element are arranged in the machine shell; the vacuum pump is communicated with the chamber for placing the container through a pipeline, and the stirring device is used for stirring the materials in the container; and the driving device is used for driving the machine shell to act so as to drive the heated and melted materials in the container to infiltrate the inner side wall of the container.
When the vacuum stirring and refining system works, materials with various specific mass ratios are filled into the container, for example, the amount of the materials filled into the container is not more than three quarters of the volume of a chamber of the container, the container is vacuumized by the vacuum pump to provide a vacuum environment, the container is heated by the heating element to melt the materials in the container, and the materials in the container are stirred by the stirring device to uniformly mix various materials. The driving device can drive the machine shell to act, the material in a melting state in the container infiltrates the inner side wall of the container when the machine shell acts, the material attached to the inner side wall of the container is fully mixed with other materials when the material in the melting state infiltrates the inner side wall of the container, the deviation of the mass proportion of each material in the finally obtained mixed product and the preset mass proportion is small, and the qualified rate of the mixed product is high.
In one embodiment, the driving device comprises a rotating mechanism and a gradient adjusting mechanism; the inclination adjusting mechanism is arranged on the rotating mechanism, the rotating mechanism is used for driving the inclination adjusting mechanism to rotate, the machine shell is arranged on the inclination adjusting mechanism, and the inclination adjusting mechanism is used for adjusting the inclination of the bottom wall surface of the machine shell relative to the horizontal plane; the inclination adjusting mechanism comprises a bottom plate, an elastic piece, a supporting plate and a jacking mechanism; the supporting plate is connected with the bottom plate through the elastic piece; the jacking mechanism is used for jacking one side of the supporting plate to adjust the inclination of the supporting plate relative to the horizontal plane, and the jacking part of the jacking mechanism and the jacking part of the supporting plate are in sliding contact fit with the supporting plate.
In one embodiment, the pressing mechanism includes a pressing rod for pressing one side of the supporting plate to adjust an inclination of the supporting plate relative to a horizontal plane, the bottom plate is disposed on the rotating mechanism, and the housing is disposed on the supporting plate.
In one embodiment, the driving device comprises a rotating mechanism and a gradient adjusting mechanism; the rotating mechanism is arranged on the inclination adjusting mechanism, the casing is connected with the rotating mechanism, the rotating mechanism is used for driving the casing to rotate, and the inclination adjusting mechanism is used for adjusting the inclination of the bottom wall surface of the rotating mechanism and the bottom wall surface of the casing relative to the horizontal plane.
In one embodiment, the rotating mechanism is disposed between the casing and the supporting plate of the inclination adjusting mechanism, and the rotating mechanism includes a rotating motor, and a rotating shaft of the rotating motor drives the casing to rotate; or the rotating mechanism and the casing are both rotatably arranged on the supporting plate of the inclination adjusting mechanism, the rotating mechanism comprises a rotating motor and a first gear connected with an output shaft of the rotating motor, and a second gear meshed with the first gear is arranged on the outer side wall of the casing.
In one embodiment, the inclination adjusting mechanism comprises a lifting mechanism and a supporting plate, the lifting mechanism is located below the supporting plate, the lifting mechanism is used for driving one side of the supporting plate to lift or fall so as to adjust the inclination of the supporting plate relative to the horizontal plane, and the rotating mechanism and the machine shell are both arranged on the supporting plate;
or, the inclination adjusting mechanism comprises a bottom plate, an elastic part, a supporting plate and a jacking mechanism, the supporting plate is connected with the bottom plate through the elastic part, the jacking mechanism comprises a jacking rod, the jacking rod is used for jacking one side of the supporting plate to adjust the inclination of the supporting plate relative to the horizontal plane, and the rotating mechanism and the casing are both arranged on the supporting plate.
In one embodiment, the driving device includes a plurality of lifting mechanisms, the lifting mechanisms are circumferentially arranged around the periphery of the bottom of the machine shell at intervals, and the lifting mechanisms are used for driving the bottom of the machine shell to lift or fall.
In one embodiment, the driving device includes a bottom plate, an elastic member, a supporting plate, and a pressing mechanism, the supporting plate is connected to the bottom plate through the elastic member, the pressing mechanism includes a movable base, a lifting member, and a pressing rod, the movable base moves around the circumferential direction of the casing, the lifting member is disposed on the movable base, the pressing rod is disposed on the lifting member, the lifting member is configured to drive the pressing rod to move up and down to press one side of the supporting plate so as to adjust the inclination of the supporting plate relative to the horizontal plane, and the casing is disposed on the supporting plate.
In one embodiment, the inclination is 5 ° to 50 °.
In one embodiment, the chamber comprises a cavity body provided with a mouth part and a sealing cover which is arranged at the mouth part in an openable way, and the pipeline and the stirring device are fixed on the sealing cover; agitating unit includes agitator motor and stirring rake, the agitator motor drive the stirring rake rotates, agitator motor's pivot is run through sealed lid, agitator motor's pivot with the stirring rake links to each other, the stirring rake stretches into in the container.
In one embodiment, the vacuum stirring and refining system further comprises a cooling member for cooling the container, wherein the cooling member is arranged in the casing and is positioned between the sealing cover and the heating member.
In one embodiment, the housing is provided with a viewing port.
In one embodiment, a fixing member for fixing the container is provided in the chamber.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of this application, are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification.
In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings needed to be used in the description of the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.
Fig. 1 is a diagram of an operating state of a vacuum stirring and refining system according to a first embodiment of the present invention;
FIG. 2 is another diagram of the vacuum stirring and refining system according to the first embodiment of the present invention;
FIG. 3 is a diagram illustrating an operation state of a vacuum stirring and refining system according to a second embodiment of the present invention;
FIG. 4 is another diagram of the vacuum stirring and refining system according to the second embodiment of the present invention;
FIG. 5 is a diagram illustrating an operation state of a vacuum stirring and refining system according to a third embodiment of the present invention;
FIG. 6 is another state diagram of the vacuum blending and refining system according to the third embodiment of the present invention;
fig. 7 is a diagram illustrating an operation state of a vacuum stirring and refining system according to a fourth embodiment of the present invention;
FIG. 8 is another state diagram of the vacuum blending and refining system according to the fourth embodiment of the present invention;
fig. 9 is a diagram illustrating an operation state of a vacuum stirring and refining system according to a fifth embodiment of the present invention;
fig. 10 is another operation state diagram of the vacuum stirring refining system according to the fifth embodiment of the present invention;
fig. 11 is a further operational state diagram of a vacuum blending and refining system according to a fifth embodiment of the present invention;
fig. 12 is a diagram illustrating an operation state of a vacuum stirring and refining system according to a sixth embodiment of the present invention;
fig. 13 is another operation state diagram of the vacuum stirring and refining system according to the sixth embodiment of the present invention.
10. A container; 12. a chamber; 121. a cavity; 122. a sealing cover; 20. a heating member; 30. a housing; 31. a window; 40. a vacuum pump; 41. a pipeline; 50. a stirring device; 51. a stirring motor; 52. a stirring paddle; 60. a drive device; 61. a rotating mechanism; 62. an inclination adjusting mechanism; 621. a lifting mechanism; 622. a support plate; 623. a base plate; 624. an elastic member; 625. a jacking mechanism; 6251. a top pressure rod; 6252. rotating the ball; 6253. a movable seat; 6254. a guide rail; 70. and (7) an insulating layer.
Detailed Description
In order to make the above objects, features and advantages of the present invention more comprehensible, embodiments of the present invention are described in detail below with reference to the accompanying drawings. In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention. The present invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein, as those skilled in the art will be able to make similar modifications without departing from the spirit and scope of the present invention.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", "axial", "radial", "circumferential", and the like, indicate the orientation or positional relationship based on the orientation or positional relationship shown in the drawings, and are only for convenience of description and simplicity of description, and do not indicate or imply that the device or element referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include at least one such feature. In the description of the present invention, "a plurality" means at least two, e.g., two, three, etc., unless specifically limited otherwise.
In the present invention, unless otherwise expressly stated or limited, the terms "mounted," "connected," and "fixed" are to be construed broadly and may, for example, be fixedly connected, detachably connected, or integrally formed; can be mechanically or electrically connected; they may be directly connected or indirectly connected through intervening media, or they may be connected internally or in any other suitable relationship, unless expressly stated otherwise. The specific meaning of the above terms in the present invention can be understood according to specific situations by those skilled in the art.
In the present application, unless expressly stated or limited otherwise, the first feature may be directly on or directly under the second feature or indirectly via intermediate members. Also, a first feature "on," "over," and "above" a second feature may be directly or diagonally above the second feature, or may simply indicate that the first feature is at a higher level than the second feature. A first feature being "under," "below," and "beneath" a second feature may be directly under or obliquely under the first feature, or may simply mean that the first feature is at a lesser elevation than the second feature.
It will be understood that when an element is referred to as being "secured to" or "disposed on" another element, it can be directly on the other element or intervening elements may also be present. When an element is referred to as being "connected" to another element, it can be directly connected to the other element or intervening elements may also be present. The terms "vertical," "horizontal," "upper," "lower," "left," "right," and the like as used herein are for illustrative purposes only and do not denote a unique embodiment.
Generally, in the process of heating and mixing materials in a conventional vacuum stirring and refining system, due to different melting points of the materials, the material with a lower melting point is melted and located at the bottom of the crucible during the heating process, and is also sublimated and attached to the upper side wall of the crucible, wherein the upper side wall refers to the side wall part close to the mouth part. The material adhered to the upper side wall is not mixed with other molten materials because the material does not contact other materials, after the cooling step is carried out, the uniformly mixed material in the crucible is cooled to become solid, and the material adhered to the upper side wall of the crucible is also cooled to become solid. On the one hand, the material of misce bene in the crucible leads to each material quality of final mixed product to account for than to have great deviation with preset quality because of lacking the adnexed material of upper portion lateral wall department, and on the other hand, when taking out the material in the crucible, can inevitably take out the adnexed material on the lateral wall of upper portion jointly, because adnexed material quality accounts for than to have great deviation with preset quality on the lateral wall, lead to the material of whole mixed product inhomogeneous, and present product, especially among the organic electroluminescent device, require extremely high to the mixed material, the adnexed material of crucible upper portion lateral wall can lead to the material qualification rate after the mixture to hang down.
Referring to fig. 1 and 2, fig. 1 shows one of the operation state diagrams of the vacuum stirring and refining system in the first embodiment of the present invention, and fig. 2 shows another operation state diagram of the vacuum stirring and refining system in the first embodiment of the present invention. An embodiment of the utility model provides a vacuum stirring refining system, vacuum stirring refining system includes: a vessel 10, a heating member 20, a housing 30, a vacuum pump 40, a stirring device 50, and a driving device 60. The container 10 is used for holding materials. The heating member 20 is used to heat the container 10. The container 10 and the heating member 20 are installed in the cabinet 30. The vacuum pump 40 communicates with the chamber 12 of the vessel 10 via a conduit 41. The stirring device 50 is used for stirring the materials in the container 10. The driving device 60 is used for driving the machine shell 30 to act so that the heated and melted material in the container 10 can infiltrate the inner side wall of the container 10.
In the vacuum stirring and refining system, during operation, a plurality of materials with specific mass ratio are filled into the container 10, for example, the amount of the materials filled into the container 10 is not more than three-fourths of the volume of the chamber 12 of the container 10, the container 10 is vacuumized by the vacuum pump 40 to provide a vacuum environment, the container 10 is heated by the heating element 20 to melt the materials in the container 10, and the materials in the container 10 are stirred by the stirring device 50 to uniformly mix the materials. The driving device 60 can drive the machine shell 30 to move, when the machine shell 30 moves, the melted material in the container 10 infiltrates the inner side wall of the container 10, when the melted material infiltrates the inner side wall of the container 10, the material attached to the inner side wall of the container 10 is fully mixed with other materials, so that the deviation of the mass proportion of each material in the finally obtained mixed product to the preset mass proportion is small, and the qualified rate of the mixed product is high.
In this embodiment, the material is an organic small molecule material. For example, the difference in melting points between the various materials does not exceed 30 ℃. Further, the difference of melting points among various materials is not more than 10 ℃. Too large a difference in melting point between the various materials may result in sublimation of the materials having a lower melting point, thereby affecting the quality ratio of the blended product.
Referring to fig. 1 and fig. 2, further, the driving device 60 includes a rotating mechanism 61 and an inclination adjusting mechanism 62. The inclination adjusting mechanism 62 is mounted on the rotating mechanism 61. The rotating mechanism 61 is configured to drive the inclination adjusting mechanism 62 to rotate, the housing 30 is mounted on the inclination adjusting mechanism 62, and the inclination adjusting mechanism 62 is configured to adjust an inclination of a bottom wall surface of the housing 30 with respect to a horizontal plane. Specifically, the tilt adjusting mechanism 62 includes a bottom plate 623, an elastic member 624, a supporting plate 622, and a pressing mechanism 625. The support plate 622 is connected to the base plate 623 through the elastic member 624. The pressing mechanism 625 is used for pressing one side of the supporting plate 622 to adjust the inclination of the supporting plate 622 relative to the horizontal plane, and the pressing portion of the pressing mechanism 625 and the supporting plate 622 is in sliding contact with the supporting plate 622. Thus, the rotating mechanism 61 drives the supporting plate 622 to rotate, and the supporting plate 622 drives the bottom plate 623 to rotate. When the bottom plate 623 rotates, the bottom plate 623 slides relative to the pressing mechanism 625. The pressing portion of the pressing mechanism 625 and the supporting plate 622 is in sliding contact with and matches with the supporting plate 622, and the pressing mechanism 625 may be specifically disposed on the ground, a workbench, or the like, and does not rotate with the bottom plate 623 and the casing 30.
Further, the pressing mechanism 625 includes a pressing rod 6251. The pressing rod 6251 is used for pressing one side of the supporting plate 622 to adjust the inclination of the supporting plate 622 with respect to the horizontal plane. The bottom plate 623 is disposed on the rotating mechanism 61, and the casing 30 is disposed on the supporting plate 622. Specifically, when the pressing rod 6251 abuts against the upper portion of the supporting plate 622, and the supporting plate 622 is required to be inclined with respect to the horizontal plane, the pressing rod 6251 is moved downward to move one side of the supporting plate 622 downward, and the pressing rod 6251 moves in the opposite direction to release the supporting plate 622, so that the supporting plate can be restored to the original shape under the action of the elastic element 624; when the pressing rod 6251 abuts against the lower portion of the supporting plate 622, when the supporting plate 622 is required to be inclined relative to the horizontal plane, the pressing rod 6251 is moved upward so that one side of the supporting plate 622 moves upward, and the pressing rod 6251 moves in the opposite direction to release the supporting plate 622, so that the supporting plate can be restored to the original shape under the action of the elastic element 624.
Furthermore, the contact part of the top pressure rod 6251 and the supporting plate 622 is a smooth surface or is provided with a rotating ball 6252, so that the relative movement effect between the top pressure rod 6251 and the supporting plate 622 is smoother in the rotating process of the inclination adjusting mechanism 62 of the rotating mechanism 61.
Referring to fig. 3 and 4, fig. 3 is a diagram illustrating an operating state of a vacuum stirring and refining system according to a second embodiment of the present invention; fig. 4 illustrates another operation state diagram of the vacuum stirring and refining system according to the second embodiment of the present invention. The vacuum stirring and refining system illustrated in fig. 3 and 4 is different from the vacuum stirring and refining system illustrated in fig. 1 and 2 mainly in the arrangement manner of the rotating mechanism 61 and the inclination adjusting mechanism 62. In the vacuum stirring and refining system illustrated in fig. 3 and 4, the driving device 60 includes a rotating mechanism 61 and an inclination adjusting mechanism 62. The rotating mechanism 61 is mounted on the inclination adjusting mechanism 62. The housing 30 is connected to the rotating mechanism 61, and the rotating mechanism 61 is used for driving the housing 30 to rotate. The inclination adjusting mechanism 62 is used for adjusting the inclination of the bottom wall surface of the rotating mechanism 61 and the bottom wall surface of the housing 30 relative to the horizontal plane.
Thus, when the material adhered to the inner side wall of the container 10 needs to be wetted, the inclination adjusting mechanism 62 adjusts the bottom wall surface of the housing 30 from a horizontal state to an inclined state, and the bottom wall of the container 10 installed in the housing 30 is correspondingly and synchronously adjusted from the horizontal state to the inclined state, specifically, for example, the bottom wall of the container 10 deflects by 5 ° to 15 ° relative to the horizontal plane. Thus, when the rotating mechanism 61 drives the casing 30 to rotate, the casing 30 synchronously rotates the obliquely arranged container 10 correspondingly, and when the obliquely arranged container 10 rotates, the material in the molten state in the container 10 can infiltrate into the material on the inner side wall of the container 10 and is fully and uniformly mixed with the material.
Referring to fig. 3 and 4, in one embodiment, the rotating mechanism 61 is disposed between the housing 30 and the supporting plate 622 of the tilt adjusting mechanism 62. The rotating mechanism 61 includes a rotating motor, and a rotating shaft of the rotating motor drives the casing 30 to rotate. Thus, when the rotating motor rotates, the rotating shaft of the rotating motor drives the housing 30 to rotate.
Referring to fig. 5 and 6, fig. 5 is a diagram illustrating an operating state of a vacuum stirring and refining system according to a third embodiment of the present invention; fig. 6 illustrates another operation state diagram of the vacuum stirring and refining system according to the third embodiment of the present invention. The vacuum stirring and refining system illustrated in fig. 5 and 6 is different from the vacuum stirring and refining system illustrated in fig. 3 and 4 mainly in that the rotating mechanism 61 is arranged at a different position, the rotating mechanism 61 illustrated in fig. 3 and 4 directly drives the casing 30 to rotate, and the rotating mechanism 61 illustrated in fig. 5 and 6 drives the casing 30 to rotate in a gear manner. In another embodiment, the rotating mechanism 61 and the housing 30 are both rotatably disposed on the supporting plate 622 of the tilt adjusting mechanism 62. The rotating mechanism 61 comprises a rotating motor and a first gear connected with an output shaft of the rotating motor, and a second gear meshed with the first gear is arranged on the outer side wall of the casing 30. Therefore, when the rotating motor rotates, the rotating motor drives the first gear to rotate, the first gear correspondingly drives the second gear to rotate, and the rotation of the driving shell 30 can also be realized.
Referring to fig. 3 and 4, the tilt adjusting mechanism 62 further includes a lifting mechanism 621 and a supporting plate 622. The lifting mechanism 621 is located below the supporting plate 622, the lifting mechanism 621 is used for driving one side of the supporting plate 622 to lift or fall so as to adjust the inclination of the supporting plate 622 relative to the horizontal plane, and the rotating mechanism 61 and the casing 30 are both disposed on the supporting plate 622.
Specifically, the inclination adjustment mechanism 62 further includes a bottom plate 623 disposed below the lift mechanism 621. In this manner, the bottom plate 623 is placed on a flat ground or table, depending on the actual situation. Of course, as a possible solution, the bottom plate 623 and the supporting plate 622 can be omitted, and the inclination of the casing 30 and the rotating mechanism 61 can be changed directly by the lifting mechanism 621.
Referring to fig. 7 and 8, fig. 7 is a diagram illustrating a working state of a vacuum stirring and refining system according to a fourth embodiment of the present invention; fig. 8 illustrates another operation state diagram of the vacuum stirring and refining system according to the fourth embodiment of the present invention. The main difference between the vacuum stirring and refining system illustrated in fig. 7 and 8 and the vacuum stirring and refining system illustrated in fig. 3 and 4 is the difference between the inclination adjusting mechanism 62. In the vacuum stirring and refining system illustrated in fig. 7 and 8, the inclination adjusting mechanism 62 includes a bottom plate 623, an elastic member 624, a supporting plate 622, and a pressing mechanism 625. The supporting plate 622 is connected to the bottom plate 623 through the elastic member 624, and the pressing mechanism 625 includes a pressing rod 6251. The pressing rod 6251 is used for pressing one side of the supporting plate 622 to adjust the inclination of the supporting plate 622 with respect to the horizontal plane. The rotating mechanism 61 and the housing 30 are both disposed on the supporting plate 622. Specifically, when the pressing rod 6251 abuts against the upper portion of the supporting plate 622, and the supporting plate 622 is required to be inclined with respect to the horizontal plane, the pressing rod 6251 is moved downward to move one side of the supporting plate 622 downward, and the pressing rod 6251 moves in the opposite direction to release the supporting plate 622, so that the supporting plate can be restored to the original shape under the action of the elastic element 624; when the pressing rod 6251 abuts against the lower portion of the supporting plate 622, when the supporting plate 622 is required to be inclined relative to the horizontal plane, the pressing rod 6251 is moved upward so that one side of the supporting plate 622 moves upward, and the pressing rod 6251 moves in the opposite direction to release the supporting plate 622, so that the supporting plate can be restored to the original shape under the action of the elastic element 624.
Further, the elastic member 624 may be a spring, an elastic block, or the like, which is not limited herein.
Referring to fig. 9 to 11, fig. 9 is a diagram illustrating an operating state of a vacuum stirring and refining system according to a fifth embodiment of the present invention; fig. 10 illustrates another operation state diagram of the vacuum stirring and refining system according to the fifth embodiment of the present invention; fig. 11 illustrates a further operation of the vacuum stirring and refining system according to the fifth embodiment of the present invention. In another embodiment, the driving device 60 includes a plurality of lifting mechanisms 621. The lifting mechanism 621 is circumferentially arranged around the bottom periphery of the casing 30 at intervals, and the lifting mechanism 621 is used for driving the bottom of the casing 30 to lift or fall. Specifically, the driving device 60 further includes a supporting plate 622 and a bottom plate 623, the plurality of lifting mechanisms 621 are disposed on the bottom plate 623, and the supporting plate 622 is disposed between the lifting mechanisms 621 and the housing 30. When the lifting mechanism 621 lifts or lowers one side of the bottom of the casing 30, the bottom wall of the casing 30 is correspondingly inclined, so that the material in the molten state in the container 10 infiltrates the inner side wall of the container 10, and the material adhered to the inner side wall of the container 10 is fully mixed with other materials when the material in the molten state infiltrates the inner side wall of the container 10.
Further, four lifting mechanisms 621 are provided, and the four lifting mechanisms 621 are disposed at equal intervals in the circumferential direction around the bottom of the housing 30. When one of the lifting mechanisms 621 is lifted, the other lifting mechanism 621 provided opposite to the one lifting mechanism 621 is lowered. Of course, the number of the lifting mechanisms 621 may be other, and is not limited herein.
Referring to fig. 12 and 13, fig. 12 is a diagram illustrating an operation state of a vacuum stirring and refining system according to a sixth embodiment of the present invention; fig. 13 illustrates another operation state diagram of the vacuum stirring and refining system according to the sixth embodiment of the present invention. In another embodiment, the driving device 60 includes a bottom plate 623, an elastic member 624, a supporting plate 622, and a pressing mechanism 625. The support plate 622 is connected to the base plate 623 through the elastic member 624. The pressing mechanism 625 includes a movable base 6253, a lifting member, and a pressing rod 6251. The movable base 6253 moves around the circumferential direction of the housing 30, the lifting member is disposed on the movable base 6253, the jacking rod 6251 is disposed on the lifting member, the lifting member is used for driving the jacking rod 6251 to move up and down to jack one side of the supporting plate 622 so as to adjust the inclination of the supporting plate 622 relative to the horizontal plane, and the housing 30 is disposed on the supporting plate 622. Specifically, when the pressing rod 6251 abuts against the upper portion of the supporting plate 622, when the supporting plate 622 is required to be inclined with respect to the horizontal plane, the pressing rod 6251 is moved downwards by the lifting member to move one side of the supporting plate 622 downwards, and the supporting plate 622 is restored under the action of the elastic member 624 when the lifting member drives the pressing rod 6251 to move reversely to release the supporting plate 622; when the pressing rod 6251 abuts against the lower portion of the supporting plate 622, when the supporting plate 622 is required to be inclined relative to the horizontal plane, the lifting member moves the pressing rod 6251 upwards to move one side of the supporting plate 622 upwards, and the pressing rod 6251 moves reversely to release the supporting plate 622, so that the supporting plate can be restored under the action of the elastic member 624.
Further, a guide rail 6254 is provided around the outer periphery of the housing 30, and the movable base 6253 moves along the guide rail 6254.
In one embodiment, the inclination in this example is greater than 0 ° and less than 90 °. Preferably, the inclination is 0 ° to 60 °. Specifically, the inclination in this example is 5 ° to 50 °.
Referring again to fig. 1 and 2, in one embodiment, the container 10 is embodied as a crucible. Wherein, the upper part of the crucible is open, thereby being convenient for installing materials.
In one embodiment, the chamber 12 includes a cavity 121 provided with a mouth and a sealing cover 122 openably provided to the mouth. The pipe 41 and the stirring device 50 are fixed on the sealing cover 122. Agitating unit 50 includes agitator motor 51 and stirring rake 52, agitator motor 51 drive stirring rake 52 rotates, agitator motor 51's pivot is run through sealed lid 122, agitator motor 51's pivot with stirring rake 52 links to each other, stirring rake 52 stretches into in the container 10. Specifically, the rotation shaft of the stirring motor 51 is tightly fitted with the sealing cover 122, thereby ensuring sealability and providing a good vacuum environment for the vacuum chamber 12.
Further, the vacuum stirring and refining system also comprises a cooling part for cooling the container 10. The cooling member is disposed in the cabinet 30 between the sealing cover 122 and the heating member 20. In this way, when cooling operation of the container 10 is required, the cooling member operates, so that rapid reduction of the temperature of the container 10 can be achieved.
Further, referring to fig. 1 and fig. 2, the housing 30 is provided with a viewing port. So, the viewing aperture is used for observing material state and crucible inclination in the crucible, prevents that the material from spilling over the crucible. The position of the viewing port on the housing 30 may be arbitrarily set, and for example, the viewing port may be a top wall of the housing 30 or a side wall of the housing 30, as long as the state of the material in the crucible and the inclination angle of the crucible can be observed through the viewing port.
Further, a fixing member for fixing the container 10 is provided in the chamber 12. In this manner, the securing member secures the container 10 within the chamber 12 and prevents the container 10 from wobbling when tilted.
Further, the vacuum stirring and refining system also comprises an insulating layer 70. The insulation layer 70 wraps the outer side wall of the chamber 12. The heat-insulating layer 70 plays a role in heat insulation of the chamber 12, so that energy loss in the heating process of the heating element 20 is avoided, and the material in the container 10 is melted and uniformly mixed.
In one embodiment, referring to fig. 1 and fig. 2 again, a refining method using the vacuum stirring refining system according to any of the above embodiments includes the following steps:
providing materials with a preset mass ratio, and filling the materials into a container 10;
wherein the container 10 is filled with a quantity of material not exceeding three quarters of the volume of the chamber 12 of the container 10.
Vacuumizing the container 10 to provide a vacuum environment, and heating the container 10 by the heating element 20 to enable the materials in the container 10 to be in a molten state;
stirring the materials in the container 10 to uniformly mix the materials;
and driving the machine shell 30 to act, wherein the machine shell 30 acts to enable the material in the molten state in the container 10 to infiltrate the inner side wall of the container 10.
When the material in the molten state wets the inner side wall of the container 10, the material adhered to the inner side wall of the container 10 is fully mixed with other materials.
In the refining method of the vacuum stirring refining system, the material in the melting state in the container 10 infiltrates the inner side wall of the container 10, and the material attached to the inner side wall of the container 10 is fully mixed with other materials when the material in the melting state infiltrates the inner side wall of the container 10, so that the deviation of the mass ratio of each material in the finally obtained mixed product to the preset mass ratio is small, and the qualified rate of the mixed product is high.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only represent some embodiments of the present invention, and the description thereof is specific and detailed, but not to be construed as limiting the scope of the present invention. It should be noted that, for those skilled in the art, without departing from the spirit of the present invention, several variations and modifications can be made, which are within the scope of the present invention. Therefore, the protection scope of the present invention should be subject to the appended claims.

Claims (13)

1. A vacuum blending system, comprising:
a container for holding a material;
the chamber is a vacuum chamber and is used for placing a container;
a heating member for performing a heating process to the chamber;
the chamber and the heating element are arranged in the machine shell;
the vacuum pump is communicated with the chamber for placing the container through a pipeline, and the stirring device is used for stirring the materials in the container;
and the driving device is used for driving the machine shell to act so as to drive the heated and melted materials in the container to infiltrate the inner side wall of the container.
2. The vacuum mixing refining system of claim 1, wherein the driving device comprises a rotating mechanism and a tilt adjusting mechanism; the inclination adjusting mechanism is arranged on the rotating mechanism, the rotating mechanism is used for driving the inclination adjusting mechanism to rotate, the machine shell is arranged on the inclination adjusting mechanism, and the inclination adjusting mechanism is used for adjusting the inclination of the bottom wall surface of the machine shell relative to the horizontal plane; the inclination adjusting mechanism comprises a bottom plate, an elastic piece, a supporting plate and a jacking mechanism; the supporting plate is connected with the bottom plate through the elastic piece; the jacking mechanism is used for jacking one side of the supporting plate to adjust the inclination of the supporting plate relative to the horizontal plane, and the jacking part of the jacking mechanism and the jacking part of the supporting plate are in sliding contact fit with the supporting plate.
3. The vacuum mixing refining system of claim 2, wherein the pressing mechanism comprises a pressing rod for pressing one side of the supporting plate to adjust the inclination of the supporting plate relative to the horizontal plane, the bottom plate is disposed on the rotating mechanism, and the casing is disposed on the supporting plate.
4. The vacuum mixing refining system of claim 1, wherein the driving device comprises a rotating mechanism and a tilt adjusting mechanism; the rotating mechanism is arranged on the inclination adjusting mechanism, the casing is connected with the rotating mechanism, the rotating mechanism is used for driving the casing to rotate, and the inclination adjusting mechanism is used for adjusting the inclination of the bottom wall surface of the rotating mechanism and the bottom wall surface of the casing relative to the horizontal plane.
5. The vacuum mixing and refining system according to claim 4, wherein the rotating mechanism is disposed between the casing and the supporting plate of the inclination adjusting mechanism, the rotating mechanism comprises a rotating motor, and a rotating shaft of the rotating motor drives the casing to rotate; or the rotating mechanism and the casing are both rotatably arranged on the supporting plate of the inclination adjusting mechanism, the rotating mechanism comprises a rotating motor and a first gear connected with an output shaft of the rotating motor, and a second gear meshed with the first gear is arranged on the outer side wall of the casing.
6. The vacuum mixing and refining system according to claim 4, wherein the inclination adjusting mechanism comprises a lifting mechanism and a supporting plate, the lifting mechanism is located below the supporting plate, the lifting mechanism is used for driving one side of the supporting plate to lift or fall so as to adjust the inclination of the supporting plate relative to the horizontal plane, and the rotating mechanism and the machine shell are both arranged on the supporting plate;
or, the inclination adjusting mechanism comprises a bottom plate, an elastic part, a supporting plate and a jacking mechanism, the supporting plate is connected with the bottom plate through the elastic part, the jacking mechanism comprises a jacking rod, the jacking rod is used for jacking one side of the supporting plate to adjust the inclination of the supporting plate relative to the horizontal plane, and the rotating mechanism and the casing are both arranged on the supporting plate.
7. The vacuum mixing and refining system of claim 1, wherein the driving device comprises a plurality of lifting mechanisms circumferentially spaced around the bottom periphery of the casing, the lifting mechanisms configured to drive the bottom of the casing up or down.
8. The vacuum stirring refining system of claim 1, wherein the driving device comprises a bottom plate, an elastic member, a supporting plate and a pressing mechanism, the supporting plate is connected to the bottom plate through the elastic member, the pressing mechanism comprises a movable base, a lifting member and a pressing rod, the movable base moves around the circumferential direction of the casing, the lifting member is arranged on the movable base, the pressing rod is arranged on the lifting member, the lifting member is used for driving the pressing rod to move up and down to press one side of the supporting plate so as to adjust the inclination of the supporting plate relative to the horizontal plane, and the casing is arranged on the supporting plate.
9. A vacuum stirred blending system according to claim 2, 4, 5 or 8, wherein said inclination is 5 ° to 50 °.
10. The vacuum stirring refining system of any one of claims 1 to 8, wherein the chamber comprises a cavity with a mouth and a sealing cover openably disposed on the mouth, and the pipe and the stirring device are both fixed on the sealing cover; agitating unit includes agitator motor and stirring rake, the agitator motor drive the stirring rake rotates, agitator motor's pivot is run through sealed lid, agitator motor's pivot with the stirring rake links to each other, the stirring rake stretches into in the container.
11. The vacuum stirred blending system of claim 10, further comprising a cooling member for cooling the container, the cooling member being disposed within the enclosure between the sealing lid and the heating member.
12. A vacuum mixing and refining system as claimed in any one of claims 1 to 8, wherein the housing is provided with a viewing port.
13. A vacuum stirring refining system according to any one of claims 1 to 8, wherein: a fixing member for fixing the container is provided in the chamber.
CN202020591253.1U 2020-04-20 2020-04-20 Vacuum stirring refining system Active CN212167228U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202020591253.1U CN212167228U (en) 2020-04-20 2020-04-20 Vacuum stirring refining system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202020591253.1U CN212167228U (en) 2020-04-20 2020-04-20 Vacuum stirring refining system

Publications (1)

Publication Number Publication Date
CN212167228U true CN212167228U (en) 2020-12-18

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Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Link
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