CN211913308U - Clean and environment-friendly soil sample and plant sample digestion device - Google Patents
Clean and environment-friendly soil sample and plant sample digestion device Download PDFInfo
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- CN211913308U CN211913308U CN201921742798.1U CN201921742798U CN211913308U CN 211913308 U CN211913308 U CN 211913308U CN 201921742798 U CN201921742798 U CN 201921742798U CN 211913308 U CN211913308 U CN 211913308U
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Abstract
The utility model discloses a soil sample and plant sample boiling device that disappears of clean environmental protection, it includes the box, and the bottom of box is connected with the bottom of the case, is equipped with the support on the bottom of the case, is equipped with heating furnace or iron plate on the support, has the side door through hinged joint in the place ahead of box, the upper portion of box is equipped with the purification groove, is equipped with neutralization pond in the purification groove, is equipped with the aeration pipe in the neutralization pond, and the side in neutralization pond is equipped with the fan, is equipped with the gas collecting channel on the bottom plate of purification groove, and import pipe and fan entry linkage are passed through at the gas collecting channel top, and the fan export passes through outlet pipe and aeration pipe intercommunication, connects the stand between the bottom of the case and the. The device reduces experimental errors and experimental time cost, improves digestion efficiency, greatly ensures the health of experimenters and the normal service life of other equipment, effectively solves the problem of pollution and damage of acid waste gas after digestion to the atmosphere, and realizes green emission of harmful gas.
Description
Technical Field
The utility model relates to a boiling device disappears, especially relates to a boiling device disappears with plant sample of soil sample of clean environmental protection, belongs to soil agricultural chemistry experimental facilities technical field.
Background
Traditional agro-chemical digestion device all moves each device that needs to use among the digestion process to fixed huge fume hood earlier, simply piece together the combination and become a set of simple and easy digestion device again, lack the wholeness and the unity of equipment, this has also led to the in-process step of actually digesting complicated, lengthened the digestion time to the sample, lead to digestion efficiency on the low side, and there are great experimental risk and potential safety hazard, if digest the high temperature splash of the strong corrosive concentrated acid among the process, the landing of digestion pipe among the sample transfer cooling process, the evaporation of the strong corrosive waste gas among the sample cooling process overflows, it has led to the fact the injury to the experimenter health greatly, and accelerated to digest other equipment's of room aging, damage. In addition, the fume hood used for traditional soil and plant sample digestion simply pumps and exhausts waste acid gas generated in the digestion process, and finally the waste acid gas is exhausted to the air or a sewer, so that the environment is greatly polluted and damaged.
Disclosure of Invention
The to-be-solved technical problem of the utility model is: the utility model provides a clean environmental protection's soil sample and plant sample boiling device that disappears has mainly unified the step of boiling the operation in-process that disappears, has reduced the error and the experimental time cost of experiment, has improved the efficiency that boils that disappears, very big guarantee the healthy of experimenter and the normal service life of other equipment to effectively solved the acidic waste gas after boiling that disappears to atmospheric pollution and destruction, realize harmful gas's green emission. Furthermore, the utility model discloses area is little, can move, and the requirement of putting to the space resource and the overall arrangement in laboratory is low, can actually put according to the laboratory, the effectual problem of having solved above-mentioned existence.
The technical scheme of the utility model is that: the utility model provides a soil sample and plant sample digestion device of clean environmental protection, it includes the box, and the bottom of box is connected with the bottom of the case, is equipped with the support on the bottom of the case, is equipped with heating furnace or iron plate on the support, has the side door through hinged joint in the place ahead of box, the upper portion of box is equipped with the purification groove, is equipped with the neutralization pond in the purification groove, is equipped with the aeration pipe in the neutralization pond, is equipped with the fan in the outside in neutralization pond, is equipped with the gas collecting channel on the bottom plate of purification groove, and import pipe and fan entry linkage are passed through at the gas collecting channel top, and the fan export passes through outlet pipe and aeration pipe intercommunication, connects the stand between the bottom of.
The door is symmetrically arranged left and right, and the door is made of transparent glass.
Purify the bottom plate and the lateral wall and the box fixed connection of groove, be equipped with power control panel on purifying the antetheca in groove, purify the top in groove and be equipped with the roof, be equipped with shutter, liquid feeding pipe, atomizer and clarifier on the roof.
The neutralizing tank is six sealed cavity box structures, and the both ends fixed connection of neutralizing tank is equipped with the liquid meter on purifying the lateral wall of groove on the side of neutralizing tank, and the aeration pipe is located the bottom and the level arrangement of neutralizing tank, and the both ends of aeration pipe are sealed and are equipped with a plurality of aeration holes on the pipe wall, still are equipped with the pH probe in neutralizing tank, and the pH probe passes through the data line to be connected with the display screen on the power control panel, are connected with the delivery pipe on the bottom side in neutralizing tank, the delivery pipe stretches out the box outside and communicates with the sewage disposal system, is equipped with the valve on the delivery pipe.
The bottom end of the liquid feeding pipe extends into the neutralizing tank, and the top end of the liquid feeding pipe is provided with a sealing cover in threaded connection.
The access connection of atomizer has the feed liquor pipe, and the feed liquor pipe stretches into the bottom in neutralization pond, and there is the shower nozzle in the export of atomizer through pipe connection, the shower nozzle is located the inboard top in neutralization pond, and the atomizer is the plunger pump of a low discharge high-lift.
The purifier is a cylindrical columnar structure, a plurality of layers are arranged in the purifier, activated carbon particles are placed on each layer, fine holes are formed in the laminates, and the bottom end of the purifier extends into the top of the inner side of the neutralization tank through a pipeline.
The digestion basket comprises two bilaterally symmetrical connecting rods, a lifting hook and a pipe support, one end of each connecting rod is fixedly connected to the lantern ring, the lantern ring can be freely rotated and movably sleeved on the stand column, the lifting hook is fixedly connected to the lower portion of the other end of each connecting rod, the pipe support is placed on the lifting hook, and the pipe support is located right above the heating furnace.
The pipe support comprises transverse rods, vertical rods, a first connecting rod, a second connecting rod, a third connecting rod and a pore plate, the two transverse rods are symmetrically arranged, the first connecting rod is fixedly connected between the transverse rods, the second connecting rod is fixedly connected between the first connecting rods and uniformly distributed, the four vertical rods are fixedly connected to the four corners of the second connecting rod, the third connecting rod is fixedly connected between the vertical rods, pore holes are uniformly distributed in the pore plate at the top ends of the vertical rods, and digestion pipes are placed in the pore holes.
The orifice plate is arranged in an inclined mode, and the inclination angle is 15 degrees.
The utility model has the advantages that: compared with the prior art, adopt the technical scheme of the utility model, firstly, the efficiency and the quality of experiment have been improved. Compared with the traditional mode of randomly placing and boiling the samples, the fixed boiling-eliminating mode with orderly arrangement of the boiling-eliminating baskets of the device can boil more samples on the same electric furnace heating area, and in addition, the device unifies the boiling-eliminating environment of the samples, reduces some fussy operation steps such as sample transfer cooling and the like, saves the experimental time, namely reduces the system error in the experimental boiling-eliminating process and shortens the experimental time; secondly, the safety of the experimental process is guaranteed. The device is used for conducting digestion work on the soil sample and the plant sample, unsafe conditions such as splashing of strong corrosive concentrated acid in the digestion process of the sample, slipping in the transfer process of a digestion pipe, overflow of strong corrosive gas in the cooling process of the sample and the like can be avoided, and the safety of experimenters is guaranteed; third, realized the green environmental protection of gas emission, this device begins to the discharge of final gas from the collection of waste gas, and acid corrosivity acid waste gas need pass through 3 stages's purification treatment to reach green emission's purpose.
Drawings
FIG. 1 is a first schematic structural diagram of the present invention;
FIG. 2 is a second schematic structural view of the present invention;
FIG. 3 is a top view of the present invention;
FIG. 4 is a schematic view showing the internal structure of the purification tank of the present invention;
FIG. 5 is a schematic view of the internal structure of the purification tank of the present invention;
FIG. 6 is a schematic view of the digestion basket of the present invention;
FIG. 7 is a first schematic view of the structure of the pipe frame of the present invention;
FIG. 8 is a second schematic view of the structure of the pipe frame of the present invention;
fig. 9 is a schematic diagram of the circuit wiring of the present invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail with reference to the accompanying drawings.
Example 1: as shown in the attached figures 1-8, a clean and environment-friendly soil sample and plant sample digestion device comprises a box body 7, the bottom of the box body 7 is connected with a box bottom 3, a support 6 is arranged on the box bottom 3, a heating furnace 5 or an iron block 4 is arranged on the support 6, a side opening door 1 is connected in front of the box body 7 through a hinge 2, a purification tank 10 is arranged on the upper portion of the box body 7, a neutralization tank 27 is arranged in the purification tank 10, an aeration pipe 26 is arranged in the neutralization tank 27, a fan 14 is arranged outside the neutralization tank 27, a gas collecting hood 11 is arranged on a bottom plate of the purification tank 10, the top of the gas collecting hood 11 is connected with an inlet of the fan 14 through an inlet pipe 15, an outlet of the fan 14 is communicated with the aeration pipe 26 through an outlet pipe 16, a stand column 9 is connected between the box bottom 3.
Further, the door 1 is arranged in a left-right symmetrical mode, and the material of the door 1 is transparent glass.
Further, the bottom plate and the side wall of the purification tank 10 are fixedly connected with the box body 7, the front wall of the purification tank 10 is provided with a power control panel 12, the top of the purification tank 10 is provided with a top plate 17, and the top plate 17 is provided with a shutter 18, a liquid feeding pipe 24, an atomizer 21 and a purifier 22.
Further, the neutralization tank 27 is a box structure with six sealed cavities, two ends of the neutralization tank 27 are fixedly connected to the side wall of the purification tank 10, a liquid meter 13 is arranged on the side edge of the neutralization tank 27, an aeration pipe 26 is positioned at the bottom of the neutralization tank 27 and is horizontally arranged, two ends of the aeration pipe 26 are sealed, a plurality of aeration holes are formed in the pipe wall of the aeration pipe 26, a pH probe 28 is further arranged in the neutralization tank 27, the pH probe 28 is connected with a display screen on the power control panel 12 through a data line 20, a discharge pipe 30 is connected to the side edge of the bottom of the neutralization tank 27, the discharge pipe 30 extends out of the box 7 and is communicated with a sewage discharge system, and a valve 31 is arranged on the discharge pipe.
Further, the bottom end of the filling pipe 24 extends into the neutralizing tank 27, and the top end of the filling pipe 24 is provided with a sealing cover 19 in threaded connection.
Further, the inlet of atomizer 21 is connected with feed liquor pipe 25, and feed liquor pipe 25 stretches into the bottom in neutralization pond 27, and there is shower nozzle 23 in the export of atomizer 21 through the pipe connection, shower nozzle 23 is located the inboard top in neutralization pond 27, and atomizer 21 is a plunger pump of low discharge high lift.
Further, the purifier 22 is a cylindrical column structure, the inner part of the purifier 22 is provided with a plurality of layers, activated carbon particles are placed on each layer, the laminate is provided with pores, and the bottom end of the purifier 22 extends into the top of the inner side of the neutralization tank 27 through a communicating pipe 221.
Furthermore, the digestion basket 8 comprises two connecting rods 81, a lifting hook 82 and a pipe frame 83 which are bilaterally symmetrical, one end of each connecting rod 81 is fixedly connected to the corresponding lantern ring 29, the lantern ring 29 is movably sleeved on the upright post 9 in a freely rotating mode, the lifting hook 82 is fixedly connected to the lower portion of the other end of each connecting rod 81, the pipe frame 83 is placed on the lifting hook 82, and the pipe frame 83 is located right above the heating furnace 5.
Further, the pipe support 83 includes a cross bar 835, vertical bars 832, a first connecting rod 833, a second connecting rod 834, a third connecting rod 836 and a pore plate 831, the two cross bars 835 are symmetrically arranged, the first connecting rod 833 is fixedly connected between the cross bars 835, the first connecting rod 833 is fixedly connected with the second connecting rod 834 which is uniformly distributed between the first connecting rod 833, four vertical bars 832 are fixedly connected with four corners of the second connecting rod 834, the third connecting rod 836 is fixedly connected between the vertical bars 832, the pore plate 831 is fixedly connected with the top end of the vertical bars 832, pore holes 837 are uniformly distributed on the pore plate 831, and digestion pipes are placed in the pore holes 837.
Further, the orifice plate 831 is arranged obliquely at an inclination angle of 15 degrees.
The box body 7 is made of corrosion-resistant plastics and can resist corrosion of strong corrosive gas generated during digestion.
The glass observation door 1 can be opened laterally from left to right, so that the effect of sealing the digestion chamber is achieved, and the digestion condition in the digestion chamber can be checked through the glass observation door 1.
The power control panel 12 integrates an electric appliance control panel integrating a corrosion-resistant fan power switch, a corrosion-resistant atomizer power switch, a pH probe 28 and a pH value display screen.
The pH display screen can display the pH of the solution in the neutralization tank 27.
The liquid level meter 13 can observe the liquid content in the neutralization tank 27 through the liquid level meter, and a viewing hole is provided in the side walls of the purification tank 10 and the tank 7 at the position of the liquid level meter 13 so that the value of the liquid level meter 13 can be observed.
The support 6 is adjustable support (hand formula elevating platform), can adjust the height of support 6 through the rotation of knob 61, can make heating furnace 5 or iron plate 4 just in time laminate and heat or cool off in the bottom of digestion pipe like this.
Except that the supports 6 for supporting the two electric heating furnaces 5 in the middle are fixed on the bottom plate of the digestion chamber through screws, the other supports 6 for supporting the iron blocks 4 on the two sides are not fixed and are directly placed in the digestion chamber.
The gas collecting channel 11 is a corrosion-resistant plastic exhaust guide opening, can play a role in guiding the absorption of waste gas and guides the waste gas to the inlet of the fan 14.
The neutralizing liquid discharging pipe is communicated with the bottom of the neutralizing tank 27, and the waste liquid after the neutralizing treatment in the neutralizing tank is discharged along the pipe.
The support 6 can adjust the height of the support 6 through the knob 61, namely, the electric furnace and the cooling metal iron block 4 are contacted with the digestion basket.
And the metal iron block 4 for cooling is used for quickly and uniformly reducing the high temperature of the digestion pipe through the metal heat conduction function of the metal iron block 4 after digestion is finished.
The electric heating furnace 5 plays a role in heating, and the purpose of uniformly heating the bottom of the digestion tube is achieved after the asbestos net is placed on the bearing net at the bottom of the digestion basket.
The digestion basket support rack is used for supporting the pipe support 83, can bear certain weight and is connected to the lantern ring.
Pipe frame 83: the inclined opening plane of the pipe frame 83 forms a certain angle inwards when the pipe frame is used for loading the digestion pipe, so that the danger that strong corrosive acid liquid in the digestion pipe splashes to people in the digestion process is prevented.
The corrosion-resistant fan 14 is made of corrosion-resistant materials, and is used for pumping out strong corrosive gas from the digestion chamber, and conveying the acidic waste gas into the alkali liquor in the neutralization tank 27 through the vent pipe, so that the acidic waste gas is completely contacted with the alkali liquor, and the first acid-base neutralization treatment of the waste gas is achieved. The fan 14 model adopts: PF-150W2, manufactured under the brand name: and (5) refreshing wind.
The aeration pipe 26: the corrosion-resistant fan 14 and the neutralization tank 27 are connected and are inclined into the bottom in the neutralization tank 27.
The heat dissipation louver 18: the heat generated by the corrosion-resistant fan 14 is dissipated to avoid excessive heat accumulation in the cavity formed between the corrosion-resistant plastic exhaust box housing and the neutralization tank 27.
Alkali liquid filling pipe 24: lye can be added to the neutralization tank (27) from the outside through a lye filling pipe 24.
Sealing cover 19: the sealed alkali liquor filling pipe is contacted with the outside.
Corrosion-resistant atomizer 21: the liquid-alkali neutralizing device is made of corrosion-resistant materials, and comprises a body fluid inlet and an outlet, wherein the inlet is connected with one section of the atomizer liquid suction pipe, one end of the outlet is connected with an atomization port, alkali liquor can be sprayed out from the atomization port after being sucked by the liquid suction pipe, the atomization port is foggy, the contact between the alkali liquor and acid waste gas is further strengthened, and secondary acid-alkali neutralizing treatment on waste liquid is formed.
probe of pH detector: made of corrosion-resistant material, and the detection probe is inserted into the treatment liquid in the neutralization tank 27.
Activated carbon purifier 22: because of the effect of corrosion-resistant convulsions motor exhaust for the gas pressure in neutralization pond 27 increases, and the gas after the acid waste gas through two preceding neutralization treatment, two-layer active carbon absorption harmful waste gas that probably remain through the active carbon purification treater finally outwards discharge forms the third processing of waste gas promptly, thereby ensures the comprehensive purification to waste gas.
Activated carbon purifier 22: the ventilation device consists of a ventilation porous stacking sheet, ventilation thin tubes, ventilation thick tubes and ventilation thin tube filter screens. The porous stacking piece that ventilates is circular thin slice, uses the centre of a circle as the outside 8 line segments that evenly set up of central point, and the partition sets up 3 air vents and 4 air vents respectively on the adjacent line segment, and every ventilates and sets up 28 air vents on the porous stacking piece altogether, the primary action: the activated carbon filter is separated into different treatment layers and is used for bearing and supporting the weight of activated carbon particles, and the small vent holes can enable gas to pass through the small vent holes to form vent channels. The ventilation tubule passes through the corrosion-resistant plastic air pumping box body shell and is directly communicated into the neutralization tank 27; the air-through thick pipe is divided into three layers of cavities by the air-through porous stacking layer, the first layer is a cavity layer, active carbon particles are not placed in the cavity layer, and the cavity layer is a gas buffer layer and is mainly used for reducing the pressure, flow rate and gas humidity of processing gas entering the active carbon layer; activated carbon particles are placed in the second layer and the third layer, and are activated carbon purification treatment layers, so that the device has the main effects that: absorbing harmful waste gas remained in the treatment gas; the tubule filter screen of ventilating is made by corrosion resistance nylon materials and has less mesh, and it is fixed in the tubule department of ventilating of first layer, and the main role is: prevent that the little piece of upper activated carbon from falling into in the exhaust-gas treatment case.
After being subjected to neutralization treatment twice in the neutralization tank 27, the acidic waste gas passes through the ventilation tubule to reach the first layer, namely the gas buffer layer, in the activated carbon purification filter, and then passes through the second and third activated carbon layers on the upper part of the activated carbon purification filter to absorb harmful waste gas possibly remaining in the gas, and finally the harmful waste gas is discharged outwards, namely the activated carbon purification filter performs third treatment on the waste gas to ensure the comprehensive purification of the waste gas.
The oblique fixed plane of the digestion tube of the oblique digestion basket 8 is inclined at 15 degrees with the horizontal plane, the oblique fixed plane of the digestion tube is square, 4 multiplied by 4 is arranged in the longitudinal and transverse directions, 16 digestion tube sockets are formed, the oblique fixed plane of the digestion tube of the oblique digestion basket 8 is connected with a basket body surrounded by 3mm thick iron wires into a whole, a basket of the oblique digestion basket is surrounded by upper, middle and lower 3 guardrail metal wires in the horizontal direction along 4 digestion basket inclined columns, the distance between the lowermost guardrail metal wire and a bearing net at the bottom of the digestion basket is 1cm, a middle hollow layer with the distance of 1cm is formed, so that asbestos gauze is inserted inwards horizontally along the layer, and 5 iron wires with the thickness of 3mm are arranged on the bearing net at the bottom of the digestion basket in the longitudinal and transverse directions in an equal way to form a square with the distance of 20cm multiplied by 20 cm; in the experiment, the asbestos mesh is required to be placed on the bearing net at the bottom of the digestion basket, and the function of the bearing net at the bottom of the digestion basket is mainly used for uniformly supporting the weight of the asbestos mesh and the digestion pipes above the asbestos mesh. The hanging rods on two sides of the bearing net at the bottom of the digestion basket are connected with metal rods with four vertical angles extending transversely. The distance between the hooks of the support hanging frame is slightly smaller than the side length of the bearing net at the bottom of the digestion basket, so that the limiting effect is achieved, and the digestion basket with the inclined opening is prevented from sliding off the support hanging frame.
The round at the bottom of the lifting platform protection fence is surrounded by 3mm thick iron wires and has the same size with the lifting platform, and four corners of the lifting platform protection fence are provided with small square iron fixing pieces in screw hole positions, the round at the upper part of the lifting platform protection fence is surrounded by 3mm thick iron wires, the vertical distance between the upper circle and the lower circle is 5cm, and the upper circle and the lower circle are connected into a whole by four 3mm thick iron wires to form the lifting platform protection fence. Wherein: set up the screw hole site on 4 apex angles of base of the hand-rotating elevating platform of bearing cooking stove that disappears, fix the elevating platform base on the inside bottom plate of corrosion-resistant plastic equipment box through the screw, be provided with the screw hole site on 4 each angles of elevating platform, fix the protective fence of falling platform and elevating platform through the screw.
The electric furnace/cooling metal iron block is arranged on the lifting platform, and the lifting platform protection fence plays a role in preventing the electric furnace/cooling metal iron block 4 from sliding and falling.
Remarking: the hand-rotating lifting platform for supporting the electric cooking stove is fixed on the bottom plate of the cooking chamber through screws, and the other hand-rotating lifting platforms for supporting the metal cooling blocks on two sides are not fixed and are directly placed in the cooking chamber.
The working principle of the device is as follows:
opening the alkali liquor filling cover on the top of the device, pouring prepared alkali liquor into the neutralization tank 27 along the alkali liquor filling pipe, observing the liquid level observation window on the side surface of the device, adding alkali liquor until the liquid level observation window is properly scaled from one half to two thirds, stopping adding the alkali liquor, and covering the alkali liquor filling cover.
And opening a glass observation window of the device, opening an air draft power switch on the control panel of the electric appliance to start an air exhaust function, and simultaneously opening a power switch of the atomizer to start an alkali liquor atomization function. Placing asbestos net water on a bearing net at the bottom of the oblique-mouth digestion basket, and sequentially inserting digestion pipes filled with soil samples into the oblique-mouth digestion basket, so that the pipe orifices of the digestion pipes are inclined towards the inside of the device (forming a safe angle with an experimenter, avoiding strong acid boiling and splashing to hurt the person in the digestion process, and meanwhile, the inclination inwards is more favorable for strong acid steam generated in the digestion process to be pumped out of a digestion chamber); according to the requirements of specific experimental techniques, sequentially adding the required digestion acid liquor into the digestion tube (at the moment, strong corrosive gas volatilized by strong acid is safely pumped out of the digestion chamber); rotating the digestion basket support hanging frame to enable the bottom of the oblique-opening digestion basket to correspond well to the plane of the electric furnace; then, the height of the electric furnace is adjusted by using the hand-rotating type lifting platform, so that the plane of the electric furnace slightly has supporting force to prop against the bottom surface of the oblique-mouth digestion basket; turning on the electric furnace and adjusting the heating size to enable the heating temperature to be proper; closing the glass observation window and stewing.
Digestion in-process constantly produces acid gas and effusion test tube this moment, acid gas is under the convulsions effect of corrosion resistance air exhauster, lead the mouth and shift to the breather pipe along corrosion-resistant plastics convulsions, and then the alkali lye bottom that enters into in the neutralization pond 27 through the aeration pipe takes place abundant reaction with alkali lye, the process of the final effusion alkali lye of acid waste gas from alkali lye bottom rebound, let acid waste gas and alkali lye direct contact promptly and produce the acid-base neutralization reaction, accomplish the first acid-base neutralization treatment to waste gas. The gas continues to rise after escaping the alkali liquor, at the moment, the atomizer water inlet pipe continuously sucks the alkali liquor into the atomizer, the alkali liquor is atomized, the atomized water spray end of the atomizer continuously sprays water-mist alkali liquor, and the water-mist alkali liquor is fully contacted with the gas treated by the waste gas in the first step in the neutralization tank 27 again to form secondary acid-base neutralization treatment on the waste gas.
The pH value of the solution will be gradually reduced along with the continuous neutralization reaction between the alkali liquor and the acidic waste gas in the neutralization tank 27, the pH value of the solution is monitored by the pH detector in real time through the pH detection probe, the pH display screen on the control panel of the electric appliance is observed, and when the pH value is lower than 9, a certain amount of alkali liquor with certain concentration needs to be added into the neutralization tank 27 to maintain the pH value of the solution above 9.
The waste gas of two rounds of acid-base neutralization treatment in the front will be discharged outward after the purification of active carbon purification filter because of the effect of pressure in the case, and the concrete process is as follows: after being subjected to neutralization treatment twice in the neutralization tank 27, the acidic waste gas passes through the ventilation tubule to reach the first layer, namely the gas buffer layer, in the activated carbon purification filter, and then passes through the second and third activated carbon layers on the upper part of the activated carbon purification filter to absorb harmful waste gas possibly remaining in the gas, and finally the harmful waste gas is discharged outwards, namely the activated carbon purification filter performs third treatment on the waste gas to ensure the comprehensive purification of the waste gas.
After the sample is cooked, the hand-rotating lifting platform where the electric furnace is located is adjusted to enable the height of the hand-rotating lifting platform to be lowered until the heating plane of the electric furnace is completely separated from the bottom surface of the bevel-opening cooking basket, then the bevel-opening cooking basket supporting rack is rotated to enable the bevel-opening cooking basket to be completely rotated away from the vertical surface where the electric furnace is located, namely, the bevel-opening cooking basket is rotated to the other side of the electric furnace, then the hand-rotating lifting platform where the cooling metal block is located is adjusted to enable the hand-rotating lifting platform to be raised until the upper top surface of the cooling metal block supports and props against the bottom of the. Therefore, the purpose of quickly and uniformly reducing the high temperature of the digestion tube is achieved by utilizing the metal quick heat conduction function of the metal block and the temperature buffering of the asbestos gauze. When the temperature of the digestion tube is reduced to the room temperature, the digestion tube can be taken out in sequence, or the oblique-mouth digestion basket is taken down integrally. The digestion work is finished.
During the use process, the pH value on the pH display screen is observed, and when alkali liquor is added into the neutralization tank 27, the liquid level observation window on the side surface is observed, so that the maximum liquid level scale mark of the liquid level observation window cannot be exceeded. When the liquid level is close to the maximum liquid level scale mark and alkali liquor needs to be added, the neutralizing liquid discharging valve is opened, the solution in the neutralizing tank 27 is discharged, and the alkali liquor is added again.
The parts of the present invention not described in detail are the known techniques of those skilled in the art. Finally, although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the present invention can be modified or replaced by other means without departing from the spirit and scope of the present invention, which should be construed as limited only by the appended claims.
Claims (10)
1. The utility model provides a soil sample and plant sample boiling device that disappears of clean environmental protection, it includes box (7), and the bottom of box (7) is connected with bottom of the case (3), is equipped with support (6) on bottom of the case (3), is equipped with heating furnace (5) or iron plate (4) on support (6), is connected with side door (1), its characterized in that through hinge (2) in the place ahead of box (7): the upper portion of box (7) is equipped with purification tank (10), be equipped with neutralization pond (27) in purification tank (10), be equipped with aeration pipe (26) in neutralization pond (27), outside at neutralization pond (27) is equipped with fan (14), be equipped with gas collecting channel (11) on the bottom plate of purification tank (10), import pipe (15) and fan (14) entry linkage are passed through at gas collecting channel (11) top, fan (14) export is passed through outlet pipe (16) and is communicate with aeration pipe (26), connect stand (9) between bottom of the case (3) and purification tank (10) bottom plate, be equipped with digestion basket (8) on stand (9).
2. The clean, environmentally friendly soil and plant sample digestion unit of claim 1, further comprising: the door (1) is arranged in a bilateral symmetry mode, and the door (1) is made of transparent glass.
3. The clean, environmentally friendly soil and plant sample digestion unit of claim 1, further comprising: the bottom plate and the side wall of the purification tank (10) are fixedly connected with the box body (7), the front wall of the purification tank (10) is provided with a power supply control panel (12), the top of the purification tank (10) is provided with a top plate (17), and the top plate (17) is provided with a shutter (18), a liquid feeding pipe (24), an atomizer (21) and a purifier (22).
4. The clean, environmentally friendly soil and plant sample digestion unit of claim 1, further comprising: the neutralization pond (27) are six sealed cavity box structures, the both ends fixed connection of neutralization pond (27) is on the lateral wall of purifying groove (10), be equipped with liquid meter (13) on the side of neutralization pond (27), aeration pipe (26) are located the bottom and the horizontal arrangement of neutralization pond (27), the both ends of aeration pipe (26) are sealed and are equipped with a plurality of aeration holes on the pipe wall, still be equipped with pH probe (28) in neutralization pond (27), pH probe (28) are connected with the display screen on power control panel (12) through data line (20), be connected with discharge pipe (30) on the bottom side of neutralization pond (27), discharge pipe (30) stretch out the box (7) outside and communicate with the drainage system, be equipped with valve (31) on discharge pipe (30).
5. The clean, environmentally friendly soil and plant sample digestion unit of claim 3, further comprising: the bottom end of the liquid adding pipe (24) extends into the neutralizing tank (27), and the top end of the liquid adding pipe (24) is provided with a sealing cover (19) in threaded connection.
6. The clean, environmentally friendly soil and plant sample digestion unit of claim 3, further comprising: the access connection of atomizer (21) has feed liquor pipe (25), and feed liquor pipe (25) stretch into the bottom in neutralization pond (27), and there is shower nozzle (23) in the export of atomizer (21) through the pipe connection, shower nozzle (23) are located the inboard top in neutralization pond (27), and atomizer (21) are the plunger pump of a low discharge high-lift.
7. The clean, environmentally friendly soil and plant sample digestion unit of claim 3, further comprising: the purifier (22) is of a cylindrical columnar structure, a plurality of layers are arranged in the purifier (22), activated carbon particles are placed on each layer, fine holes are formed in the laminated plates, and the bottom end of the purifier (22) extends into the top of the inner side of the neutralization tank (27) through a pipeline.
8. The clean, environmentally friendly soil and plant sample digestion unit of claim 1, further comprising: digestion basket (8) are including two connecting rods (81), lifting hook (82) and pipe support (83) of bilateral symmetry, and the one end fixed connection of connecting rod (81) is on lantern ring (29), and the activity that lantern ring (29) can freely rotate is cup jointed on stand (9), and lifting hook (82) fixed connection is in the other end below of connecting rod (81), and pipe support (83) are placed on lifting hook (82), and pipe support (83) are located heating furnace (5) directly over.
9. The clean, environmentally friendly soil and plant sample digestion unit of claim 8, further comprising: pipe support (83) are including horizontal pole (835), montant (832), connecting rod (833), connecting rod two (834), connecting rod three (836) and orifice plate (831), two horizontal pole (835) symmetrical arrangement, two connecting rod one (833) fixed connection are between horizontal pole (835), five connecting rod two (834) of fixed connection evenly distributed between connecting rod one (833), four montants of fixed connection (832) on the four corners of connecting rod two (834), fixed connection connecting rod three (836) between montant (832), top fixed connection orifice plate (831) at montant (832), evenly distributed has pore hole (837) on orifice plate (831), the boiling tube that disappears has been placed in pore hole (837).
10. The clean, environmentally friendly soil and plant sample digestion unit of claim 9, further comprising: the orifice plate (831) is arranged in an inclined manner, and the inclination angle is 15 degrees.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110514511A (en) * | 2019-06-17 | 2019-11-29 | 贵州大学 | The soil sample and plant sample of a kind of clean and environmental protection, which disappear, boils device |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110514511A (en) * | 2019-06-17 | 2019-11-29 | 贵州大学 | The soil sample and plant sample of a kind of clean and environmental protection, which disappear, boils device |
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