CN211611655U - Crude glycerin-based microwave distillation device convenient for self-cleaning - Google Patents
Crude glycerin-based microwave distillation device convenient for self-cleaning Download PDFInfo
- Publication number
- CN211611655U CN211611655U CN201922266339.7U CN201922266339U CN211611655U CN 211611655 U CN211611655 U CN 211611655U CN 201922266339 U CN201922266339 U CN 201922266339U CN 211611655 U CN211611655 U CN 211611655U
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- Prior art keywords
- distillation
- fixed mounting
- case
- connecting pipe
- sanitizer
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- 238000004821 distillation Methods 0.000 title claims abstract description 133
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title claims abstract description 64
- 238000004140 cleaning Methods 0.000 title claims abstract description 34
- 235000011187 glycerol Nutrition 0.000 title claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 67
- 239000012153 distilled water Substances 0.000 claims abstract description 27
- 238000003756 stirring Methods 0.000 claims abstract description 20
- 239000012459 cleaning agent Substances 0.000 claims description 23
- 238000003860 storage Methods 0.000 claims description 17
- 238000007789 sealing Methods 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 239000004744 fabric Substances 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 6
- 238000005406 washing Methods 0.000 abstract description 2
- 239000003599 detergent Substances 0.000 description 12
- 238000007599 discharging Methods 0.000 description 6
- 238000009835 boiling Methods 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 239000000284 extract Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 238000010977 unit operation Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
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- Detergent Compositions (AREA)
- Cleaning By Liquid Or Steam (AREA)
Abstract
The utility model discloses a microwave distillation plant based on crude glycerine convenient to automatically cleaning, including the distillation case, the inside bottom fixed mounting of distillation case has the cushion, the up end fixed mounting of cushion has distillation container, the middle fixed mounting at distillation container top has the feed inlet. According to the crude glycerin microwave-based distillation device convenient for self cleaning, microwaves can be emitted through the arranged magnetron, the microwaves penetrate through the distillation container to heat crude glycerin in the distillation container, the crude glycerin is heated in a microwave heating mode, the microwaves can heat the inside of the distillation container, and the heating effect is improved; adopt the sanitizer case to save the sanitizer, the inside of sanitizer case is provided with the stirring rake simultaneously, mixes the stirring to the sanitizer, prevents to deposit, and after the distillation container finishes through the sanitizer washing, rethread distilled water washes for the distillation container can be by the cleaner that washes, improves the cleaning performance, and clean effectual, convenient to use.
Description
Technical Field
The utility model relates to a distillation plant technical field specifically is a be convenient for automatically cleaning based on crude glycerine microwave distillation plant.
Background
Distillation is a thermodynamic separation process that utilizes the difference in boiling points of components in a mixed liquid or liquid-solid system to vaporize lower boiling components and recondense to separate the entire component, a unit operation that combines the two unit operations of evaporation and condensation.
The crude glycerine is required to be distilled in the production and processing process, but the crude glycerine is generally heated under normal pressure at present, and is not heated in a vacuum environment, so that the boiling point is higher, the distillation time is longer, the distillation efficiency is reduced, and meanwhile, the crude glycerine distillation device is difficult to clean and inconvenient to use after the distillation is finished.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a be convenient for automatically cleaning based on crude glycerine microwave distillation plant to it generally heats under the ordinary pressure to propose present crude glycerine in the above-mentioned background art, does not heat in vacuum environment, leads to the boiling point higher, makes the time of distillation longer, has reduced the efficiency of distillation, and simultaneously, present crude glycerine distillation plant is after the distillation is finished, is difficult to wash distillation plant, the problem of being not convenient for to use.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a be convenient for automatically cleaning based on crude glycerine microwave distillation plant, includes the distillation case, the inside bottom fixed mounting of distillation case has the cushion, the up end fixed mounting of cushion has the distillation container, the middle fixed mounting at distillation container top has the feed inlet, the feed inlet upwards extends to the outside of distillation case, the inside top fixed mounting of distillation case has the agitator, the inside right side of distillation case is from last to having transformer, rectifier and magnetron down fixed mounting in proper order, transformer electric connection has power plug, the inside fixed mounting of distillation container has the scavenge pipe, a plurality of hole spouts have been seted up to the intensive cloth on the scavenge pipe.
Preferably, the left side fixed mounting of distillation case up end has the vacuum pump, the one end of extraction opening fixedly connected with exhaust tube of vacuum pump, the other end of exhaust tube passes the distillation case and extends to the inside of distillation container, the left side fixed mounting of distillation case has the manometer, the manometer communicates with each other with the distillation container is inside, the bottom fixed mounting of distillation container has the discharge gate, the discharge gate extends to the bottom of distillation case, fixed mounting has ejection of compact valve on the discharge gate.
Preferably, the left side of distillation case is provided with the sanitizer case, the top fixed mounting of sanitizer case has agitator motor, the inside of sanitizer case is provided with the stirring rake, the upper end of stirring rake and agitator motor's output shaft fixed connection, the left side fixed mounting of sanitizer case up end has the sanitizer to add the mouth, the bottom fixed mounting of sanitizer case has the sanitizer discharge port.
Preferably, the detergent discharge port is connected with one end of a first connecting pipe, the other end of the first connecting pipe is connected with a water inlet of a first water pump, an outlet of the first water pump is connected with one end of a second connecting pipe, the other end of the second connecting pipe is fixedly connected with the left end of the cleaning pipe in a sealing manner, and a first ball valve is fixedly mounted on the second connecting pipe.
Preferably, the right side of distillation tank is provided with distilled water storage jar, the one end of the top fixedly connected with distillation column of distilled water storage jar, the other end of distillation column passes the inside that the distillation tank extends to distillation container, the bottom fixed mounting of distilled water storage jar has the delivery port, the delivery port is connected with the one end of connecting pipe three, the other end fixed mounting of connecting pipe three is at the water inlet of water pump two, the one end of outlet fixedly connected with connecting pipe four of water pump two, the other end of connecting pipe four and the right-hand member sealing fixed connection of scavenge pipe, fixed mounting has ball valve two on the connecting pipe four.
Compared with the prior art, the beneficial effects of the utility model are that:
1. according to the crude glycerin microwave-based distillation device convenient for self cleaning, microwaves can be emitted through the arranged magnetron, the microwaves penetrate through the distillation container to heat crude glycerin in the distillation container, the crude glycerin is heated in a microwave heating mode, the microwaves can heat the inside of the distillation container, and the heating effect is improved;
2. this be convenient for automatically cleaning based on crude glycerine microwave distillation device, adopt the sanitizer case to save the sanitizer, the inside of sanitizer case is provided with the stirring rake simultaneously, mix the stirring to the sanitizer, prevent to deposit, improve clean effect, save distilled water through distilled water storage jar simultaneously, after the distilled container finishes through the sanitizer washing, rethread distilled water washes for distilled container can be by the cleaner that washes, improve the cleaning performance, clean effectual, convenient to use.
Drawings
FIG. 1 is a schematic perspective view of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
FIG. 3 is a schematic side view of the present invention;
fig. 4 is a schematic view of the structure of the cleaning tube of the present invention.
In the figure: 1. a distillation box; 2. cushion blocks; 3. a distillation vessel; 4. a feed inlet; 5. a stirrer; 6. a transformer; 7. a power plug; 8. a rectifier; 9. a magnetron; 10. a vacuum pump; 11. an air exhaust pipe; 12. a discharge port; 13. a discharge valve; 14. a pressure gauge; 15. a detergent tank; 16. a stirring motor; 17. a stirring paddle; 18. a detergent addition port; 19. a detergent discharge port; 20. a first connecting pipe; 21. a first water pump; 22. a second connecting pipe; 23. a first ball valve; 24. cleaning the tube; 25. a distillation tube; 26. a distilled water storage tank; 27. a water outlet; 28. a third connecting pipe; 29. a second water pump; 30. a fourth connecting pipe; 31. and a second ball valve.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-4, the present invention provides a technical solution: a microwave distillation device convenient for self-cleaning and based on crude glycerin comprises a distillation box 1, a cushion block 2, a distillation container 3, a feed inlet 4, a stirrer 5, a transformer 6, a power plug 7, a rectifier 8, a magnetron 9, a vacuum pump 10, an exhaust tube 11, a discharge port 12, a discharge valve 13, a pressure gauge 14, a detergent box 15, a stirring motor 16, a stirring paddle 17, a detergent adding port 18, a detergent discharge port 19, a connecting tube I20, a water pump I21, a connecting tube II 22, a ball valve I23, a cleaning tube 24, a distillation tube 25, a distilled water storage tank 26, a water outlet 27, a connecting tube III 28, a water pump II 29, a connecting tube IV 30 and a ball valve II 31, wherein the cushion block 2 is fixedly installed at the bottom inside the distillation box 1, the distillation container 3 is fixedly installed on the upper end face of the cushion block 2, the feed inlet 4 is fixedly installed in the middle of the top of the distillation, the inside top fixed mounting of distillation box 1 has agitator 5, distillation box 1 inside right side is from last to having transformer 6 down fixed mounting in proper order, rectifier 8 and magnetron 9, 6 electric connection of transformer has power plug 7, distillation container 3's inside fixed mounting has scavenge pipe 24, a plurality of hole for water sprayings have been seted up to the last densely covered of scavenge pipe 24, send the microwave through magnetron 9, magnetron 9 passes distillation container 3 and heats the inside crude glycerine of distillation container 3, the mode that adopts microwave heating heats crude glycerine, the microwave can carry out the internal heating, improve the heating effect.
Further, the left side fixed mounting of distillation case 1 up end has vacuum pump 10, the one end of extraction opening fixedly connected with exhaust tube 11 of vacuum pump 10, the other end of exhaust tube 11 passes distillation case 1 and extends to the inside of distillation container 3, the left side fixed mounting of distillation case 1 has manometer 14, manometer 14 communicates with each other with distillation container 3 is inside, distillation container 3's bottom fixed mounting has discharge gate 12, discharge gate 12 extends to the bottom of distillation case 1, fixed mounting has ejection of compact valve 13 on discharge gate 12, the inside evacuation of distillation container 3 through vacuum pump 10, observe the inside pressure of distillation container 3 through manometer 14, vacuum heating can reduce the distillation temperature of crude glycerine, shorten the distillation time, accelerate distillation's efficiency greatly, through the distilled extraction material of discharge gate 12 discharge.
Furthermore, a cleaning agent box 15 is arranged on the left side of the distillation box 1, a stirring motor 16 is fixedly mounted at the top of the cleaning agent box 15, a stirring paddle 17 is arranged inside the cleaning agent box 15, the upper end of the stirring paddle 17 is fixedly connected with an output shaft of the stirring motor 16, a cleaning agent adding port 18 is fixedly mounted on the left side of the upper end face of the cleaning agent box 15, a cleaning agent discharging port 19 is fixedly mounted at the bottom of the cleaning agent box 15, cleaning agent is injected into the cleaning agent box 15 through the cleaning agent adding port 18, the stirring motor 16 is started to drive the stirring paddle 17 to rotate, the cleaning agent is mixed, the cleaning agent is prevented from precipitating, and the cleaning effect is improved.
Furthermore, the detergent discharge port 19 is connected with one end of a first connecting pipe 20, the other end of the first connecting pipe 20 is connected with a water inlet of a first water pump 21, an outlet of the first water pump 21 is connected with one end of a second connecting pipe 22, the other end of the second connecting pipe 22 is fixedly connected with the left end of the cleaning pipe 24 in a sealing manner, a first ball valve 23 is fixedly mounted on the second connecting pipe 22, the first water pump 21 extracts detergent in the detergent box 15 through the first connecting pipe 20 and discharges the detergent into the cleaning pipe 24 through the second connecting pipe 22, and finally the detergent is sprayed out through a water spray port on the cleaning pipe 24 to flush the inside of the distillation container 3.
Further, a distilled water storage tank 26 is arranged on the right side of the distillation box 1, one end of a distillation pipe 25 is fixedly connected to the top of the distilled water storage tank 26, the other end of the distillation pipe 25 penetrates through the distillation box 1 and extends into the distillation container 3, a water outlet 27 is fixedly arranged at the bottom of the distilled water storage tank 26, the water outlet 27 is connected with one end of a connecting pipe III 28, the other end of the connecting pipe III 28 is fixedly arranged at the water inlet of a water pump II 29, the outlet of the water pump II 29 is fixedly connected with one end of a connecting pipe IV 30, the other end of the connecting pipe IV 30 is fixedly connected with the right end of the cleaning pipe 24 in a sealing manner, a ball valve II 31 is fixedly arranged on the connecting pipe IV 30, distilled gas in the distillation container 3 is discharged into the distilled water storage tank 26 through the distillation pipe 25 and is collected into distilled water, the distilled water is, start two water pumps 29, open two 31 of ball valves, close one 23 of ball valves, two 29 of water pumps extract distilled water through three 28 of connecting pipes, and in the scavenge pipe 24 was discharged into to the connecting pipe four 30 of rethread, the inside of distillation vessel 3 was washed through the water jet on the scavenge pipe 24, and distilled water storage jar 26 can add external water source simultaneously for distillation vessel 3 can be by the cleaner who washes, improves the cleaning performance.
The working principle is as follows: firstly, adding crude glycerin into a distillation container 3 through a feeding hole 4, then closing the feeding hole 4, vacuumizing the interior of the distillation container 3 through a vacuum pump 10, observing the pressure in the distillation container 3 through a pressure gauge 14, reducing the distillation temperature of the crude glycerin through vacuum heating, shortening the distillation time, greatly accelerating the distillation efficiency, connecting a power plug 7 with an external power supply, emitting microwaves through a magnetron 9, heating the crude glycerin in the distillation container 3 through the distillation container 3 by the magnetron 9, discharging the distilled gas in the distillation container 3 into a distilled water storage tank 26 through a distillation pipe 25, collecting the distilled water, storing the distilled water through the distilled water storage tank 26, discharging the distilled extracted materials through a discharging hole 12 after the distillation is finished, and then cleaning the distillation container 3, injecting a cleaning agent into the cleaning agent box 15 through a cleaning agent adding port 18, driving a stirring paddle 17 to rotate by starting a stirring motor 16, mixing the cleaning agent to prevent the cleaning agent from precipitating, then starting a water pump 21, starting a ball valve 23, pumping the cleaning agent in the cleaning agent box 15 by the water pump 21 through a connecting pipe 20, discharging the cleaning agent into a cleaning pipe 24 through a connecting pipe two 22, finally spraying the cleaning agent out through a water spraying port on the cleaning pipe 24 to flush the inside of the distillation container 3, starting a water pump two 29 after the distillation container 3 is cleaned by the cleaning agent, opening a ball valve two 31, closing the ball valve one 23, pumping distilled water by the water pump two 29 through a connecting pipe three 28, discharging the distilled water into the cleaning pipe 24 through a connecting pipe four 30, flushing the inside of the distillation container 3 through a water spraying port on the cleaning pipe 24, and simultaneously adding an external water source into a distilled water storage tank 26, so that the distillation container 3 can be washed more cleanly and the cleaning effect is improved.
It should be finally noted that the above only serves to illustrate the technical solution of the present invention, and not to limit the scope of the present invention, and that simple modifications or equivalent replacements performed by those skilled in the art to the technical solution of the present invention do not depart from the spirit and scope of the technical solution of the present invention.
Claims (5)
1. The utility model provides a microwave distillation plant based on crude glycerine convenient to automatically cleaning, includes the distillation case, its characterized in that: the inside bottom fixed mounting of distillation case has the cushion, the up end fixed mounting of cushion has the distillation container, the middle fixed mounting at distillation container top has the feed inlet, the feed inlet upwards extends to the outside of distillation case, the inside top fixed mounting of distillation case has the agitator, the inside right side of distillation case is from last to down in proper order fixed mounting have transformer, rectifier and magnetron, transformer electric connection has power plug, the inside fixed mounting of distillation container has the scavenge pipe, a plurality of hole spouts have been seted up to the intensive cloth on the scavenge pipe.
2. A crude glycerol based microwave distillation apparatus to facilitate self-cleaning according to claim 1, wherein: the left side fixed mounting of distillation case up end has the vacuum pump, the one end of extraction opening fixedly connected with exhaust tube of vacuum pump, the other end of exhaust tube passes the distillation case and extends to the inside of distillation container, the left side fixed mounting of distillation case has the manometer, the manometer communicates with each other with the distillation container is inside, the bottom fixed mounting of distillation container has the discharge gate, the discharge gate extends to the bottom of distillation case, fixed mounting has ejection of compact valve on the discharge gate.
3. A crude glycerol based microwave distillation apparatus to facilitate self-cleaning according to claim 1, wherein: the left side of distillation case is provided with the sanitizer case, the top fixed mounting of sanitizer case has agitator motor, the inside of sanitizer case is provided with the stirring rake, the upper end of stirring rake and agitator motor's output shaft fixed connection, the left side fixed mounting of sanitizer case up end has the sanitizer to add the mouth, the bottom fixed mounting of sanitizer case has the sanitizer discharge port.
4. A crude glycerol based microwave distillation apparatus to facilitate self-cleaning according to claim 3, wherein: the cleaning agent outlet is connected with one end of a first connecting pipe, the other end of the first connecting pipe is connected with a water inlet of a first water pump, an outlet of the first water pump is connected with one end of a second connecting pipe, the other end of the second connecting pipe is fixedly connected with the left end of the cleaning pipe in a sealing mode, and a first ball valve is fixedly mounted on the second connecting pipe.
5. A crude glycerol based microwave distillation apparatus to facilitate self-cleaning according to claim 1, wherein: the right side of distillation tank is provided with distilled water storage jar, the one end of the top fixedly connected with distillation column of distilled water storage jar, the other end of distillation column passes the inside that the distillation tank extends to distillation container, the bottom fixed mounting of distilled water storage jar has the delivery port, the delivery port is connected with the one end of connecting pipe three, the other end fixed mounting of connecting pipe three is at the water inlet of water pump two, the one end of outlet fixedly connected with connecting pipe four of water pump two, the other end of connecting pipe four and the sealed fixed connection of right-hand member of scavenge pipe, fixed mounting has ball valve two on the connecting pipe four.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201922266339.7U CN211611655U (en) | 2019-12-17 | 2019-12-17 | Crude glycerin-based microwave distillation device convenient for self-cleaning |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201922266339.7U CN211611655U (en) | 2019-12-17 | 2019-12-17 | Crude glycerin-based microwave distillation device convenient for self-cleaning |
Publications (1)
Publication Number | Publication Date |
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CN211611655U true CN211611655U (en) | 2020-10-02 |
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ID=72629845
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CN201922266339.7U Expired - Fee Related CN211611655U (en) | 2019-12-17 | 2019-12-17 | Crude glycerin-based microwave distillation device convenient for self-cleaning |
Country Status (1)
Country | Link |
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CN (1) | CN211611655U (en) |
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2019
- 2019-12-17 CN CN201922266339.7U patent/CN211611655U/en not_active Expired - Fee Related
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Legal Events
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20201002 |