CN211486665U - Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid - Google Patents

Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid Download PDF

Info

Publication number
CN211486665U
CN211486665U CN201922256396.7U CN201922256396U CN211486665U CN 211486665 U CN211486665 U CN 211486665U CN 201922256396 U CN201922256396 U CN 201922256396U CN 211486665 U CN211486665 U CN 211486665U
Authority
CN
China
Prior art keywords
flocculation
soybean polysaccharide
soluble soybean
sedimentation tank
pipeline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201922256396.7U
Other languages
Chinese (zh)
Inventor
崔红亮
程学稳
李金木
崔玉红
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pingdingshan Jinjing Biological Technology Co ltd
Original Assignee
Pingdingshan Jinjing Biological Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pingdingshan Jinjing Biological Technology Co ltd filed Critical Pingdingshan Jinjing Biological Technology Co ltd
Priority to CN201922256396.7U priority Critical patent/CN211486665U/en
Application granted granted Critical
Publication of CN211486665U publication Critical patent/CN211486665U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Separation Of Suspended Particles By Flocculating Agents (AREA)

Abstract

The utility model provides an easy scale deposit material clean system in soluble soybean polysaccharide settling liquid, includes flocculation retort, material delivery pump, swirler and flocculation and precipitation jar, flocculation retort's top is provided with the flocculating agent batcher that the settling liquid was imported and was used for adding the flocculating agent respectively, flocculation retort's bottom export is passed through the pipeline and is connected with the material delivery pump, the export of material delivery pump is passed through the pipeline and is connected with the feed inlet of swirler, the overflow pipe at swirler top passes through the pipeline and is connected with alcohol distillation equipment, and the underflow opening and the flocculation and precipitation jar of swirler bottom are connected, flocculation and precipitation jar's bottom is provided with row cinder notch, and flocculation and precipitation jar's top is provided with the back flow of backward flow transport to flocculation and precipitation jar in. The utility model discloses can separate out the easy scale deposit material that contains in the precipitation liquid before retrieving alcohol to effectively solve the problem of the easy scale deposit of distillation plant.

Description

Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid
Technical Field
The utility model relates to a soybean polysaccharide production technical field specifically is an easy scale deposit material clean system in soluble soybean polysaccharide precipitate liquid.
Background
The soluble soybean polysaccharide is water soluble polysaccharide but not soluble in alcohol, and the alcohol is used as the extractant of the soluble soybean polysaccharide to precipitate the soybean polysaccharide in water solution from the water solution, so as to achieve the purposes of precipitation, dehydration and separation. In the process, 1% of solid matters exist in the solid-liquid separation process, namely soluble soybean polysaccharide particles, soluble protein and micromolecular soybean polysaccharide enter a precipitation liquid phase, namely, the waste alcohol is precipitated. The using amount of the alcohol is large, the residual alcohol in the precipitation liquid needs to be recovered, the alcohol recovery method in the prior art is to distill and recover by a double-effect alcohol tower complete set of equipment, however, because the waste alcohol produced by the precipitation process contains soluble soybean polysaccharide particle solid matter, soluble protein, micromolecular soybean polysaccharide and the like, the method has the advantages that the method can cause serious scaling in rectification heat exchange equipment, the heat exchange efficiency of the reboiler, the feed preheater wine gas preheater, the condensate water preheater and the residual liquid preheater is reduced due to scaling of heat exchange surfaces, system operation parameters are damaged, the wine making capacity is reduced, the energy consumption is increased, the continuity and the stability of the production process of the soluble soybean polysaccharide are influenced, the manufacturing cost of the soluble soybean polysaccharide is increased by 30%, in addition, equipment scaling increases the corrosion risk of equipment, and the service life of the equipment is shortened. Therefore, separating the easily-scaling substances contained in the precipitation liquid before recovering the alcohol is a targeted problem in the production process of the soluble soybean polysaccharide.
SUMMERY OF THE UTILITY MODEL
In order to solve the problem, the utility model aims at providing an easy scale deposit material clean system in soluble soybean polysaccharide precipitate liquid can separate out the easy scale deposit material that contains in the precipitate liquid before retrieving alcohol to effectively solve the problem of the easy scale deposit of distillation plant.
The utility model discloses a solve the technical scheme who takes of above-mentioned problem and do: the utility model provides an easy scale deposit material clean system in soluble soybean polysaccharide settling liquid, includes flocculation retort, material delivery pump, swirler and flocculation and precipitation jar, flocculation retort's top is provided with the flocculating agent batcher that the settling liquid was imported and was used for adding the flocculating agent respectively, flocculation retort's bottom export is passed through the pipeline and is connected with the material delivery pump, the export of material delivery pump is passed through the pipeline and is connected with the feed inlet of swirler, the overflow pipe at swirler top passes through the pipeline and is connected with alcohol distillation equipment, and the underflow opening and the flocculation and precipitation jar of swirler bottom are connected, flocculation and precipitation jar's bottom is provided with row cinder notch, and flocculation and precipitation jar's top is provided with the back flow of backward flow transport to flocculation and precipitation jar in.
Preferably, the bottom flow port is inserted into the flocculation sedimentation tank from the top of the flocculation sedimentation tank and vertically extends downwards to the middle lower part of the flocculation sedimentation tank, and the flocculation sedimentation tank is in sealed connection with the bottom flow port.
Preferably, the return pipe is provided with an underflow adjusting valve for adjusting the underflow flow of the underflow port.
Preferably, an anti-rotation grid is erected at the bottom of the flocculation sedimentation tank, and the anti-rotation grid is composed of a plurality of inclined plates which are obliquely arranged and are parallel to each other.
Preferably, a plurality of sight glasses are arranged on the tank body of the flocculation sedimentation tank.
Preferably, the tube body of the overflow pipe positioned in the inner cavity of the cyclone is of a double-layer tube body structure.
Preferably, the slag discharging port is connected with the centrifugal equipment through a pipeline, and a pulse valve is arranged on the pipeline at the bottom of the slag discharging port.
Preferably, a flow meter for monitoring the feeding amount is arranged on the precipitation liquid inlet.
Preferably, the swirler has a lower cone angle of 15 °.
Compared with the prior art, the utility model discloses following beneficial effect has:
an easy scale deposit material clean system in soluble soybean polysaccharide precipitant solution, can effectively reach the purifying effect of the easy scale deposit impurity of distillation in the residual alcohol of precipitant solution, total solid content reduces to 0.047% by original 0.2% in the residual alcohol of precipitant solution after purifying, total crude protein content reduces to 1% by original 4% in the solid; the centrifugal quantity of the 4000rpm flocculating particle content in the residual alcohol of the precipitation liquid is reduced from the original 1% to 0.29%, the particle size is reduced from the original 100 mu m to below 40 mu m, and easily-scaling substances contained in the precipitation liquid are effectively separated.
After the residual alcohol of the precipitation liquid is purified, the economic operation of an alcohol distillation system is improved: the cleaning period of the alcohol distillation system is prolonged to 45-60 days from the original 15 days; the average gas consumption per ton of finished wine is reduced to 0.45t/t wine from the original 0.75t/t wine; the economic, smooth operation of the distillation system, and even the entire production system, is improved. The process system has simple equipment, convenient control and low investment cost, thereby effectively solving the problem that the alcohol distillation equipment is easy to scale.
Drawings
Fig. 1 is a schematic view of the connection structure of the present invention;
the labels in the figure are: 1. the system comprises a flocculation reaction tank, 2, a material delivery pump, 3, a cyclone, 4, a flocculation precipitation tank, 5, a precipitation liquid inlet, 51, a flowmeter, 6, a flocculant quantitative feeder, 7, an overflow pipe, 8, a bottom flow port, 9, a slag discharge port, 91, a pulse valve, 10, a return pipe, 11, an underflow adjusting valve, 12, an anti-rotation grid, 13 and a sight glass.
Detailed Description
The present invention will be described in detail with reference to the following embodiments, which are based on the technical solution of the present invention and provide detailed embodiments and specific operation processes.
As shown in the figure, the utility model relates to an easy scale deposit material clean system in soluble soybean polysaccharide precipitate liquid, including flocculation retort 1, material delivery pump 2, swirler 3 and flocculation precipitation jar 4, the top of flocculation retort 1 is provided with precipitate liquid import 5 respectively and is used for adding flocculating agent's flocculating agent batcher 6, the bottom export of flocculation retort 1 is passed through the pipeline and is connected with material delivery pump 2, the export of material delivery pump 2 is passed through the pipeline and is connected with the feed inlet of swirler 3, the overflow pipe 7 at swirler 3 top passes through the pipeline and is connected with alcohol distillation equipment, and the underflow opening 8 and the flocculation precipitation jar 4 of swirler 3 bottom are connected, the bottom of flocculation precipitation jar 4 is provided with row cinder notch 9, and the top of flocculation precipitation jar 4 is provided with the back flow 10 of backward flow transport to the flocculation precipitation jar 1 in.
The foregoing is a basic embodiment of the invention, and further modifications, optimizations, or limitations may be made on the foregoing.
Further, the bottom flow port 8 is inserted into the flocculation deposition tank 4 from the top of the flocculation deposition tank 4 and vertically extends downwards to the middle lower part of the flocculation deposition tank 4, and the flocculation deposition tank 4 is in sealed connection with the bottom flow port 8.
Further, the return pipe 10 is provided with an underflow adjusting valve 11 for adjusting the underflow flow of the underflow port 8.
Further, an anti-rotation grid 12 is erected at the bottom of the flocculation sedimentation tank 4, and the anti-rotation grid 12 is composed of a plurality of inclined plates which are obliquely arranged and are parallel to each other.
Further, a plurality of sight glasses 13 are arranged on the tank body of the flocculation sedimentation tank 4.
Further, the pipe body of the overflow pipe 7 positioned in the inner cavity of the cyclone 3 is a double-layer pipe body structure.
Further, the slag discharging port 9 is connected with a centrifugal device through a pipeline, and a pulse valve 91 is arranged on the pipeline at the bottom of the slag discharging port 9.
Further, a flow meter 51 for monitoring the feeding amount is arranged on the precipitation liquid inlet 5.
Further, the lower cone angle of the swirler 3 is 15 °.
The principle of the application is as follows: in the soluble soybean polysaccharide precipitation liquid, the solid matter mainly comprises two parts: part of solid matter is soluble soybean polysaccharide fine particles caused by the separation effect of a centrifugal machine, the part of particles can be easily separated by measures such as sedimentation, and the other part of particles is alcohol-soluble protein and small molecular polysaccharide with strong water solubility, and the two exist in the form of solution or colloid.
According to the analysis of the scale sample, the protein content is higher than that of the residual wine, which shows that the protein is influenced by factors such as alcohol phase to water phase and thermal denaturation along with the gradual reduction of the alcohol concentration in the distillation process, so that the protein becomes a main scaling factor in the alcohol distillation process. In order to remove the soluble substances in the residual liquor of the precipitation liquid, a proper flocculating agent is selected, and the solid substances in the precipitation liquid are flocculated and settled to form flocculate under the action of the flocculating agent.
In order to separate flocculate in time, the material delivery pump is used as power, a cyclone separation technology is adopted, so that the flocculated precipitate is subjected to accelerated settling separation under the action of centrifugal force, and the conveying and separation are carried out synchronously, so that the flocculate is separated out.
Wherein, in order to improve the separation effect of the cyclone 3: the swirler 3 adopts a lower cone angle of 15 degrees; the part of the overflow pipe 7 inserted into the cyclone 3 adopts a double-layer pipe structure, so that the distance between the overflow pipe 7 and the barrel of the cyclone 3 is reduced, the internal energy loss is reduced, and the separation effect is improved; the underflow port 8 extends to the middle lower part in the flocculation sedimentation tank 4, underflow is discharged through two paths, one path is at the top of the sedimentation tank, and the underflow flow is adjusted by the underflow adjusting valve 11 to control the separation effect of the cyclone 3; one way is to discharge high-concentration flocculation sediment through a pulse valve 91 and return the sediment to a centrifuge feeding section to be recycled as a finished product.
In addition, the anti-rotation grille 12 composed of inclined plates is arranged at the position 1/3 at the lower part of the flocculation settling tank 4, so that the sedimentation area is increased, and the rotation disturbance of the underflow outlet is reduced, thereby playing a role in accelerating flocculation and sedimentation.
The above description is only a preferred embodiment of the present invention, and the present invention is not limited to the above description, and although the present invention has been described with reference to the preferred embodiment, it is not limited to the present invention, and any skilled person in the art can make equivalent modifications or changes within the technical scope of the present invention, and any simple modifications, equivalent changes and modifications made by the technical spirit of the present invention to the above embodiments are within the technical scope of the present invention.

Claims (9)

1. A easy scale deposit material clean system in soluble soybean polysaccharide precipitate liquid which characterized in that: comprises a flocculation reaction tank (1), a material delivery pump (2), a cyclone (3) and a flocculation sedimentation tank (4), the top of the flocculation reaction tank (1) is respectively provided with a precipitation liquid inlet (5) and a flocculant quantitative feeder (6) for adding a flocculant, the bottom outlet of the flocculation reaction tank (1) is connected with a material delivery pump (2) through a pipeline, the outlet of the material conveying pump (2) is connected with the feed inlet of the cyclone (3) through a pipeline, an overflow pipe (7) at the top of the cyclone (3) is connected with alcohol distillation equipment through a pipeline, a bottom flow port (8) at the bottom of the cyclone (3) is connected with a flocculation sedimentation tank (4), the bottom of the flocculation sedimentation tank (4) is provided with a slag discharge port (9), and the top of the flocculation sedimentation tank (4) is provided with a return pipe (10) which returns and is conveyed into the flocculation reaction tank (1).
2. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: the bottom flow port (8) is inserted into the flocculation sedimentation tank (4) from the top of the flocculation sedimentation tank (4) and vertically extends downwards to the middle lower part of the flocculation sedimentation tank (4), and the flocculation sedimentation tank (4) is connected with the bottom flow port (8) in a sealing way.
3. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: the backflow pipe (10) is provided with an underflow adjusting valve (11) used for adjusting the underflow flow of the underflow port (8).
4. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: an anti-rotation grating (12) is erected at the bottom in the flocculation sedimentation tank (4), and the anti-rotation grating (12) is composed of a plurality of inclined plates which are obliquely arranged and are parallel to each other.
5. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: a plurality of sight glasses (13) are arranged on the tank body of the flocculation sedimentation tank (4).
6. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: the pipe body of the overflow pipe (7) positioned in the inner cavity of the swirler (3) is of a double-layer pipe body structure.
7. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: the slag discharging port (9) is connected with centrifugal equipment through a pipeline, and a pulse valve (91) is arranged on the pipeline at the bottom of the slag discharging port (9).
8. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: and a flow meter (51) for monitoring the feeding amount is arranged on the precipitation liquid inlet (5).
9. The system for purifying scale-prone substances in soluble soybean polysaccharide precipitant of claim 1, wherein: the lower cone angle of the swirler (3) is 15 degrees.
CN201922256396.7U 2019-12-16 2019-12-16 Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid Active CN211486665U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201922256396.7U CN211486665U (en) 2019-12-16 2019-12-16 Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201922256396.7U CN211486665U (en) 2019-12-16 2019-12-16 Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid

Publications (1)

Publication Number Publication Date
CN211486665U true CN211486665U (en) 2020-09-15

Family

ID=72416384

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201922256396.7U Active CN211486665U (en) 2019-12-16 2019-12-16 Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid

Country Status (1)

Country Link
CN (1) CN211486665U (en)

Similar Documents

Publication Publication Date Title
CN109851139B (en) High-salt wastewater softening and concentrating device and method
CN201665593U (en) Desulfurization waste water treating system
CN104457315A (en) Cooling tower purification method and device
CN211486665U (en) Easily scale deposit material clean system in soluble soybean polysaccharide precipitate liquid
CN207276278U (en) Combined type coagulative precipitation device
CN102225799A (en) Enhanced dephosphorization reactor
CN203540146U (en) Novel efficient physical-chemical water processing and precipitating device
CN207175661U (en) A kind of desulfurization wastewater treatment system
CN205241438U (en) Contain coal waste water electron flocculation facility
CN204404834U (en) A kind of cooling tower purifier and modular cooling tower purifier
CN108147642A (en) Highly effective sludge concentration basin
CN208949026U (en) A kind of water purifier using particulate matter
CN209392786U (en) Deep cone thickener for the processing of hydropower industry sandstone wastewater
CN110960901A (en) Flocculating agent for separating easy-scaling substances in soybean polysaccharide precipitation liquid and separation process
CN208865300U (en) Sewage running piping device for filtering and collecting impurities
CN202283434U (en) Slag discharge water tank
CN208577650U (en) A kind of overflow mechanism reducing phenates amount in raw material dephenolize naphtalene oil
CN205442862U (en) System for magnesium method desulfurization waste water suspended solid is got rid of to high efficiency
CN206424794U (en) Internal circulating membrane system
CN111547798A (en) Waste water MVR evaporimeter is smelted to gold
CN205933521U (en) Energy -conserving high -efficient sewage treatment plant's salt recovery system
CN205088167U (en) Concentration of cocoon cooking waste water silk albumen is recovery system again
CN217077210U (en) High-efficient retrieval and utilization device of fluorine-containing acid waste liquid
CN220758087U (en) Clarifying device for extracting tobacco essential oil
CN203568925U (en) Micro-eddy hardness remover

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: A purification system for scaling substances in soluble soybean polysaccharide precipitation solution

Effective date of registration: 20201223

Granted publication date: 20200915

Pledgee: Bank of China Limited by Share Ltd. Yexian County branch

Pledgor: PINGDINGSHAN JINJING BIOLOGICAL TECHNOLOGY Co.,Ltd.

Registration number: Y2020980009793

PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20220304

Granted publication date: 20200915

Pledgee: Bank of China Limited by Share Ltd. Yexian County branch

Pledgor: PINGDINGSHAN JINJING BIOLOGICAL TECHNOLOGY CO.,LTD.

Registration number: Y2020980009793

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: A purification system for easy scaling substances in soluble soybean polysaccharide precipitation solution

Effective date of registration: 20220308

Granted publication date: 20200915

Pledgee: Bank of China Limited by Share Ltd. Yexian County branch

Pledgor: PINGDINGSHAN JINJING BIOLOGICAL TECHNOLOGY CO.,LTD.

Registration number: Y2022980002299

PC01 Cancellation of the registration of the contract for pledge of patent right

Granted publication date: 20200915

Pledgee: Bank of China Limited by Share Ltd. Yexian County branch

Pledgor: PINGDINGSHAN JINJING BIOLOGICAL TECHNOLOGY CO.,LTD.

Registration number: Y2022980002299

PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: A Purification System for Scaling Substances in Soluble Soybean Polysaccharide Precipitation Solution

Granted publication date: 20200915

Pledgee: Bank of China Limited by Share Ltd. Yexian County branch

Pledgor: PINGDINGSHAN JINJING BIOLOGICAL TECHNOLOGY CO.,LTD.

Registration number: Y2024980024396