CN211896064U

CN211896064U - Lithium sulfate's purification equipment

Info

Publication number: CN211896064U
Application number: CN202020384598.XU
Authority: CN
Inventors: 王陆培
Original assignee: Shanghai Yuli New Material Technology Co ltd
Current assignee: Shanghai Yuli New Material Technology Co ltd
Priority date: 2020-03-24
Filing date: 2020-03-24
Publication date: 2020-11-10
Anticipated expiration: 2030-03-24

Abstract

The utility model discloses a lithium sulfate purification device, which comprises a box body and a cover body, wherein the top of the box body is open, the cover body covers the upper end of the box body, the upper surface of the cover body is fixedly connected with a first motor, the output shaft of the first motor penetrates through the cover body and is fixedly connected with a stirring rod, the lower side of the stirring rod is provided with a partition plate, the partition plate is fixedly connected on the inner side wall of the box body, the lower surface of the partition plate is fixedly connected with a filter, the lower side of the filter is provided with a heating box, the heating box is fixedly connected on the upper surface of the bottom plate of the box body, the outer side wall of the box body is fixedly connected with a condenser, and the condenser is; the utility model discloses not only can also can carry out the thermal treatment to the material of downflow when stirring the material, improve the evaporation rate of material, reduce the purification time of lithium sulfate, it is convenient to have brought for the staff.

Description

Lithium sulfate's purification equipment

Technical Field

The utility model relates to a purification equipment specifically is a purification equipment of lithium sulfate.

Background

Lithium sulfate, colorless monoclinic crystal or white crystalline powder, is soluble in water, and is insoluble in acetone and absolute ethanol. The water solubility at 25 degrees was 25.7%. The crystal form is alpha, beta and gamma; the alpha type is white monoclinic crystal, the beta type is hexagonal crystal, and the gamma type is cubic crystal. It has hygroscopic property. The lithium sulfate monohydrate crystallized from the concentrated aqueous solution is very stable; has effect in treating manic depressive psychosis.

The Chinese utility model with the publication number of CN207685174U discloses a purification device of dodecyl lithium sulfate, which comprises a dissolving tank, a decoloring filter, a precise filtering system, a rectifying tank, a centrifuge and a dryer; the bottom discharge port of the dissolving tank is connected with a decoloring filter, the decoloring filter is connected with a precise filtering system through a material transferring pump, the precise filtering system is connected with the upper feed port of the rectifying tank, and the bottom discharge port of the rectifying tank is connected with a dryer through a centrifugal machine; the upper part of the rectifying tank is connected with a condenser through a reflux device, a discharge port at the bottom of the condenser is connected with a collector, the collector is connected with a water-ring vacuum pump, and the water-ring vacuum pump is connected with an emptying valve I; the dryer is connected with a condenser, the condenser is connected with a vacuum pump, and the vacuum pump is connected with an emptying valve II.

Although the purity of a purified product of the purification equipment of the dodecyl lithium sulfate is up to more than 99 percent and can be used for biological research chemical reagents, a dissolving tank, a decoloring filter, a precise filtering system, a rectifying tank, a centrifuge, a dryer and the like in the purification equipment of the dodecyl lithium sulfate are all single bodies, the occupied area is large, after all materials are dissolved, stirring equipment in the dissolving tank is stopped, next-step treatment is carried out, time and labor are consumed, inconvenience is brought to workers, and therefore the purification equipment of the lithium sulfate is provided for solving the problems.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a purification equipment of lithium sulfate to solve the problem that proposes among the above-mentioned background art.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a purification equipment of lithium sulfate, includes box and lid, the top of box is the opening form, and the lid closes the upper end at the box, the first motor of last fixed surface of lid is connected with, the output shaft of first motor runs through lid and fixedly connected with puddler, the downside of puddler is provided with the baffle, baffle fixed connection is on the inside wall of box, the lower fixed surface of baffle is connected with the filter, the downside of filter sets up the heating box, heating box fixed connection is at the bottom plate upper surface of box, fixedly connected with condenser on the lateral wall of box, the condenser is linked together through pipeline and box.

Preferably, the up end equidistance fixedly connected with gag lever post of box, the upside that the lid and extended to the lid is run through to the upper end of gag lever post, and is provided with L shape bolt on the lid, the horizontal segment of L shape bolt is inserted and is established on the gag lever post, fixedly connected with feed hopper on the lid, feed hopper is linked together with the box.

Preferably, the output shaft of first motor runs through lid and fixedly connected with axis of rotation, the lower terminal surface and the baffle of axis of rotation contact, and puddler equidistance fixed connection is on the circumference wall of axis of rotation.

Preferably, a containing cavity is formed in the partition plate, a circular plate is rotatably connected to the side wall of the containing cavity, and through holes are formed in the top and the bottom of the containing cavity and the circular plate.

Preferably, a plurality of bar teeth of lower fixed surface of circular slab are connected with, and are a plurality of the bar tooth is the annular and distributes, and the bar tooth meshing has the gear, the lower extreme of gear runs through the bottom that holds the chamber, and fixedly connected with dwang on the gear, the dwang rotates to be connected on the inside wall of box.

Preferably, the outer side wall of the box body is fixedly connected with a second motor, and one end of the rotating rod penetrates through the side wall of the box body and is fixedly connected to an output shaft of the second motor.

Preferably, the filter comprises a conical shell and a plurality of filter plates with filter holes, the filter plates are fixedly connected to the inner side wall of the conical shell, and the lower end of the conical shell is close to the heating box.

Preferably, the heating box includes box body and heating resistor silk, the top and the bottom of heating box all are the opening form, fixedly connected with heat-conducting plate on the inside wall of heating box, the heat-conducting plate is close to the lower terminal surface of box body, and heating resistor silk fixed connection is at the lower surface of heat-conducting plate.

Compared with the prior art, the beneficial effects of the utility model are that: the partition board is arranged in the box body, so that the solution stirred in the box body can be conveniently distinguished from the distilled solution, the stirring rod is arranged on the upper side of the partition board, so that the lithium sulfate can be conveniently kept away from the solvent to be stirred, the fusion speed of the lithium sulfate raw material and the solvent is improved, the solution which is well stirred can conveniently flow downwards by arranging the through hole on the partition board, the opening and closing of the through hole can be conveniently controlled by arranging the circular plate in the partition board, the filter is arranged on the lower side of the partition board, so that the filtering treatment on particles in the downflow solution can be conveniently carried out, the heating box is arranged on the lower side of the filter, so that the solution flowing into the heating box can be conveniently heated, the condenser is arranged on one side of the box body; the purification equipment for lithium sulfate can be used for stirring materials and heating the materials flowing downwards, so that the evaporation speed of the materials is increased, the purification time of the lithium sulfate is shortened, and convenience is brought to workers.

Drawings

FIG. 1 is a perspective view of the present invention;

FIG. 2 is a schematic view of the front internal structure of the present invention;

FIG. 3 is a schematic view of a portion of the enlarged structure at A in FIG. 2;

fig. 4 is a perspective view of the filter of the present invention.

In the figure: the device comprises a box body 1, a limiting rod 11, a second motor 12, a cover body 2, a 21L-shaped bolt, a feeding funnel 22, a first motor 3, a rotating shaft 31, a stirring rod 4, a partition plate 5, a containing cavity 51, a circular plate 52, a strip-shaped tooth 521, a gear 522, a rotating rod 523, a through hole 53, a filter 6, a conical shell 61, a filter plate 62, a heating box 7, a box body 71, a heating resistance wire 72, a heat conducting plate 73, a condenser 8 and a pipeline 9.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-4, the present invention provides a technical solution: the utility model provides a purification equipment of lithium sulfate, including box 1 and lid 2, the top of box 1 is the opening form, and 2 lids of lid close the upper end at box 1, the first motor 3 of last fixed surface of lid 2, the output shaft of first motor 3 runs through lid 2 and fixedly connected with puddler 4, the downside of puddler 4 is provided with

baffle

5, 5 fixed connection of baffle are on the inside wall of box 1, the lower fixed surface of baffle 5 is connected with filter 6, the downside of filter 6 sets up heating box 7, heating box 7 fixed connection is at the bottom plate upper surface of box 1, fixedly connected with condenser 8 on the lateral wall of box 1, condenser 8 is linked together through pipeline 9 and box 1.

The up end equidistance fixedly connected with gag lever post 11 of box 1, the upside that lid 2 and extended to lid 2 is run through to the upper end of gag lever post 11, and be provided with L shape bolt 21 on the lid 2, the horizontal segment of L shape bolt 21 is inserted and is established on

gag lever post

11, 2 lids of the lid of being convenient for close on box 1, and L shape bolt 21 can prevent to break away from box 1 because of vibrations about the lid 2, fixedly connected with feed hopper 22 on the lid 2, feed hopper 22 is linked together with box 1, be convenient for drop into in the box 1 with the material.

The output shaft of first motor 3 runs through lid 2 and fixedly connected with axis of rotation 31, and the lower terminal surface of axis of rotation 31 contacts with baffle 5, and puddler 4 equidistance fixed connection is on the circumference wall of axis of rotation 31, the rotation of the first motor 3 drive puddler 4 of being convenient for.

Have seted up in baffle 5 and have held chamber 51, it is connected with circular plate 52 to rotate on the lateral wall that holds chamber 51, has all seted up through-hole 53 on top, the bottom and the circular plate 52 that hold chamber 51, and the material of 5 upsides of baffle of being convenient for carries out through-hole 53 and flows down to heating box 7 in.

A plurality of bar teeth 521 of lower surface fixedly connected with of circular plate 52, a plurality of bar teeth 521 are the annular and distribute, and the meshing of bar teeth 521 has gear 522, the bottom that holds chamber 51 is run through to gear 522's lower extreme, and fixedly connected with dwang 523 on the gear 522, dwang 523 rotates and connects on the inside wall of box 1, be convenient for control circular plate 52's rotation, make through-hole 53 on circular plate 52 and baffle 5 go up the position of through-hole 53 crisscross, thereby control opening and closing of through-hole 53.

Fixedly connected with second motor 12 on the lateral wall of box 1, the one end of dwang 523 runs through the lateral wall of box 1 and fixed connection is on the output shaft of second motor 12, is convenient for drive the intermittent type of dwang 523 and rotates to the opening and close of through-hole 53 on the automatic control baffle 5.

The filter 6 comprises a conical shell 61 and a plurality of filter plates 62 with filter holes, the filter plates 62 are fixedly connected to the inner side wall of the conical shell 61, the lower end of the conical shell 61 is close to the heating box 7, and therefore materials flowing up and down the partition plate 5 can be conveniently filtered, and the filtered materials can flow into the heating box 7.

The heating box 7 comprises a box body 71 and a heating resistance wire 72, the top and the bottom of the heating box 7 are both in an open shape, a heat conduction plate 73 is fixedly connected to the inner side wall of the heating box 7, the heat conduction plate 73 is close to the lower end face of the box body 71, the heating resistance wire 72 is fixedly connected to the lower surface of the heat conduction plate 73, a through hole is formed in the bottom of the box body 1, a wire on the heating resistance wire 72 penetrates through the through hole to extend to the outer side of the box body 1, the heating resistance wire 72 can conduct heating treatment on materials in the box body 71, and the materials.

The working principle is as follows: the utility model discloses in the use, be connected the wire on first motor 3, second motor 12, the heating resistor silk 72 with the power, pour into box 1 with the solvent into, drop into the lithium sulfate raw materials into in feed hopper 22 again for in the lithium sulfate raw materials got into box 1 through feed hopper 22, when first motor 3 during operation, the output shaft of first motor 3 drove the rotation of puddler 4, thereby made the lithium sulfate raw materials fuse mutually with the solvent.

When the second motor 12 is operated, the output shaft of the second motor 12 drives the circular plate 52 to rotate intermittently by the engagement of the gear 522 and the rack 521, and when the through hole 53 in the circular plate 52 and the through hole 53 in the partition plate 5 are staggered, the through hole 53 is closed, so that the lithium sulfate on the partition plate is difficult to separate from the mixed solution of the lithium sulfate and the solvent and flow downwards.

When through-hole 53 on circular plate 52 corresponds with the position of through-hole 53 on the baffle 5, lithium sulfate raw materials and solvent mixed liquid can flow into filter 6 downwards through-hole 53, thereby carry out filtration treatment through filter 6 to the particulate matter in lithium sulfate raw materials and the solvent mixed liquid, and the mixed liquid after the filtration then flows into in the heating box 7, when heating resistor wire 72 during operation, heat on the heating resistor wire 72 passes through in heat-conducting plate 73 transmits the mixed solvent in the heating box 7, make the mixed solvent evaporation, and steam carries out cooling process in getting into condenser 8 through pipeline 9, place the below of liquid outlet on condenser 8 with collection device if collection box again, collect the condensate, thereby the purification of lithium sulfate is handled.

The internal structures of the first motor 3, the second motor 12 and the heating resistance wire 72 are known structures in the prior art, and therefore are not described herein again, wherein the condenser 8 is a water-cooled condenser, and the upper end portion and the lower end portion of the condenser 8 are respectively provided with a water inlet hole and a water outlet hole.

"fixedly connected" as described in the present invention means that two parts connected to each other are fixed together, typically by welding, screwing or gluing; "rotationally coupled" means that two components are coupled together and capable of relative motion.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a purification equipment of lithium sulfate, includes box (1) and lid (2), its characterized in that: the top of box (1) is the opening form, and lid (2) lid closes the upper end at box (1), the last fixed surface of lid (2) is connected with first motor (3), the output shaft of first motor (3) runs through lid (2) and fixedly connected with puddler (4), the downside of puddler (4) is provided with baffle (5), baffle (5) fixed connection is on the inside wall of box (1), the lower fixed surface of baffle (5) is connected with filter (6), the downside of filter (6) sets up heating box (7), heating box (7) fixed connection is at the bottom plate upper surface of box (1), fixedly connected with condenser (8) on the lateral wall of box (1), condenser (8) are linked together through pipeline (9) and box (1).

2. The apparatus for purifying lithium sulfate according to claim 1, wherein: the utility model discloses a solar energy water heater, including box (1), the up end equidistance fixedly connected with gag lever post (11) of box (1), the upper end of gag lever post (11) runs through lid (2) and extends to the upside of lid (2), and is provided with L shape bolt (21) on lid (2), the horizontal segment of L shape bolt (21) is inserted and is established on gag lever post (11), fixedly connected with feed hopper (22) on lid (2), feed hopper (22) are linked together with box (1).

3. The apparatus for purifying lithium sulfate according to claim 1, wherein: the output shaft of first motor (3) runs through lid (2) and fixedly connected with axis of rotation (31), the lower terminal surface of axis of rotation (31) contacts with baffle (5), and puddler (4) equidistance fixed connection is on the circumference wall of axis of rotation (31).

4. The apparatus for purifying lithium sulfate according to claim 1, wherein: the baffle (5) is internally provided with a containing cavity (51), the side wall of the containing cavity (51) is rotatably connected with a circular plate (52), and the top and the bottom of the containing cavity (51) and the circular plate (52) are all provided with through holes (53).

5. The apparatus for purifying lithium sulfate according to claim 4, wherein: the lower surface fixedly connected with of circular plate (52) is a plurality of bar tooth (521), and is a plurality of bar tooth (521) are the annular and distribute, and bar tooth (521) meshing has gear (522), the lower extreme of gear (522) runs through the bottom that holds chamber (51), and fixedly connected with dwang (523) on gear (522), dwang (523) rotate to be connected on the inside wall of box (1).

6. The apparatus for purifying lithium sulfate according to claim 5, wherein: fixedly connected with second motor (12) on the lateral wall of box (1), the one end of dwang (523) runs through the lateral wall of box (1) and fixed connection is on the output shaft of second motor (12).

7. The apparatus for purifying lithium sulfate according to claim 1, wherein: the filter (6) comprises a conical shell (61) and a plurality of filter plates (62) with filter holes, wherein the filter plates (62) are fixedly connected to the inner side wall of the conical shell (61), and the lower end of the conical shell (61) is close to the heating box (7).

8. The apparatus for purifying lithium sulfate according to claim 1, wherein: heating box (7) are including box body (71) and heating resistor silk (72), the top and the bottom of heating box (7) all are the opening form, fixedly connected with heat-conducting plate (73) on the inside wall of heating box (7), heat-conducting plate (73) are close to the lower terminal surface of box body (71), and heating resistor silk (72) fixed connection is at the lower surface of heat-conducting plate (73).