Tantalum liquid deposits circulation and dashes ammonia device
Technical Field
The utility model relates to a tantalum liquid deposits technical field, specifically is a tantalum liquid deposits circulation and dashes ammonia device.
Background
The tantalum liquid is in the form of tantalum liquid, which has very excellent chemical properties and very high corrosion resistance. Under cold and hot conditions, it does not react with hydrochloric acid, concentrated nitric acid and "aqua regia", and can be used to make evaporation utensils, etc. and also can be used as electrode, rectifier and electrolytic capacitor of electronic tube.
The tantalum liquid needs to be filled with ammonia in the precipitation process, so that the overall working efficiency is improved, however, the existing circulating ammonia filling device for tantalum liquid precipitation cannot be used for circulating and continuously filling ammonia, the overall using effect is reduced, and the defect that the application range is narrow is caused.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a tantalum liquid deposits circulation and dashes ammonia device to propose in solving above-mentioned background art and can't circulate continuous filling ammonia work, reduced holistic result of use, lead to the narrower problem of its application scope.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a tantalum liquid deposits circulation and dashes ammonia device, includes the drip chamber, the positive bottom fixed position of drip chamber installs the observation window, the refrigeration interface has been seted up to the positive upper end position of drip chamber, one side of drip chamber is fixed with the empty case of gas collection, the opposite side movable mounting of drip chamber has the ammonia jar, the intermediate position fixed mounting of the empty case avris lower extreme of gas collection has the circulating pipe, the empty case of gas collection passes through circulating pipe and ammonia jar lower extreme swing joint, the outside movable mounting of circulating pipe has the check valve, the intermediate position of ammonia jar upper end has been seted up and has been filled the ammonia interface, the inside intermediate position of ammonia jar is fixed with sealed bulkhead.
Preferably, the bottom position in the settling chamber is fixedly provided with a settling net, and the refrigeration interfaces are arranged at the upper end position of the front surface of the settling chamber at equal intervals.
Preferably, the inside of the ammonia tank is divided into two parts by a sealing partition plate, and an ammonia charging chamber and an ammonia circulating chamber are respectively arranged at the upper end and the lower end of the sealing partition plate.
Preferably, two ammonia filling pipes with the same specification are longitudinally and symmetrically fixed on the side of the ammonia tank, the ammonia tank is communicated and connected with the side of the precipitation chamber through the ammonia filling pipes, and a communicating pipe is longitudinally fixed in the middle position between the two ammonia filling pipes.
Preferably, three ammonia tanks having the same specification are installed at equal intervals on the side of the settling chamber, and the three ammonia tanks are connected to each other through a connecting pipe ().
Preferably, an ammonia-filling circulating pump is fixedly installed at the middle position outside the communicating pipe.
Compared with the prior art, the beneficial effects of the utility model are that: this tantalum liquid deposits circulation and dashes ammonia device adopts the ammonia structure of dashing of many ammonia gas pitchers combination to carry out stable connection through a plurality of intercommunication pipe fittings, effectively promoted holistic result of use, and through addding the circulating pump, make the device wholly can effectively circulate continuous work of filling ammonia, improved holistic working property, effectively enlarged the holistic application scope of device.
Drawings
FIG. 1 is a schematic front view of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
fig. 3 is a schematic view of the top view structure of the present invention.
In the figure: 1. a settling chamber; 2. an observation window; 3. a refrigeration interface; 4. a gas collection empty box; 5. a circulation pipe; 6. an ammonia tank; 7. a check valve; 8. an ammonia charging interface; 9. sealing the partition plate; 10. an ammonia charging chamber; 11. an ammonia gas circulation chamber; 12. an ammonia filling pipe; 13. a communicating pipe; 14. an ammonia-charging circulating pump; 15. a precipitation net; 16. and (7) connecting pipes.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution: a tantalum liquid precipitation circulating ammonia flushing device comprises a precipitation chamber 1, an observation window 2, a refrigeration interface 3, a gas collection empty box 4, a circulating pipe 5, an ammonia gas tank 6, a check valve 7, an ammonia filling interface 8 and a sealing partition plate 9, wherein the observation window 2 is fixedly installed at the bottom of the front of the precipitation chamber 1, the refrigeration interface 3 is arranged at the upper end of the front of the precipitation chamber 1, the gas collection empty box 4 is fixed at one side of the precipitation chamber 1, the ammonia gas tank 6 is movably installed at the other side of the precipitation chamber 1, the circulating pipe 5 is fixedly installed at the middle position of the lower end of the side of the gas collection empty box 4, the gas collection empty box 4 is movably connected with the lower end of the ammonia gas tank 6 through the circulating pipe 5, the check valve 7 is movably installed outside the circulating pipe 5, the ammonia filling interface 8 is arranged at the middle position of the upper end of;
furthermore, a settling net 15 is fixedly arranged at the bottom position inside the settling chamber 1, and the refrigeration interfaces 3 are arranged at the upper end position of the front surface of the settling chamber 1 at equal intervals, so that the overall functionality is enriched;
furthermore, the interior of the ammonia gas tank 6 is divided into two parts by a sealing partition plate 9, and an ammonia filling chamber 10 and an ammonia gas circulating chamber 11 are respectively arranged at the upper end and the lower end of the sealing partition plate 9, so that the used ammonia gas is prevented from being mixed with new ammonia in the ammonia gas tank 6, and the integral using effect is prevented from being influenced;
furthermore, two ammonia filling pipes 12 with the same specification are longitudinally and symmetrically fixed on the side of the ammonia gas tank 6, the ammonia gas tank 6 is communicated and connected with the side of the settling chamber 1 through the ammonia filling pipes 12, and a communicating pipe 13 is longitudinally fixed in the middle position between the two ammonia filling pipes 12, so that the reasonable stability of the whole structure of the device is ensured;
furthermore, three ammonia tanks 6 with the same specification are arranged on the side of the settling chamber 1 at equal intervals, and the three ammonia tanks 6 are connected with each other through connecting pipes (16), so that the ammonia filling chambers 10 in the three ammonia tanks 6 are ensured to be communicated with each other, and the three ammonia tanks 6 can be conveniently filled with ammonia during working and using;
further, an ammonia-charging circulation pump 14 is fixedly installed at an intermediate position outside the communication pipe 13, so that the whole device has basic operation performance of ammonia circulation in actual operation.
The working principle is as follows: the method comprises the steps of stably pouring tantalum liquid into a settling chamber 1, effectively settling the tantalum liquid by using a settling net 15, visually observing the settling process of the tantalum liquid in the settling chamber 1 by using an observation window 2, providing necessary refrigeration conditions for the interior of the settling chamber 1 through a refrigeration interface 3, stably butting with external ammonia filling equipment through an ammonia filling interface 8, filling ammonia gas into three ammonia gas tanks 6 at the same time, and starting an ammonia filling circulating pump 14, wherein the ammonia gas enters the settling chamber 1 through an ammonia filling pipe 12 in the ammonia filling chamber 10, and then enters an ammonia gas circulating chamber 11 in the ammonia gas tanks 6 from a circulating pipe 5 through a gas collection empty tank 4, and the ammonia filling circulating pump 12 is started to circularly and continuously fill ammonia into the settling chamber 1, so that the whole application range of the device is effectively expanded.
It should be finally noted that the above only serves to illustrate the technical solution of the present invention, and not to limit the scope of the present invention, and that simple modifications or equivalent replacements performed by those skilled in the art to the technical solution of the present invention do not depart from the spirit and scope of the technical solution of the present invention.