CN211800799U - Double-layer glass reaction kettle device for producing bendazac lysine bulk drug - Google Patents
Double-layer glass reaction kettle device for producing bendazac lysine bulk drug Download PDFInfo
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- CN211800799U CN211800799U CN202020029761.0U CN202020029761U CN211800799U CN 211800799 U CN211800799 U CN 211800799U CN 202020029761 U CN202020029761 U CN 202020029761U CN 211800799 U CN211800799 U CN 211800799U
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- Prior art keywords
- glass layer
- layer
- reaction kettle
- steel ring
- double
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- 239000011521 glass Substances 0.000 title claims abstract description 51
- 229940079593 drug Drugs 0.000 title claims abstract description 14
- 239000003814 drug Substances 0.000 title claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 title claims description 20
- 229960005149 bendazac Drugs 0.000 title claims description 10
- BYFMCKSPFYVMOU-UHFFFAOYSA-N bendazac Chemical compound C12=CC=CC=C2C(OCC(=O)O)=NN1CC1=CC=CC=C1 BYFMCKSPFYVMOU-UHFFFAOYSA-N 0.000 title claims description 10
- 239000007788 liquid Substances 0.000 claims abstract description 20
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 244000309464 bull Species 0.000 claims abstract description 6
- 238000004519 manufacturing process Methods 0.000 claims abstract description 6
- 239000010410 layer Substances 0.000 claims description 46
- 239000011229 interlayer Substances 0.000 claims description 28
- 238000004140 cleaning Methods 0.000 claims description 25
- 229910000831 Steel Inorganic materials 0.000 claims description 24
- 239000010959 steel Substances 0.000 claims description 24
- 238000009434 installation Methods 0.000 claims description 5
- 230000006978 adaptation Effects 0.000 claims description 2
- 238000003466 welding Methods 0.000 claims description 2
- 238000009826 distribution Methods 0.000 claims 1
- 239000004519 grease Substances 0.000 abstract description 5
- GFQYFRTWQLDRCH-LBPRGKRZSA-N (2s)-6-amino-2-(benzylamino)hexanoic acid Chemical compound NCCCC[C@@H](C(O)=O)NCC1=CC=CC=C1 GFQYFRTWQLDRCH-LBPRGKRZSA-N 0.000 abstract description 2
- 238000005406 washing Methods 0.000 abstract 4
- 238000010030 laminating Methods 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 2
- 239000004472 Lysine Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model relates to a reation kettle technical field, concretely relates to double glazing reation kettle device of benzyl lysine bulk drug production usefulness, which comprises a bracket, the inside of support is equipped with the reation kettle body of constituteing by outer glass layer and interior glass layer, be equipped with the intermediate layer between outer glass layer and the interior glass layer, interbedded inside top is provided with the washing liquid pipe of loop configuration, and the bottom of washing liquid pipe is provided with the nozzle that is the annular and distributes, the motor is installed on the top of support, the bull stick is installed to the output shaft tip of motor, and the bottom of bull stick passes the inside that outer glass layer and intermediate layer extend to interior glass layer and install the stirring leaf, loop configuration's carousel is installed on the top of interior glass layer. The utility model overcomes prior art's is not enough, through the starter motor, because the both sides of scraper blade and interbedded inner wall laminating, the grease on the interbedded inner wall can be struck off to scraper blade cooperation washing liquid, need not artifical manual washing, labour saving and time saving.
Description
Technical Field
The utility model relates to a reation kettle technical field, concretely relates to double glazing reation kettle device of production usefulness of benzyda lysine bulk drug.
Background
The double-layer glass reaction kettle is designed by double-layer glass, reaction solvent is placed in the inner layer to carry out stirring reaction, and different cold and heat sources can be introduced into the interlayer to carry out circulating heating or cooling reaction. The stirring reaction can be carried out under the condition of normal pressure or negative pressure in a closed glass reactor under the condition of set constant temperature according to the use requirement, and the device is ideal pilot-plant test and production equipment for modern fine factories, biological pharmacy and new material synthesis.
However, most of the existing cold and heat sources are oily materials, and after the interlayer in the traditional double-layer glass reaction kettle passes through the cold and heat sources, grease is easily adhered to the inner wall of the interlayer, so that manual cleaning is troublesome, and the cleaning speed is slow.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
The utility model provides a double glazing reation kettle device of benzyl lysine bulk drug production usefulness, overcome the not enough of prior art, structural design is simple, and the effectual grease of having solved is glutinous easily on intermediate layer inner wall, and the manual cleaning is comparatively troublesome, the slow problem of cleaning speed.
(II) technical scheme
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes:
a double-layer glass reaction kettle device for producing a bendazac lysine bulk drug comprises a support, wherein a reaction kettle body consisting of an outer glass layer and an inner glass layer is arranged inside the support, an interlayer is arranged between the outer glass layer and the inner glass layer, a cleaning liquid pipe of an annular structure is arranged at the top end inside the interlayer, a nozzle distributed in an annular shape is arranged at the bottom end of the cleaning liquid pipe, a motor is installed at the top end of the support, a rotating rod is installed at the end part of an output shaft of the motor, the bottom end of the rotating rod penetrates through the outer glass layer and the interlayer to extend to the inside of the inner glass layer and is provided with stirring blades, a turntable of the annular structure is installed at the top end of the inner glass layer, the rotating rod is located on a central axis of the turntable, a steel ring is installed at the top end of the turntable, connecting rods symmetrically arranged are welded on the outer wall of the, the bull stick is located the inside section outer wall of steel ring and has cup jointed the driving gear, the inner circle wall of steel ring is provided with the internal tooth, the top on outer glass layer is provided with the installation sleeve, and installs telescopic inside and peg graft and have the regulation pole, and the bottom of adjusting the pole extends to the inside of steel ring and installs driven gear.
Preferably, the bottom end of the outer glass layer is provided with a discharge hole communicated with the inner glass layer.
Preferably, the scraper blade is located the interbedded inside, and the upper segment of scraper blade is vertical form, and the hypomere of scraper blade is the arc structure, the width of scraper blade and interbedded width looks adaptation, set up the chute that the equidistance distributes on the lateral wall of scraper blade.
Preferably, notches at two ends of the inclined groove are respectively positioned on the same vertical surface with the side wall of the scraper.
Preferably, the driven gear is meshed with the driving gear and the internal teeth.
Preferably, the top of reation kettle body is provided with the inlet pipe, and the bottom of inlet pipe runs through in the inside of steel ring, leave the clearance between inlet pipe and the driving gear.
(III) advantageous effects
The embodiment of the utility model provides a double glazing reation kettle device of benzyl da lysine bulk drug production usefulness possesses following beneficial effect:
the novel structure design is flexible, when the inner wall of the interlayer needs to be cleaned, the adjusting rod extends downwards to enable the driven gear at the bottom end of the adjusting rod to move between the driving gear and the inner teeth, cleaning liquid in the cleaning liquid pipe is sprayed to the inner wall of one side of the interlayer through the nozzle, the cleaning liquid flows downwards along the inner wall of the interlayer, the rotating rod is driven to rotate by the starting motor, the rotating rod drives the driving gear to rotate, the driving gear drives the driven gear to rotate, the driven gear drives the steel ring to rotate through the inner teeth, the steel ring drives the scraper to rotate through the connecting rod, the scraper is attached to the inner wall of the interlayer by two sides of the scraper, the scraper can scrape grease on the inner wall of the interlayer by matching with the cleaning liquid, manual cleaning is not needed, time and labor are saved, and when cleaning is not needed, the adjusting rod, the adjusting rod is fixed, the rotating rod can be guaranteed to be tightly driven to rotate the stirring blades to stir, and the whole device is simple to operate and convenient to use.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of a partial top view of the present invention;
fig. 3 is an enlarged schematic view of part a of the present invention.
In the figure: the device comprises a support 1, an outer glass layer 2, an inner glass layer 3, an interlayer 4, a cleaning liquid pipe 5, a nozzle 6, a motor 7, a rotating rod 8, a stirring blade 9, a rotating disc 10, a steel ring 11, a connecting rod 12, a scraping plate 13, a chute 14, a driving gear 15, internal teeth 16, a mounting sleeve 17, an adjusting rod 18, a driven gear 19 and a feeding pipe 20.
Detailed Description
The invention will be further described with reference to the following figures 1-3 and examples:
a double-layer glass reaction kettle device for producing a bendazac lysine bulk drug comprises a support 1, wherein a reaction kettle body consisting of an outer glass layer 2 and an inner glass layer 3 is arranged inside the support 1, an interlayer 4 is arranged between the outer glass layer 2 and the inner glass layer 3, the interlayer 4 can be used for circulating heating or cooling reaction through different cold and heat sources, a cleaning liquid pipe 5 of an annular structure is arranged at the top end inside the interlayer 4, nozzles 6 which are distributed annularly are arranged at the bottom end of the cleaning liquid pipe 5, so that cleaning liquid can be sprayed to the inner wall of the interlayer 4 conveniently, a motor 7 is arranged at the top end of the support 1, a rotating rod 8 is arranged at the end part of an output shaft of the motor 7, the bottom end of the rotating rod 8 penetrates through the outer glass layer 2 and the interlayer 4 to extend into the inner glass layer 3 and is provided with stirring blades 9, a rotating disk 10 of an annular structure is arranged at the top end of the inner, the utility model discloses a glass transition piece, including carousel 10, bull stick 8, steel ring 11, connecting rod 12, regulation pole 18, driven gear 19, the bottom of regulation pole 18 extends to the inside of steel ring 11 and installs, and the outer wall welding of steel ring 11 has two connecting rods 12 that the symmetry set up, and the one end that steel ring 11 was kept away from to connecting rod 12 is provided with scraper blade 13, bull stick 8 is located steel ring 11's inside section outer wall and has cup jointed driving gear 15, steel ring 11's inner circle wall is provided with internal tooth 16, the top of outer glass layer 2 is provided with installation sleeve 17, and the inside of installation sleeve 17 is pegged graft and is had regulation pole 18, and.
In this embodiment, as shown in fig. 1, a discharge hole communicated with the inner glass layer 3 is formed at the bottom end of the outer glass layer 2, so that the discharging is facilitated.
In this embodiment, as shown in fig. 1, the scraper 13 is located inside the interlayer 4, an upper section of the scraper 13 is vertical, a lower section of the scraper 13 is an arc-shaped structure, a width of the scraper 13 is adapted to a width of the interlayer 4, and the side wall of the scraper 13 is provided with chutes 14 distributed at equal intervals, so that the cleaning solution can flow into the inner wall of the other side of the interlayer 4 along the chutes 14 to be sufficiently cleaned by matching with the scraper 13.
In this embodiment, as shown in fig. 1, the notches at the two ends of the chute 14 are respectively located on the same vertical plane with the side wall of the scraper 13, so as to facilitate the circulation of the cleaning liquid.
In this embodiment, as shown in fig. 1-2, the driven gear 19 is engaged with the driving gear 15 and the internal teeth 16, so as to form linkage.
In this embodiment, as shown in fig. 1 and 3, a feeding pipe 20 is disposed at the top end of the reaction kettle body, and the bottom end of the feeding pipe 20 penetrates through the inside of the steel ring 11, and a gap is left between the feeding pipe 20 and the driving gear 15.
The utility model discloses a theory of operation: when the inner wall of the interlayer 4 needs to be cleaned, the adjusting rod 18 extends downwards, the driven gear 19 at the bottom end of the adjusting rod 18 moves between the driving gear 15 and the inner teeth 16, cleaning liquid in the cleaning liquid pipe 5 is sprayed to the inner wall of one side of the interlayer 4 through the nozzle 6, the cleaning liquid flows downwards along the inner wall of the interlayer 4, the motor 7 is started, the rotating rod 8 is driven to rotate, the rotating rod 8 drives the driving gear 15 to rotate, the driving gear 15 drives the driven gear 19 to rotate, the driven gear 19 drives the steel ring 11 to rotate through the inner teeth 16, the steel ring 11 drives the scraper 13 to rotate through the connecting rod 12, as the two sides of the scraper 13 are attached to the inner wall of the interlayer 4, the scraper 13 can scrape off grease on the inner wall of the interlayer 4 by matching with the cleaning liquid, manual cleaning is not needed, time and labor are saved, and when, the driven gear 19 is separated from the driving gear 15 and the internal teeth 16 to form no linkage, and then the adjusting rod 18 is fixed, so that the rotating rod 8 can be ensured to tightly drive the stirring blades 9 to rotate for stirring.
The embodiment of the present invention discloses a preferred embodiment, but not limited thereto, and those skilled in the art can easily understand the spirit of the present invention according to the above embodiment, and make different extensions and changes, but do not depart from the spirit of the present invention, all of which are within the protection scope of the present invention.
Claims (6)
1. The utility model provides a double glazing reation kettle device of production usefulness of bendazac lysine bulk drug, includes support (1), its characterized in that: the reaction kettle comprises a support (1), wherein a reaction kettle body consisting of an outer glass layer (2) and an inner glass layer (3) is arranged in the support (1), an interlayer (4) is arranged between the outer glass layer (2) and the inner glass layer (3), a cleaning liquid pipe (5) of an annular structure is arranged at the top end of the interlayer (4), a nozzle (6) which is distributed in an annular shape is arranged at the bottom end of the cleaning liquid pipe (5), a motor (7) is installed at the top end of the support (1), a rotating rod (8) is installed at the end part of an output shaft of the motor (7), the bottom end of the rotating rod (8) penetrates through the outer glass layer (2) and the interlayer (4) to extend to the inside of the inner glass layer (3) and is provided with stirring blades (9), a turntable (10) of the annular structure is installed at the top end of the inner glass layer (3), the rotating rod (8) is located on the central axis of the turntable (10), and a steel ring, the outer wall welding of steel ring (11) has connecting rod (12) that two symmetries set up, and connecting rod (12) keep away from the one end of steel ring (11) and be provided with scraper blade (13), bull stick (8) are located the inside section outer wall cup joint driving gear (15) of steel ring (11), the inner circle wall of steel ring (11) is provided with internal tooth (16), the top of outer glass layer (2) is provided with installation sleeve (17), and the inside of installation sleeve (17) is pegged graft and is had regulation pole (18), and the bottom of adjusting pole (18) extends to the inside of steel ring (11) and installs driven gear (19).
2. The double-layer glass reaction kettle device for producing the bendazac lysine bulk drug according to claim 1, characterized in that: the bottom of the outer glass layer (2) is provided with a discharge hole communicated with the inner glass layer (3).
3. The double-layer glass reaction kettle device for producing the bendazac lysine bulk drug according to claim 1, characterized in that: the scraper blade (13) is located the inside of intermediate layer (4), and the upper segment of scraper blade (13) is vertical form, and the hypomere of scraper blade (13) is the arc structure, the width of scraper blade (13) and the width looks adaptation of intermediate layer (4), set up equidistant distribution's chute (14) on the lateral wall of scraper blade (13).
4. The double-layer glass reaction kettle device for producing the bendazac lysine bulk drug according to claim 3, characterized in that: notches at two ends of the inclined groove (14) are respectively positioned on the same vertical surface with the side wall of the scraper (13).
5. The double-layer glass reaction kettle device for producing the bendazac lysine bulk drug according to claim 1, characterized in that: the driven gear (19) is meshed with the driving gear (15) and the internal teeth (16).
6. The double-layer glass reaction kettle device for producing the bendazac lysine bulk drug according to claim 1, characterized in that: the top of reation kettle body is provided with inlet pipe (20), and the bottom of inlet pipe (20) runs through in the inside of steel ring (11), leave the clearance between inlet pipe (20) and driving gear (15).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020029761.0U CN211800799U (en) | 2020-01-07 | 2020-01-07 | Double-layer glass reaction kettle device for producing bendazac lysine bulk drug |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020029761.0U CN211800799U (en) | 2020-01-07 | 2020-01-07 | Double-layer glass reaction kettle device for producing bendazac lysine bulk drug |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN211800799U true CN211800799U (en) | 2020-10-30 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202020029761.0U Expired - Fee Related CN211800799U (en) | 2020-01-07 | 2020-01-07 | Double-layer glass reaction kettle device for producing bendazac lysine bulk drug |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN211800799U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113651713A (en) * | 2021-08-19 | 2021-11-16 | 宁夏中盛新科技有限公司 | Synthesis method of high-purity 2-nitro-4-acetamino anisole |
| CN113823204A (en) * | 2021-08-27 | 2021-12-21 | 胡娟 | Intelligent advertisement marketing and delivering device and method |
-
2020
- 2020-01-07 CN CN202020029761.0U patent/CN211800799U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113651713A (en) * | 2021-08-19 | 2021-11-16 | 宁夏中盛新科技有限公司 | Synthesis method of high-purity 2-nitro-4-acetamino anisole |
| CN113651713B (en) * | 2021-08-19 | 2024-05-14 | 宁夏中盛新科技有限公司 | Synthesis method of high-purity 2-nitro-4-acetamido anisole |
| CN113823204A (en) * | 2021-08-27 | 2021-12-21 | 胡娟 | Intelligent advertisement marketing and delivering device and method |
| CN113823204B (en) * | 2021-08-27 | 2024-01-12 | 北京基智科技有限公司 | Intelligent advertisement marketing and delivering equipment and delivering method |
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|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20201030 |
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| CF01 | Termination of patent right due to non-payment of annual fee |