CN212017022U - Ionic liquid purification and recovery device - Google Patents
Ionic liquid purification and recovery device Download PDFInfo
- Publication number
- CN212017022U CN212017022U CN202020207435.4U CN202020207435U CN212017022U CN 212017022 U CN212017022 U CN 212017022U CN 202020207435 U CN202020207435 U CN 202020207435U CN 212017022 U CN212017022 U CN 212017022U
- Authority
- CN
- China
- Prior art keywords
- gear
- ionic liquid
- rotating column
- condenser
- tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model belongs to the field of purification and recovery, in particular to an ionic liquid purification and recovery device, which aims at the problems of poor condensation effect and resource waste, the following scheme is proposed, the ionic liquid purification and recovery device comprises a shell and a plurality of guide pipes, wherein an ionic liquid storage tank is arranged inside the shell, the ionic liquid storage tank is connected with a preheating box, a buffer filter plate is arranged on a liquid inlet of the preheating box, a spiral liquid flow passage is arranged inside the preheating box, the ionic liquid storage tank is connected with the spiral liquid flow passage through a guide pipe, and a liquid outlet of the spiral liquid flow passage is connected with a distillation kettle through a guide pipe; the utility model discloses can improve condensation efficiency, preheat the ionic liquid before the distillation, the resource has been saved in the energy resource consumption reduction in the stills.
Description
Technical Field
The utility model relates to a purification recovery technical field especially relates to an ionic liquid purification recovery unit.
Background
Purification refers to the separation of impurities from the ionic liquid to increase its purity. Purification as an important chemical method has important roles not only in chemical research but also in chemical production.
Traditional ionic liquid purification recovery unit, condensing efficiency is not high, can not preheat before the distillation, and the energy resource consumption in the stills is too big, causes the wasting of resources, consequently needs design an ionic liquid purification recovery unit and solves the problem.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the problems that the condensation effect is not good, the energy consumption in the distillation still is too large, the resource waste is caused, and the proposed ionic liquid purification and recovery device.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
an ionic liquid purification and recovery device comprises a shell and a plurality of guide pipes, wherein an ionic liquid storage tank is arranged inside the shell, the ionic liquid storage tank is connected with a preheating box, a buffering filter plate is arranged on a liquid inlet of the preheating box, a spiral liquid flow passage is arranged inside the preheating box, the ionic liquid storage tank is connected with the spiral liquid flow passage through one guide pipe, a liquid outlet of the spiral liquid flow passage is connected with a distillation kettle through one guide pipe, the distillation kettle is connected with a condenser through one guide pipe, a condenser jacket is wrapped outside the condenser and is fixedly connected with a water tank, one end of the water tank far away from the ionic liquid storage tank is connected with the condenser jacket through one guide pipe, one end of the condenser far away from the water tank is connected with a cooler through one guide pipe, and one end of the cooler far away from the, the condenser is characterized in that one end of the condenser jacket, which is far away from the water tank, is connected with a placing box through a conduit, a fan is installed in the placing box, the placing box is connected with a water guide shell through a conduit, one side, which is far away from the placing box, of the water guide shell is connected with a preheating box, a water pump fan blade is installed in the water guide shell, the water pump fan blade is fixedly connected with a sixth rotating column, a ninth gear is welded at the top of the sixth rotating column, the ninth gear is meshed with an eighth gear, the eighth gear is connected with a fifth rotating column, a seventh gear is welded at one end, which is far away from the eighth gear, of the fifth rotating column, the seventh gear is meshed with a sixth gear, the sixth gear is connected with a fourth rotating column, a fifth gear is welded at one end, which is far away from the sixth gear, of the fourth rotating column, a fourth gear is meshed with a first rotating column, and the one end meshing that fifth gear was kept away from to the fourth gear has the third gear, the third gear connection has the third to rotate the post, just the third rotates the one end welding that the third gear was kept away from to the post and has the second gear, the second gear meshing has first gear, just first gear connection has the second to rotate the post, the fan of incasement is placed to the second rotation post fixed connection, its the one end that the fourth gear was kept away from to the first rotation post is connected with the motor.
Preferably, condenser internally mounted has the condensation spiral pipe, be equipped with the hot plate in the stills, install temperature sensor in the stills, just the stills shell is equipped with temperature controller.
Preferably, the fans are located on two sides of the guide pipe, the fans on the two sides are fixedly connected, the second rotating column drives the fan on one side to rotate, and the fan drives the fan on the other side to rotate together.
Preferably, the device also comprises a fixed box, and a motor, a first gear, a fourth gear, a fifth gear, a third gear, a sixth gear, a seventh gear, a second gear, a first rotating column, a second rotating column, a third rotating column, a fourth rotating column and a fifth rotating column are placed in the fixed box.
Preferably, the concentration sensor is connected with a first two-way valve, a first valve of the first two-way valve is connected with an ionic liquid storage tank, and a second valve is connected with an ionic liquid collection tank.
1. Because the device is provided with a shell, an ionic liquid storage tank, a guide pipe, a buffer filter plate, a preheating tank, a spiral liquid flow channel, a condenser jacket, a water tank, a motor, a first rotating column, a second rotating column, a third rotating column, a fourth rotating column, a fifth rotating column, a sixth rotating column, a first gear, a second gear, a third gear, a fourth gear, a fifth gear, a sixth gear, a seventh gear, an eighth gear, a ninth gear and a water pump fan blade, distilled ionic liquid enters the condenser, water discharged from the water tank enters the water tank jacket to perform thermal reaction, cold water is heated, the temperature of the ionic liquid is reduced, the heated cold water enters the preheating tank through the guide pipe, the ionic liquid is fully preheated in the spiral liquid flow channel, then the water guide shell starts to absorb water, a fan in the storage box blows heated cold water, the water is cooled a little, and the water enters the outer sleeve of the condenser, so that resources are saved.
2. Due to the fact that the distillation kettle, the heating plate, the temperature controller, the temperature sensor, the first two-way valve, the ionic liquid collecting tank, the cooler and the concentration sensor are arranged, after ionic liquid is purified through a series of steps, the ionic liquid which does not reach the standard can reenter the distillation kettle through the first valve of the first two-way valve to be purified for the second time through induction of the concentration sensor, and the ionic liquid which reaches the standard can enter the ionic liquid collecting tank through the second valve of the first two-way valve.
The utility model discloses can improve condensation efficiency, preheat the ionic liquid before the distillation, the resource has been saved in the energy resource consumption reduction in the stills.
Drawings
Fig. 1 is a schematic front view of an ion liquid purification and recovery device provided by the present invention;
fig. 2 is a schematic perspective view of an ionic liquid purification and recovery device provided by the present invention;
fig. 3 is a schematic structural diagram of a condenser of an ionic liquid purification and recovery device provided by the present invention;
FIG. 4 is an enlarged schematic view of part A of an ionic liquid purification and recovery device provided by the present invention;
FIG. 5 is an enlarged schematic view of part B of an ionic liquid purification and recovery device provided by the present invention;
fig. 6 is an enlarged schematic view of a part C of the ion liquid purification and recovery device provided by the present invention.
In the figure: the device comprises a shell 1, an ionic liquid storage tank 2, a conduit 3, a buffer filter plate 4, a preheating tank 5, a spiral liquid flow channel 6, a distillation still 7, a heating plate 8, a temperature controller 9, a temperature sensor 10, a condenser 11, a condenser jacket 12, a water tank 13, a cooler 14, a concentration sensor 15, a first two-way valve 16, an ionic liquid collection tank 17, a placement tank 18, a fan 19, a first gear 20, a second gear 21, a third rotating column 22, a third gear 23, a fourth gear 24, a fifth gear 25, a fourth rotating column 26, a fifth rotating column 27, a sixth gear 28, a seventh gear 29, an eighth gear 30, a ninth gear 31, a sixth rotating column 32, a first rotating column 33, a water pump fan 34, a motor 35, a second rotating column 36 and a fixed tank 37.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-6, an ionic liquid purification and recovery device comprises a shell 1 and a plurality of guide pipes 3, wherein an ionic liquid storage tank 2 is arranged inside the shell 1, the ionic liquid storage tank 2 is connected with a preheating tank 5, a buffer filter plate 4 is arranged on a liquid inlet of the preheating tank 5, a spiral liquid flow passage 6 is arranged inside the preheating tank 5, the ionic liquid storage tank 2 is connected with the spiral liquid flow passage 6 through one guide pipe 3, a liquid outlet of the spiral liquid flow passage 6 is connected with a distillation kettle 7 through one guide pipe 3, the distillation kettle 7 is connected with a condenser 11 through one guide pipe 3, the condenser 11 is externally wrapped with a condenser jacket 12, the condenser jacket 12 is fixedly connected with a water tank 13, one end of the water tank 13 far away from the ionic liquid storage tank 2 is connected with the condenser jacket 12 through one guide pipe 3, one end of the condenser 11 far away from the water tank 13 is connected with, and the one end that condenser 11 was kept away from to cooler 14 is connected with concentration sensor 15, the one end that water tank 13 was kept away from to condenser overcoat 12 is connected with through a pipe 3 and places case 18, just place and install fan 19 in the case 18, it is connected with the water guide shell through a pipe 3 to place case 18, and the water guide shell is kept away from the one side of placing case 18 and is connected with preheating cabinet 5, install water pump flabellum 34 in the water guide shell, and water pump flabellum 34 fixedly connected with rotates post 32 sixth, sixth rotates post 32 top welding has ninth gear 31, and ninth gear 31 meshes has eighth gear 30, eighth gear 30 is connected with fifth rotation post 27, and the one end welding that fifth rotation post 27 kept away from eighth gear 30 has seventh gear 29, seventh gear 29 meshes has sixth gear 28, just sixth gear 28 is connected with fourth rotation post 26, fourth rotates the one end welding that sixth gear 28 was kept away from to post 26 has fifth gear 25, and the meshing of fifth gear 25 has fourth gear 24, fourth gear 24 is connected with first rotation post 33, just fourth gear 24 keeps away from the one end meshing of fifth gear 25 has third gear 23, third gear 23 is connected with third rotation post 22, just the welding of the one end that third gear 23 was kept away from to third rotation post 22 has second gear 21, the meshing of second gear 21 has first gear 20, just first gear 20 is connected with second rotation post 36, fan 19 in the case 18 is placed to second rotation post 36 fixed connection, its the one end that fourth gear 24 was kept away from to first rotation post 33 is connected with motor 35.
The utility model discloses in, 11 internally mounted of condenser has the condensation spiral pipe, be equipped with hot plate 8 in stills 7, install temperature sensor 10 in stills 7, just the 7 shells of stills are equipped with temperature controller 9.
The utility model discloses in, fan 19 is located the pipe both sides, and fixed connection between the fan 19 of both sides, and second rotation post 36 drives a side fan 19 and rotates, and fan 19 drives the fan 19 of opposite side and rotates together.
The utility model discloses in, still include fixed case 37, just motor 35, first gear 20, fourth gear 24, fifth gear 25, third gear 23, sixth gear 28, seventh gear 29, second gear 21, first rotation post 38, second rotation post 36, third rotation post 22, fourth rotation post 26, fifth rotation post 27 have been placed in fixed case 37.
The utility model discloses in, concentration sensor 15 is connected with first two-way valve 16, just the first valve of first two-way valve 16 is connected with ionic liquid storage tank 2, and the second valve is connected with ionic liquid collection tank 17.
The working principle is as follows: in the utility model, the ionic liquid to be purified is put into the ionic liquid storage tank 2 and starts working, the ionic liquid starts to flow into the preheating tank 5 through the conduit 3, the buffer filter plate 4 is installed at the feed inlet of the preheating tank 5 to filter some impurities in the ionic liquid, the ionic liquid enters the spiral liquid flow passage 6 in the preheating tank 5, the water with a certain temperature in the water tank 13 flows into the condenser jacket 12 and flows into the preheating tank 5 through the conduit 3, the ionic liquid extends the preheating time in the spiral liquid flow passage 6, the ionic liquid enters the distillation kettle 7, the heating plate 8 in the distillation kettle 7 starts working, the temperature sensor 10 in the distillation kettle 7 monitors the temperature, the temperature controller 9 of the shell controls the temperature, the ionic liquid enters the condenser 11 through the conduit 3, the water in the preheating tank 5 starts to absorb water through the water guide shell, the water flows in the conduit 3, the guide pipe 3 is provided with a placing box 18, fans 19 are arranged in two sides of the placing box 18, the fans 19 are driven to reduce the temperature of water, the water enters a condenser outer sleeve 12 wrapped outside the condenser 11, distilled ionic liquid flows in a condensation spiral pipe in the condenser 11 and is subjected to thermal reaction with the water in the condenser outer sleeve 12, the temperature of the ionic liquid is absorbed by the water, the ionic liquid enters a cooler 14 for cooling, the water of the condenser outer sleeve 12 is continuously circulated with a preheating box 5, the cooled ionic liquid is detected through a concentration sensor 15 arranged at the outlet of the cooler 14, the concentration sensor 15 sends the detection result to a through valve controller, when the concentration of the ionic liquid reaches the standard, the second valve of the first two-way valve 16 is opened, the qualified ionic liquid enters the ionic liquid collecting tank 17, and when the concentration does not reach the standard, opening the first valve, and feeding unqualified ionic liquid into the ionic liquid storage tank 2 for secondary purification.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (5)
1. An ionic liquid purification and recovery device comprises a shell (1) and a plurality of guide pipes (3), wherein an ionic liquid storage tank (2) is installed inside the shell (1), the ionic liquid storage tank (2) is connected with a preheating tank (5), a buffering filter plate (4) is arranged on a liquid inlet of the preheating tank (5), a spiral liquid flow passage (6) is installed inside the preheating tank (5), the ionic liquid storage tank (2) is connected with the spiral liquid flow passage (6) through one guide pipe (3), and a liquid outlet of the spiral liquid flow passage (6) is connected with a distillation kettle (7) through one guide pipe (3); it is characterized in that the preparation method is characterized in that,
the distillation kettle (7) is connected with a condenser (11) through a guide pipe (3), the condenser (11) is externally wrapped by a condenser jacket (12), the condenser jacket (12) is fixedly connected with a water tank (13), one end of the water tank (13) far away from the ionic liquid storage tank (2) is connected with the condenser jacket (12) through the guide pipe (3), one end of the condenser (11) far away from the water tank (13) is connected with a cooler (14) through the guide pipe (3), one end of the cooler (14) far away from the condenser (11) is connected with a concentration sensor (15), one end of the condenser jacket (12) far away from the water tank (13) is connected with a placing box (18) through the guide pipe (3), a fan (19) is installed in the placing box (18), the placing box (18) is connected with a water guide shell through the guide pipe (3), and one side of the water guide shell, which is far away from the placement box (18), is connected with the preheating box (5), a water pump fan blade (34) is installed in the water guide shell, a sixth rotating column (32) is fixedly connected with the water pump fan blade (34), a ninth gear (31) is welded at the top of the sixth rotating column (32), an eighth gear (30) is meshed with the ninth gear (31), the eighth gear (30) is connected with a fifth rotating column (27), a seventh gear (29) is welded at one end, which is far away from the eighth gear (30), of the fifth rotating column (27), the seventh gear (29) is meshed with a sixth gear (28), the sixth gear (28) is connected with a fourth rotating column (26), a fifth gear (25) is welded at one end, which is far away from the sixth gear (28), of the fourth rotating column (26), and a fourth gear (24) is meshed with the fifth gear (25), fourth gear (24) are connected with first rotation post (33), just fourth gear (24) keep away from the one end meshing of fifth gear (25) has third gear (23), third gear (23) are connected with third rotation post (22), just third rotation post (22) keep away from the one end welding of third gear (23) has second gear (21), second gear (21) meshing has first gear (20), just first gear (20) are connected with second rotation post (36), fan (19) in case (18) are placed to second rotation post (36) fixed connection, its first rotation post (33) keep away from the one end of fourth gear (24) and are connected with motor (35).
2. The ionic liquid purification and recovery device as claimed in claim 1, wherein a condensation spiral pipe is installed inside the condenser (11), a heating plate (8) is arranged inside the distillation kettle (7), a temperature sensor (10) is installed inside the distillation kettle (7), and a temperature controller (9) is arranged on the shell of the distillation kettle (7).
3. The ionic liquid purifying and recycling device of claim 1, wherein the fans (19) are disposed on two sides of the duct (3), and the fans (19) on the two sides are fixedly connected.
4. The ionic liquid purification and recovery device according to claim 1, further comprising a fixing box (37), wherein a motor (35), a first gear (20), a fourth gear (24), a fifth gear (25), a third gear (23), a sixth gear (28), a seventh gear (29), a second gear (21), a first rotating column (33), a second rotating column (36), a third rotating column (22), a fourth rotating column (26) and a fifth rotating column (27) are placed in the fixing box (37).
5. The ionic liquid purification and recovery device as claimed in claim 1, wherein a first two-way valve (16) is connected to the concentration sensor (15), the ionic liquid storage tank (2) is connected to a first valve of the first two-way valve (16), and the ionic liquid collection tank (17) is connected to a second valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020207435.4U CN212017022U (en) | 2020-02-25 | 2020-02-25 | Ionic liquid purification and recovery device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020207435.4U CN212017022U (en) | 2020-02-25 | 2020-02-25 | Ionic liquid purification and recovery device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212017022U true CN212017022U (en) | 2020-11-27 |
Family
ID=73493001
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202020207435.4U Active CN212017022U (en) | 2020-02-25 | 2020-02-25 | Ionic liquid purification and recovery device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212017022U (en) |
-
2020
- 2020-02-25 CN CN202020207435.4U patent/CN212017022U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN2232916Y (en) | Seawater desalination unit utilizing solar vacuum tube | |
| CN201104133Y (en) | Aluminum electrolysis flue gas residual heat utilization device | |
| CN212017022U (en) | Ionic liquid purification and recovery device | |
| CN206245389U (en) | A kind of outdoor solar air water-making machine | |
| CN210965129U (en) | Organosilicon cooling and heat recovery device | |
| CN207113642U (en) | A kind of Nitrobenzene Rectification tower byproduct steam condensate recycling device | |
| CN215798989U (en) | Device for deeply resolving waste liquid of urea | |
| CN113634044A (en) | Liquid concentration and purification device for indoxacarb production and working method thereof | |
| CN114396812A (en) | Sulfuric acid process primary conversion heating medium type high-temperature flue gas waste heat recovery system | |
| CN201081442Y (en) | Thermotube plate type split passive high-efficiency solar heat hot water system | |
| CN112696941A (en) | Power plant cooling tower waste heat recovery device with bypass | |
| CN211953742U (en) | Waste heat recovery device of rotary cement kiln | |
| CN207952203U (en) | Mercury lamp pipe recycling equipment | |
| CN111547798A (en) | Waste water MVR evaporimeter is smelted to gold | |
| CN219546745U (en) | High efficiency waste water evaporation equipment | |
| CN220472332U (en) | Flue gas treatment device for electric melting furnace | |
| CN219674839U (en) | Waste heat utilization mechanism of submerged arc furnace | |
| CN217955926U (en) | Recycling device for electrolyte of vanadium redox flow battery | |
| CN219829107U (en) | Heat exchange energy-saving steam water heater | |
| CN214333430U (en) | High-efficiency cold-resistant anti-corrosion condensing steam turbine condenser | |
| CN215855974U (en) | Plant extraction of essential oil device for cosmetics | |
| CN2525447Y (en) | Heat energy recovering device from waste hot water containing impurities | |
| CN220597096U (en) | Recovery treatment device for waste water containing n-butyl acetate | |
| CN216320018U (en) | Liquid collecting device for chemical distillation tower | |
| CN217424057U (en) | Anti-blocking high-efficiency heat recovery heat exchanger |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |