CN211845706U

CN211845706U - Sample containing device for testing white carbon black performance by gas phase method

Info

Publication number: CN211845706U
Application number: CN202020209070.9U
Authority: CN
Inventors: 陈珍; 刘国晶; 谭军; 杨晓义; 范建平; 徐慧芬; 孙飞; 王德球; 范佳延; 刘晶雅
Original assignee: Zhejiang Fushite Silicon Materials Co ltd
Current assignee: Zhejiang Fushite Silicon Materials Co ltd
Priority date: 2020-02-25
Filing date: 2020-02-25
Publication date: 2020-11-03
Anticipated expiration: 2030-02-25

Abstract

The utility model discloses a vapor phase method white carbon black performance test holds device with sample, including sample storage tank and drive mechanism, the top outer wall of sample storage tank links up there is the discharging pipe, and the outer wall parcel of discharging pipe has discharge mechanism, sample storage tank inner wall is provided with the inner chamber, and the left side outer wall of inner chamber settles and have the fixed block, the bottom outer wall of fixed block bonds and has the spring, the bottom middle part of inner chamber is fixed with the main shaft. This sample holds device for fumed silica performance test passes through the setting of third bottle lid, can dismantle the back with discharge mechanism and install the top at the discharging pipe, rotate between the outer wall of the inner wall that utilizes the third bottle lid and discharging pipe, the inside fumed silica who deposits of inner chamber can be mixed through the puddler that sets up, thereby avoid leading to the phenomenon production that fumed silica bonded because of the moisture gets into, can make the inside temperature of inner chamber rise through the heating pipe simultaneously, guarantee the drying of fumed silica.

Description

Sample containing device for testing white carbon black performance by gas phase method

Technical Field

The utility model relates to a white carbon black device technical field of vapor phase method specifically is a sample holds device for white carbon black performance test of vapor phase method.

Background

The fumed silica is one of the most important high-tech superfine inorganic new materials, and has the unique properties of large specific surface area, strong surface adsorption, large surface energy, high chemical purity, good dispersion performance, thermal resistance, electric resistance and the like due to small particle size, and has the unique characteristics of excellent stability, reinforcement, thickening property and thixotropy in various subjects and fields, so that the fumed silica has an irreplaceable effect.

The existing fumed silica needs to be sampled when performance detection is carried out on the fumed silica, detection data is often inaccurate due to the fact that fumed silica is stored in the past and is wet, and meanwhile, the flexibility is not strong, and the use is inconvenient.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a vapor phase method white carbon black performance test holds device with sample to the vapor phase method white carbon black who proposes in solving above-mentioned background art need will take a sample to it when carrying out the performance detection, often leads to the detection data inaccuracy because of the past humidity of vapor phase method white carbon black after depositing, and the flexibility leads to awkward problem not by force simultaneously.

In order to achieve the above object, the utility model provides a following technical scheme: a sample containing device for testing the white carbon black performance by a gas phase method comprises a sample storage tank and a transmission mechanism, wherein the outer wall of the top end of the sample storage tank is connected with a discharge pipe, the outer wall of the discharge pipe is wrapped with a discharge mechanism, the inner wall of the sample storage tank is provided with an inner cavity, the outer wall of the left side of the inner cavity is provided with a fixed block, a spring is bonded on the outer wall of the bottom end of the fixed block, a main shaft is fixed in the middle of the bottom end of the inner cavity, the middle part of the outer wall of the main shaft is wrapped with a transfer shaft, the outer wall of the left side of the transfer shaft is connected with fan blades, the outer wall of the bottom end of the sample storage tank is welded with a sleeving column, and the inner wall of the sleeving column is provided with a base, the outer wall of the bottom end of the base is bonded with a magnet, the outer wall of the front end of the sample storage tank is provided with a limiting bulge, and the bottom of the outer wall of the front end of the sample storage tank is provided with a vent hole, and the transmission mechanism is positioned at the top end of the discharge pipe.

Preferably, discharge mechanism includes first bottle lid, second bottle lid, discharge opening and discharge gate, and the outer wall parcel of first bottle lid has the second bottle lid, the discharge opening has been seted up to the top outer wall of second bottle lid, the top outer wall left side of first bottle lid is provided with the discharge gate.

Preferably, the discharge holes are equidistantly distributed on the outer wall of the top end of the second bottle cap, the bottom end of the inner wall of the first bottle cap is of a thread-shaped structure, and the second bottle cap is tightly attached to the inner wall of the first bottle cap.

Preferably, drive mechanism includes third bottle lid, single chip microcomputer controller, links up piece, puddler and heating pipe, and the top mid-mounting of third bottle lid has single chip microcomputer controller, the bottom middle part welding of third bottle lid links up the piece, and links up the right side outer wall of piece and be fixed with the puddler, the heating pipe has been linked up in the middle part of the left side outer wall of puddler.

Preferably, the heating pipe is provided with three, and the puddler is symmetrical about the outer wall central point of heating pipe and distributes, and is welding integrated structure between puddler, heating pipe and the linking piece.

Preferably, the fan blades are distributed annularly about the outer wall of the transfer shaft, and the fan blades and the main shaft form a rotating structure through the transfer shaft.

Preferably, the springs are equidistantly distributed around the outer wall of the inner cavity, and the inner cavity, the fixed block, the springs and the sample storage tank are tightly attached.

Preferably, be fixed connection between the top outer wall of magnet and the bottom outer wall of base, and the sample storage tank establishes post and base through the cover and constitutes the active structure.

Compared with the prior art, the beneficial effects of the utility model are that:

1. this test of gaseous phase method white carbon black performance holds device utilizes the outer wall of discharging pipe and the bottom inner wall of first bottle lid to be the setting of screw thread column structure, thereby be convenient for install and change it, setting through the discharge opening, can rotate the back at the outer wall of first bottle lid and second bottle lid, take out gaseous phase method white carbon black after discharge opening and discharge gate overlap mutually, thereby the effectual gaseous phase method white carbon black that has avoided removing the sample storage tank spills, and can take out according to gram number, the accuracy of test result has been guaranteed.

2. This sample holds device for fumed silica performance test passes through the setting of third bottle lid, can dismantle the back with discharge mechanism and install the top at the discharging pipe, rotate between the outer wall of the inner wall that utilizes the third bottle lid and discharging pipe, the inside fumed silica who deposits of inner chamber can be mixed through the puddler that sets up, thereby avoid leading to the phenomenon production that fumed silica bonded because of the moisture gets into, can make the inside temperature of inner chamber rise through the heating pipe simultaneously, guarantee the drying of fumed silica.

3. This sample holds device for vapor phase method white carbon black performance test passes through the setting of flabellum, can be about carrying out clockwise rotation between the outer wall of switching axle and the main shaft, thereby reach the effect of ventilation, the spring has good shock attenuation, the antidetonation function, can effectually prevent to lead to the sample storage tank to damage because of dropping, the security and the stability of the device have been guaranteed, on being fixed in the desktop of workstation with the base, utilize the magnet to make the base can and the desktop between the structure more stable, establish the post with the cover and place on the top outer wall of base, thereby accomplish the location to the sample storage tank, the flexibility is strong, the sample storage tank appears droing when preventing the operation simultaneously.

Drawings

FIG. 1 is a schematic structural view of the present invention;

FIG. 2 is a schematic view of the internal structure of the present invention;

fig. 3 is a schematic view of the top view structure of the discharging mechanism of the present invention.

In the figure: 1. a sample storage tank; 2. a discharge pipe; 3. a discharging mechanism; 301. a first bottle cap; 302. a second bottle cap; 303. a discharge hole; 304. a discharge port; 4. a transmission mechanism; 401. a third bottle cap; 402. a single chip controller; 403. a joining block; 404. a stirring rod; 405. heating a tube; 5. an inner cavity; 6. a fixed block; 7. a spring; 8. a main shaft; 9. a transfer shaft; 10. a fan blade; 11. sleeving a column; 12. a base; 13. a magnet; 14. a vent hole; 15. and a limiting bulge.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-3, the present invention provides a technical solution: a sample containing device for testing white carbon black performance by a gas phase method comprises a sample storage tank 1, a discharge pipe 2, a discharge mechanism 3, a first bottle cap 301, a second bottle cap 302, a discharge hole 303, a discharge hole 304, a transmission mechanism 4, a third bottle cap 401, a single chip microcomputer controller 402, a connecting block 403, a stirring rod 404, a heating pipe 405, an inner cavity 5, a fixing block 6, a spring 7, a main shaft 8, a switching shaft 9, a fan blade 10, a sleeving column 11, a base 12, a magnet 13, a ventilation hole 14 and a limiting bulge 15, wherein the discharge pipe 2 is connected with the outer wall of the top end of the sample storage tank 1, the discharge mechanism 3 wraps the outer wall of the discharge pipe 2, the inner cavity 5 is arranged on the inner wall of the sample storage tank 1, the fixing block 6 is arranged on the outer wall of the left side of the inner cavity 5, the spring 7 is bonded on the outer wall of the bottom end of the fixing block 6, the, the fan blade 10 is connected with the outer wall of the left side of the transfer shaft 9, the sleeving column 11 is welded on the outer wall of the bottom end of the sample storage tank 1, the base 12 is arranged on the inner wall of the sleeving column 11, the magnet 13 is adhered on the outer wall of the bottom end of the base 12, the limiting bulge 15 is installed on the outer wall of the front end of the sample storage tank 1, the vent hole 14 is formed in the bottom of the outer wall of the front end of the sample storage tank 1, the transmission mechanism 4 is located at the top end of the discharge pipe 2, the discharge mechanism 3 comprises a first bottle cap 301, a second bottle cap 302, a discharge hole 303 and a discharge hole 304, the outer wall of the first bottle cap 301 is wrapped with the second bottle cap 302, the discharge hole 303 is formed in the outer wall of the top end of the second bottle cap 302, the discharge holes 304 are formed in the left side of the outer wall of the top end of the first bottle cap 301, the discharge holes 303 are distributed on the outer wall of the top end of, the outer wall of the discharge pipe 2 and the inner wall of the bottom end of the first bottle cap 301 are in a thread structure, so that the first bottle cap 301 and the second bottle cap 302 can be conveniently installed and replaced, and after the outer walls of the first bottle cap 301 and the second bottle cap 302 rotate through the arrangement of the discharge hole 303, the fumed silica can be taken out after the discharge hole 303 and the discharge hole 304 are overlapped, so that the fumed silica is effectively prevented from leaking when the sample storage tank 1 is moved, the fumed silica can be taken out according to gram number, and the accuracy of a test result is ensured;

the transmission mechanism 4 comprises a third bottle cap 401, a single chip microcomputer controller 402, a connecting block 403, a stirring rod 404 and a heating pipe 405, the single chip microcomputer controller 402 is installed in the middle of the top end of the third bottle cap 401, the connecting block 403 is welded in the middle of the bottom end of the third bottle cap 401, the stirring rod 404 is fixed on the outer wall of the right side of the connecting block 403, three heating pipes 405 are connected in the middle of the outer wall of the left side of the stirring rod 404, the three heating pipes 405 are symmetrically distributed on the center of the outer wall of the heating pipe 405, the stirring rod 404, the heating pipe 405 and the connecting block 403 are of a welding integrated structure, the discharging mechanism 3 can be installed at the top end of the discharging pipe 2 after being detached through the arrangement of the third bottle cap 401, the inner wall of the third bottle cap 401 and the outer wall of the discharging pipe 2 are rotated, and fumed silica stored in the inner cavity 5 can, thereby avoiding the bonding phenomenon of fumed silica caused by moisture, simultaneously, the temperature in the inner cavity 5 can be raised through the heating pipe 405, the drying of fumed silica is ensured, the fan blades 10 are distributed in an annular shape relative to the outer wall of the adapter shaft 9, the fan blades 10 form a rotating structure with the main shaft 8 through the adapter shaft 9, and the clockwise rotation can be carried out between the outer wall of the adapter shaft 9 and the main shaft 8 through the arrangement of the fan blades 10, thereby achieving the ventilation effect, the springs 7 are distributed around the outer wall of the inner cavity 5 at equal intervals, the inner cavity 5, the fixed block 6, the springs 7 and the sample storage tank 1 are tightly attached, the springs 7 have good shock absorption and shock resistance functions, the damage of the sample storage tank 1 caused by dropping can be effectively prevented, the safety and the stability of the device are ensured, the outer wall of the top end of the magnet 13 is fixedly connected with the outer wall of the bottom end of the base, and sample storage tank 1 establishes post 11 and base 12 through the cover and constitutes the active structure, through on being fixed in the desktop of workstation with base 12, utilizes magnet 13 to make base 12 can and the desktop between the structure more stable, establishes post 11 with the cover and places on the top outer wall of base 12 to accomplish the location to sample storage tank 1, the flexibility is strong, prevents that sample storage tank 1 from appearing droing during the operation simultaneously.

The working principle is as follows: for the sample containing device for the fumed silica performance test, firstly, fumed silica is placed in the inner cavity 5 in advance, the discharging mechanism 3 can be installed at the top end of the discharging pipe 2 after being detached by the arrangement of the third bottle cap 401, the fumed silica stored in the inner cavity 5 can be mixed by the arranged stirring rod 404 by utilizing the rotation between the inner wall of the third bottle cap 401 and the outer wall of the discharging pipe 2, so that the generation of the phenomenon of bonding of the fumed silica caused by moisture entering is avoided, meanwhile, the temperature in the inner cavity 5 can be increased by the heating pipe 405, the drying of the fumed silica is ensured, the heating pipe 405 is controlled by the single chip microcomputer controller 402, the purpose of controlling the temperature is achieved, the clockwise rotation between the outer wall of the adapter shaft 9 and the main shaft 8 can be realized by the arrangement of the fan blades 10, the moisture can be discharged from the vent hole 14, thereby achieving the ventilation effect, the base 12 and the magnet 13 are fixed, the base 12 and the top surface of the workbench are fixed, the sleeve column 11 and the base 12 are matched with each other, so that the sample storage tank 1 can be fixed with the workbench, the flexibility is strong, the sample storage tank 1 is prevented from falling off during operation, the spring 7 has good shock absorption and shock resistance functions, the sample storage tank 1 can be effectively prevented from being damaged due to falling off, the safety and the stability of the device are ensured, the outer wall of the discharge pipe 2 and the inner wall of the bottom end of the first bottle cap 301 are arranged in a thread structure during use, so that the installation and replacement of the device are convenient, the gas phase method white carbon black can be taken out after the outer walls of the first bottle cap 301 and the second bottle cap 302 rotate through the arrangement of the discharge hole 303 and the discharge hole 304 are overlapped, thereby effectively avoiding the gas phase method white carbon black from leaking when the sample storage tank 1 is moved, and can take out according to gram number, guarantee the accuracy of test result, spacing arch 15 that the outer wall of sample holding tank 1 evenly set up can play the effect of protection when sample holding tank 1 falls to the ground, has prolonged the device's life.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a vapor phase method white carbon black performance test holds device with sample, includes that the sample deposits jar (1) and drive mechanism (4), its characterized in that: the sample storage tank is characterized in that the outer wall of the top end of the sample storage tank (1) is connected with a discharge pipe (2), the outer wall of the discharge pipe (2) is wrapped with a discharge mechanism (3), the inner wall of the sample storage tank (1) is provided with an inner cavity (5), the outer wall of the left side of the inner cavity (5) is provided with a fixed block (6), the outer wall of the bottom end of the fixed block (6) is bonded with a spring (7), the middle part of the bottom end of the inner cavity (5) is fixed with a main shaft (8), the middle part of the outer wall of the main shaft (8) is wrapped with a transfer shaft (9), the outer wall of the left side of the transfer shaft (9) is bonded with a fan blade (10), the outer wall of the bottom end of the sample storage tank (1) is welded with a sleeve-arranged column (11), the inner wall of the sleeve-arranged column (11) is provided with a base (12), and the bottom of the outer wall of the front end of the sample storage tank (1) is provided with a vent hole (14), and the transmission mechanism (4) is positioned at the top end of the discharge pipe (2).

2. The sample containing device for the fumed silica performance test according to claim 1, characterized in that: discharge mechanism (3) include first bottle lid (301), second bottle lid (302), discharge opening (303) and discharge gate (304), and the outer wall parcel of first bottle lid (301) has second bottle lid (302), discharge opening (303) have been seted up to the top outer wall of second bottle lid (302), the top outer wall left side of first bottle lid (301) is provided with discharge gate (304).

3. The sample containing device for the fumed silica performance test according to claim 2, characterized in that: the discharge holes (303) are distributed on the outer wall of the top end of the second bottle cap (302) at equal intervals, the bottom end of the inner wall of the first bottle cap (301) is of a thread-shaped structure, and the second bottle cap (302) is tightly attached to the inner wall of the first bottle cap (301).

4. The sample containing device for the fumed silica performance test according to claim 1, characterized in that: drive mechanism (4) include third bottle lid (401), single chip microcomputer controller (402), link up piece (403), puddler (404) and heating pipe (405), and the top mid-mounting of third bottle lid (401) has single chip microcomputer controller (402), the welding of the bottom middle part of third bottle lid (401) has link up piece (403), and the right side outer wall that links up piece (403) is fixed with puddler (404), heating pipe (405) have been linked up in the middle part of the left side outer wall of puddler (404).

5. The sample containing device for the fumed silica performance test according to claim 4, characterized in that: the heating pipe (405) is provided with three, and puddler (404) are the symmetric distribution about the outer wall central point of heating pipe (405), and for welding integrated structure between puddler (404), heating pipe (405) and linking piece (403).

6. The sample containing device for the fumed silica performance test according to claim 1, characterized in that: the fan blades (10) are distributed in an annular shape around the outer wall of the transfer shaft (9), and the fan blades (10) and the main shaft (8) form a rotating structure through the transfer shaft (9).

7. The sample containing device for the fumed silica performance test according to claim 1, characterized in that: the springs (7) are equidistantly distributed around the outer wall of the inner cavity (5), and the inner cavity (5), the fixed block (6), the springs (7) and the sample storage tank (1) are tightly attached.

8. The sample containing device for the fumed silica performance test according to claim 1, characterized in that: the outer wall of the top end of the magnet (13) is fixedly connected with the outer wall of the bottom end of the base (12), and the sample storage tank (1) and the base (12) form a movable structure through the sleeved column (11).