CN212039080U

CN212039080U - Reducing agent preparation fractionating device

Info

Publication number: CN212039080U
Application number: CN202020586919.4U
Authority: CN
Inventors: 陈雯; 赵宗林; 陈健
Original assignee: Yunnan Quankai Metallurgical Materials Co ltd; Kunming Ligong Jingcheng Science & Technology Co ltd
Current assignee: Yunnan Quankai Metallurgical Materials Co ltd; Kunming Ligong Jingcheng Science & Technology Co ltd
Priority date: 2020-04-20
Filing date: 2020-04-20
Publication date: 2020-12-01
Anticipated expiration: 2030-04-20

Abstract

The utility model discloses a reducing agent preparation fractionating device, including unable adjustment base, one side at unable adjustment base top is provided with the heating seat, the center of heating seat is provided with the retort, the center and the week side of heating seat bottom all are provided with the heating solenoid who corresponds with the retort, the fractionating column is installed at the top of retort, the one end that the retort was kept away from to the fractionating column is installed and is customized condenser pipe, first vacuum drainage tube, second vacuum drainage tube and third vacuum drainage tube are installed respectively to the bottom of customization condenser pipe, the center at unable adjustment base top is provided with the receiving tank corresponding with first vacuum drainage tube, second vacuum drainage tube and third vacuum drainage tube. The utility model discloses in, this reductant preparation fractionating device not only design has heating mechanism, and it has the water conservancy diversion mechanism of fractionating still to design, through the condenser pipe of design customization, can improve condensation efficiency greatly for fractional distillation volume and fractional distillation efficiency are worth wideling popularize.

Description

Reducing agent preparation fractionating device

Technical Field

The utility model relates to a fractionation equipment technical field especially relates to a reductant preparation fractionation device.

Background

Fractional distillation is a method of separating several mixtures of different boiling points; heating a certain mixture, and cooling and separating the mixture into relatively pure single substances according to different boiling points of each component in the mixture, wherein no new substance is generated in the process, only the original substance is separated, the physical change is realized, the fractionation is actually repeated distillation, and the method is more suitable for separating and purifying liquid organic mixtures with slightly different boiling points, such as the fractionation of coal tar; fractionation of petroleum, when the boiling points of the materials are very close, about 20 degrees apart, makes it impossible to use simple distillation, but instead fractionation, where a small column of the fractionation column provides a large surface area for condensation of the vapor, as in distillation, i.e., a means of separating a mixture of several volatile components of different boiling points; the mixture is first distilled at the lowest boiling point until the temperature of the vapor rises, indicating that the next higher boiling component in the mixture begins to distill, and then this group is collected separately, fractionation being an important method for separating and purifying the less boiling components of the liquid organic mixture, petroleum being separated by fractional distillation.

A fractionating device is needed to be used for preparing a liquid reducing agent, but the structural design of the existing device has certain defects, the existing fractionating device is poor in fractionating effect, the fractionating amount is small each time, the fractionating progress is influenced greatly, a large amount of time is needed when the reducing agent is fractionated, time and labor are wasted, and therefore a novel reducing agent preparing and fractionating device is provided.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the defects existing in the prior art and providing a reducing agent preparation fractionating device.

In order to achieve the above purpose, the utility model adopts the following technical scheme: a reducing agent preparation fractionating device comprises a fixed base, a heating seat is arranged on one side of the top of the fixed base, a distillation flask is arranged at the center of the heating seat, heating electromagnetic coils corresponding to the distillation flask are arranged at the center and the peripheral side of the bottom of the heating seat, an electric cabinet is arranged on one side of the heating seat, a fractionating column is arranged on the top of the distillation flask, a customized condensing pipe is arranged at one end of the fractionating column far away from the distillation flask, a fixed mount is fixedly connected with one end of the top of the fixed base far away from the heating seat, a water inlet and a water outlet are respectively arranged on two sides of the outer wall of the customized condensation pipe, the bottom of the customized condensation pipe is respectively provided with a first vacuum drainage pipe, a second vacuum drainage pipe and a third vacuum drainage pipe, and a receiving groove corresponding to the first vacuum drainage tube, the second vacuum drainage tube and the third vacuum drainage tube is formed in the center of the top of the fixed base.

As a further description of the above technical solution:

one side fixedly connected with of retort outer wall annotates the liquid pipe, just the center of heating seat bottom is provided with the asbestos gauge that corresponds with the retort.

As a further description of the above technical solution:

the center of the top of the fractionating column is provided with a thermometer corresponding to the distillation flask.

As a further description of the above technical solution:

the top fixedly connected with of mount outer wall one side and the corresponding holding ring of customization condenser pipe, just the one end that the fractionation post was kept away from to the customization condenser pipe cup joints with the center of holding ring.

As a further description of the above technical solution:

and a plurality of flow guide holes corresponding to the first vacuum drainage tube, the second vacuum drainage tube and the third vacuum drainage tube are formed in the bottom of the customized condensation tube.

As a further description of the above technical solution:

and the top parts of the first vacuum drainage tube, the second vacuum drainage tube and the third vacuum drainage tube are provided with thread fixing rings corresponding to the customized condensation tube.

The utility model discloses following beneficial effect has: 1. the utility model provides a pair of reducing agent preparation fractionating device compares with traditional device, the device simple structure, convenient and practical through the simple mechanism of fractionating of design, can accomplish reducing agent solution's quick fractionation fast, has saved a large amount of time.

2. Compared with the traditional device, the device has the advantages that the structure and the design are greatly innovated and improved, the reducing agent preparation fractionating device is not only provided with the heating mechanism, but also provided with the fractionating and guiding mechanism, the condensing pipe customized through design can greatly improve the condensing efficiency, the fractionating amount and the fractionating efficiency are accelerated, the working efficiency is greatly improved, and the device is worthy of great popularization.

Drawings

Fig. 1 is a front view structural diagram of a fractionating apparatus for preparing a reducing agent according to the present invention;

FIG. 2 is an enlarged view of a portion of FIG. 1 at A;

fig. 3 is a partially enlarged view of B in fig. 1.

Illustration of the drawings:

1. a fixed base; 2. a heating base; 3. a distillation flask; 4. heating the electromagnetic coil; 5. an asbestos web; 6. an electric cabinet; 7. a fractionating column; 8. customizing a condensation pipe; 9. a thermometer; 10. a fixed mount; 11. a positioning ring; 12. a water inlet; 13. a water outlet; 14. a first vacuum draft tube; 15. a second vacuum draft tube; 16. a third vacuum draft tube; 17. a flow guide hole; 18. a threaded retainer ring; 19. a receiving groove.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus, should not be construed as limiting the present invention; the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance, and furthermore, unless otherwise explicitly stated or limited, the terms "mounted," "connected," and "connected" are to be construed broadly and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.

Referring to fig. 1-3, the present invention provides an embodiment: a fractionating device for preparing a reducing agent comprises a fixed base 1, wherein a heating seat 2 is arranged on one side of the top of the fixed base 1, a distillation flask 3 is arranged at the center of the heating seat 2, heating electromagnetic coils 4 corresponding to the distillation flask 3 are arranged at the center and the peripheral sides of the bottom of the heating seat 2, an electric cabinet 6 is arranged on one side of the heating seat 2, a fractionating column 7 is arranged at the top of the distillation flask 3, a customized condensation pipe 8 is arranged at one end, far away from the distillation flask 3, of the fractionating column 7, a fixed frame 10 is fixedly connected to one end, far away from the heating seat 2, of the top of the fixed base 1, a water inlet 12 and a water outlet 13 are respectively arranged on two sides of the outer wall of the customized condensation pipe 8, a first vacuum drainage pipe 14, a second vacuum drainage pipe 15 and a third vacuum drainage pipe 16 are respectively arranged at the bottom of the customized condensation, The second vacuum drainage tube 15 and the third vacuum drainage tube 16 correspond to the receiving groove 19.

One side fixedly connected with of the outer wall of retort 3 annotates the liquid pipe, and the center of heating seat 2 bottom is provided with the asbestos gauge 5 corresponding with retort 3, annotates the liquid pipe and can conveniently annotate reductant stoste to retort 3.

A thermometer 9 corresponding to the distillation flask 3 is installed at the center of the top of the fractionating column 7, and the thermometer 9 facilitates observation of the temperature in the fractionating column 7.

The top fixedly connected with of mount 10 outer wall one side and the corresponding holding ring 11 of customization condenser pipe 8, and the one end that the fractionation post 7 was kept away from to customization condenser pipe 8 cup joints the center with holding ring 11, and holding ring 11 both can play the supporting role to customization condenser pipe 8, also can play the fixed action of location to customization condenser pipe 8 simultaneously.

The customized condensation pipe 8 is provided at the bottom thereof with a plurality of guide holes 17 corresponding to the first vacuum draft tube 14, the second vacuum draft tube 15 and the third vacuum draft tube 16, and the guide holes 17 having an inverted trapezoidal shape may play a role of guiding flow, so that the cooled liquid may flow into the first vacuum draft tube 14, the second vacuum draft tube 15 and the third vacuum draft tube 16 through the guide holes 17.

The top parts of the first vacuum draft tube 14, the second vacuum draft tube 15 and the third vacuum draft tube 16 are all provided with a screw thread fixing ring 18 corresponding to the customized condensation duct 8, and the screw thread fixing ring 18 facilitates the detachment and installation of the first vacuum draft tube 14, the second vacuum draft tube 15 and the third vacuum draft tube 16.

The working principle is as follows: the utility model provides a reducing agent preparation fractionating device which is greatly improved and innovated together with the traditional device, when the reducing agent is used for preparing the fractionating device, one side of the outer wall of the distillation flask 3 is fixedly connected with a liquid injection pipe, the reducing agent stock solution can be conveniently injected into the distillation flask 3 through the liquid injection pipe, after all the fractionating pipelines are connected, the heating electromagnetic coil 4 can be controlled by the electric cabinet 6 to heat the distillation flask 3, the reducing agent stock solution in the distillation flask 3 is heated at high temperature, the solution with lower boiling point in the reducing agent can be quickly evaporated, the evaporated water vapor can enter the customized condenser pipe 8 through the fractionating column 7, the increased customized condenser pipe 8 can accelerate the cooling speed, so that the rapidly fractionated solution can be introduced into the receiving tank 19 through the first vacuum draft tube 14, the second vacuum draft tube 15 and the third vacuum draft tube 16.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications and variations can be made in the embodiments or in part of the technical features of the embodiments without departing from the spirit and the scope of the invention.

Claims

1. The utility model provides a reducing agent preparation fractionating device, includes unable adjustment base (1), its characterized in that: one side at unable adjustment base (1) top is provided with heating seat (2), the center of heating seat (2) is provided with retort (3), the center and the week side of heating seat (2) bottom all are provided with heating solenoid (4) corresponding with retort (3), one side of heating seat (2) is provided with electric cabinet (6), fractionating column (7) are installed at the top of retort (3), the one end that retort (3) were kept away from in fractionating column (7) is installed customization condenser pipe (8), one end fixedly connected with mount (10) of heating seat (2) are kept away from at the top of unable adjustment base (1), the both sides of customization condenser pipe (8) outer wall are provided with water inlet (12) and delivery port (13) respectively, first vacuum drainage tube (14) are installed respectively to the bottom of customization condenser pipe (8), A second vacuum drainage tube (15) and a third vacuum drainage tube (16), wherein a receiving groove (19) corresponding to the first vacuum drainage tube (14), the second vacuum drainage tube (15) and the third vacuum drainage tube (16) is arranged at the center of the top of the fixing base (1).

2. A reducing agent preparation fractionating apparatus according to claim 1, wherein: one side fixedly connected with of distillation flask (3) outer wall annotates the liquid pipe, just the center of heating seat (2) bottom is provided with asbestos gauge (5) corresponding with distillation flask (3).

3. A reducing agent preparation fractionating apparatus according to claim 1, wherein: a thermometer (9) corresponding to the distillation flask (3) is arranged at the center of the top of the fractionating column (7).

4. A reducing agent preparation fractionating apparatus according to claim 1, wherein: the top of the outer wall of the fixing frame (10) is fixedly connected with a positioning ring (11) corresponding to the customized condensation pipe (8), and one end, far away from the fractionating column (7), of the customized condensation pipe (8) is sleeved at the center of the positioning ring (11).

5. A reducing agent preparation fractionating apparatus according to claim 1, wherein: the bottom of the customized condensation pipe (8) is provided with a plurality of diversion holes (17) corresponding to the first vacuum drainage pipe (14), the second vacuum drainage pipe (15) and the third vacuum drainage pipe (16).

6. A reducing agent preparation fractionating apparatus according to claim 1, wherein: the tops of the first vacuum drainage tube (14), the second vacuum drainage tube (15) and the third vacuum drainage tube (16) are respectively provided with a thread fixing ring (18) corresponding to the customized condensation pipe (8).