CN211284488U - Large cover with heat-insulating heating and connecting device for titanium sponge distillation production - Google Patents

Large cover with heat-insulating heating and connecting device for titanium sponge distillation production Download PDF

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Publication number
CN211284488U
CN211284488U CN202020034871.6U CN202020034871U CN211284488U CN 211284488 U CN211284488 U CN 211284488U CN 202020034871 U CN202020034871 U CN 202020034871U CN 211284488 U CN211284488 U CN 211284488U
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China
Prior art keywords
pipe
large cover
connecting device
heating
passageway
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Expired - Fee Related
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CN202020034871.6U
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Chinese (zh)
Inventor
张履国
李斗良
舒煜
陈太武
曹海国
李金泽
刘建国
蔡增新
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Zunyi Titanium Industry Co Ltd
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Zunyi Titanium Industry Co Ltd
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Priority to CN202020034871.6U priority Critical patent/CN211284488U/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The large cover with the heat-preservation heating and connecting device for the titanium sponge distillation production comprises a large cover bottom plate, a large cover cylinder, a large cover panel, a vertical pipe, a horizontal pipe and an evacuation pipe; the top end of the transverse pipe is provided with a connecting device; a passage pipe with a radial angle of 90 degrees is arranged in the large cover cylinder body, the vertical pipe and the transverse pipe; a heating element is arranged on the outer pipe surface of the passageway pipe; the heat-insulating layer is filled in a closed cavity formed by the large cover bottom plate, the large cover barrel, the large cover panel, the vertical pipe, the channel pipe, the transverse pipe and the connecting device. The utility model overcomes the welding quality problem of the large-cover passageway, reduces the air inlet probability of the product and improves the production quality of the titanium sponge; the corridor heating is adopted, and compared with the existing corridor heating technology with a large cover, the power consumption cost is reduced, and the working procedure of manually assembling the corridor heater during distillation is reduced. And the flange connection of the aisle device is adopted to replace welding connection, so that the production period is shortened and the labor intensity of welding workers is reduced. Adopt the utility model discloses big lid passageway heating device reduces the operation of overhead traveling crane and operative employee's intensity of labour.

Description

Large cover with heat-insulating heating and connecting device for titanium sponge distillation production
Technical Field
The utility model relates to a device that production titanium sponge was used, what specifically said so relates to a big lid of titanium sponge distillation production usefulness of taking heat preservation heating and connecting device.
Background
At present, the industrial production of titanium sponge at home and abroad adopts a method for reducing titanium tetrachloride by magnesium. The method comprises the steps of adding liquid magnesium into a reactor, continuously adding titanium tetrachloride to react with the liquid magnesium to obtain granular titanium, slowly forming titanium sponge lump, after reduction charging production is finished, carrying out distillation production to remove a small amount of magnesium and magnesium chloride in the titanium lump, and adopting a distillation furnace type mode to comprise a series furnace and a parallel furnace (an inverted U-shaped combination method). In the reduction distillation production process, most furnace types are produced by adopting an inverted U-shaped combined method, and the method has the advantages of large yield, high qualification rate, low energy consumption, low labor cost and the like compared with a small single furnace. In order to improve the production quality of the titanium sponge and reduce the production cost, the large-scale equipment is taken as a technical development direction in all countries. The combined furnace parallel connection furnace is characterized in that a cold end reaction tank which is the same as a hot end system is connected with a passage (the passage is connected by a transverse pipe and a vertical pipe in a welding way) arranged on a large cover in the prior art by a transverse pipe beside a reduction production furnace, and the joint of the hot end transverse pipe and the cold end transverse pipe is connected with the cold end reaction tank in a welding way. Magnesium and magnesium chloride steam is distilled from a hot end system to a cold end system through a passageway, and in order to ensure that the high-temperature magnesium and the magnesium chloride steam are not condensed in the passageway, a vertical pipe heater and a transverse pipe heater are independently installed on a passageway vertical pipe above a large cover panel. The vertical pipe heater and the horizontal pipe heater are large in size, the overhead travelling crane is required to hoist each time the vertical pipe heater and the horizontal pipe heater are mounted and dismounted, and the operation of workers for butting the passage takes about 2 hours during assembling and dismounting; when heating, the heater is heated to above 850 ℃ to consume electric energy; during distillation, the welding of the vertical pipe and the transverse pipe is easy to generate cracks, and if leakage occurs, production has to be stopped and the product quality is affected; under the high-temperature and high-vacuum environment, the pressure difference between the inside of the passageway and the outside is large, so that the passageway pipe is easy to deform, and the welding line is easily cracked by thermal stress, so that the production is stopped and the product quality is influenced; when the junction of the hot end transverse pipe and the cold end transverse pipe is connected by welding, in order to prevent the hot end titanium sponge lump from being polluted by air inflow, argon gas must be continuously filled into the hot end reactor for protection, the argon gas flows out from the pressure relief port for 3 hours, the welding time is long, the argon gas is wasted, and the possibility of polluting products by air inflow is also caused.
SUMMERY OF THE UTILITY MODEL
The utility model discloses a for solving exist among the prior art: 1. the heaters of the vertical pipe and the horizontal pipe of the large cover consume electricity; 2. the heater for the large-cover vertical pipe and the horizontal pipe is large in size; 3. the passageway pipe generates deformation passageway high-temperature deformation and thermal stress cracks a welding line.
In order to solve the technical problem, the utility model discloses a following technical scheme:
the large cover with the heat preservation heating and connecting device for the titanium sponge distillation production comprises a large cover bottom plate 1, a large cover cylinder 2, a large cover panel 4, a vertical pipe 5, a horizontal pipe 8 and an evacuation pipe 10; the evacuation pipe 10 is arranged on the large cover panel 4; the top end of the transverse pipe 8 is provided with a connecting device 9; a passage pipe 6 with a 90-degree radial angle is arranged in the large cover cylinder body 2, the vertical pipe 5 and the transverse pipe 8; a heating element 7 is arranged on the outer pipe surface of the aisle pipe 6; and a heat-insulating layer 3 is filled in a closed cavity formed by the large cover bottom plate 1, the large cover cylinder body 2, the large cover panel 4, the vertical pipe 5, the passageway pipe 6, the transverse pipe 8 and the connecting device 9.
The connecting device 9 is integrally formed and comprises a flange hole 901, an annular groove 902, an annular clamping groove 903, a trapezoidal circular truncated cone 904 and a flange 905.
The trapezoidal round platform 904 is filled with a heat insulation layer, and the surface of the trapezoidal round platform is provided with an asbestos rope.
The surface of the flange 905 is provided with a sealing gasket.
Adopt above-mentioned technical scheme's beneficial effect:
1. the utility model discloses overcome big lid passageway welding quality problem, reduce the product probability of admitting air, improve titanium sponge production quality.
2. Adopt the utility model discloses a passageway heating reduces artifical equipment passageway heater process when reducing power consumption cost and distillation than current big lid passageway heating technique.
3. Adopt the utility model discloses passageway device flange joint replaces welded connection, shortens production cycle and reduces welding workman intensity of labour.
4. Adopt the utility model discloses big lid passageway heating device reduces the operation of overhead traveling crane and operative employee's intensity of labour.
Drawings
Fig. 1 is a schematic structural view of the present invention;
in the figure: 1-large cover bottom plate, 2-large cover cylinder, 3-insulating layer, 4-large cover panel, 5-vertical pipe, 6-channel pipe, 7-heating element, 8-horizontal pipe, 9-connecting device and 10-evacuation pipe.
FIG. 2 is a schematic view of the connecting device of the present invention;
in the figure: 901-flange hole, 902-ring groove, 903-ring groove, 904-trapezoid truncated cone and 905-flange.
Fig. 3 is an enlarged view of the aisle and connection arrangement of fig. 1.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings.
The large cover for the titanium sponge distillation production with the heat preservation heating and connecting device comprises a large cover bottom plate 1, a large cover cylinder 2, a large cover panel 4, a vertical pipe 5, a horizontal pipe 8 and an evacuation pipe 10, wherein the large cover bottom plate is provided with a heat preservation heating and connecting device; the evacuation pipe 10 is arranged on the large cover panel 4; the top end of the transverse pipe 8 is provided with a connecting device 9; a passage pipe 6 with a 90-degree radial angle is arranged in the large cover cylinder body 2, the vertical pipe 5 and the transverse pipe 8; a heating element 7 is arranged on the outer pipe surface of the aisle pipe 6; and a heat-insulating layer 3 is filled in a closed cavity formed by the large cover bottom plate 1, the large cover cylinder body 2, the large cover panel 4, the vertical pipe 5, the passageway pipe 6, the transverse pipe 8 and the connecting device 9.
As shown in fig. 2, the connecting device 9 is integrally formed, and is composed of a flange hole 901, an annular groove 902, an annular clamping groove 903, a trapezoidal circular platform 904 and a flange 905.
The inside of trapezoidal garden 904 is filled with the heat preservation, and during the distillation, trapezoidal garden 904 surface sets up the asbestos cord, and the asbestos cord plays the thermal-insulated effect that keeps warm.
During distillation, the surface of the flange 905 is provided with a sealing pad, and the sealing pad plays a role in sealing high vacuum.
The flange holes 901 are used for bolt connection between the passageways.
The annular groove 902 is used for facilitating the operation of the bolt connection.
The annular clamping groove 903 is used for clamping a clamp for plugging a pipeline port during reduction production.
As shown in figure 1, the channel passing pipe 6 is formed by a round pipe, and the radial direction of the channel passing pipe is 90 degrees, so that the main function is to avoid the problem of welding quality of a transverse pipe and a vertical pipe in the prior art.
As shown in fig. 1, the large cover bottom plate 1 is provided with an evacuation pipe 10, which is connected to a low vacuum system during distillation, and functions to reduce the pressure difference between the inside of the bypass pipe 6 and the outside atmosphere and protect the bypass pipe 6 from deformation.

Claims (4)

1. The large cover with the heat preservation heating and connecting device for the titanium sponge distillation production comprises a large cover bottom plate (1), a large cover cylinder body (2), a large cover panel (4), a vertical pipe (5), a horizontal pipe (8) and an evacuation pipe (10); the evacuation pipe (10) is arranged on the large cover panel (4); the method is characterized in that: a connecting device (9) is arranged at the top end of the transverse pipe (8); a passage pipe (6) which radially forms an angle of 90 degrees is arranged in the large cover cylinder body (2), the vertical pipe (5) and the transverse pipe (8); a heating element (7) is arranged on the outer pipe surface of the passageway pipe (6); the heat-insulating layer (3) is filled in a closed cavity formed by the large cover bottom plate (1), the large cover cylinder body (2), the large cover panel (4), the vertical pipe (5), the aisle pipe (6), the transverse pipe (8) and the connecting device (9).
2. The large lid according to claim 1, characterized in that: the connecting device (9) is integrally formed and consists of a flange hole (901), an annular groove (902), an annular clamping groove (903), a trapezoidal circular truncated cone (904) and a flange (905).
3. The large lid according to claim 2, characterized in that: the trapezoidal round platform (904) is filled with a heat insulation layer, and the surface of the trapezoidal round platform is provided with an asbestos rope.
4. The large lid according to claim 2, characterized in that: the surface of the flange (905) is provided with a sealing gasket.
CN202020034871.6U 2020-01-08 2020-01-08 Large cover with heat-insulating heating and connecting device for titanium sponge distillation production Expired - Fee Related CN211284488U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202020034871.6U CN211284488U (en) 2020-01-08 2020-01-08 Large cover with heat-insulating heating and connecting device for titanium sponge distillation production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202020034871.6U CN211284488U (en) 2020-01-08 2020-01-08 Large cover with heat-insulating heating and connecting device for titanium sponge distillation production

Publications (1)

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CN211284488U true CN211284488U (en) 2020-08-18

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111139369A (en) * 2020-01-08 2020-05-12 遵义钛业股份有限公司 Large cover with heat-insulating heating and connecting device for titanium sponge distillation production
CN112662895A (en) * 2020-11-25 2021-04-16 贵州省钛材料研发中心有限公司 Reactor big cover for titanium sponge reduction distillation production

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111139369A (en) * 2020-01-08 2020-05-12 遵义钛业股份有限公司 Large cover with heat-insulating heating and connecting device for titanium sponge distillation production
CN112662895A (en) * 2020-11-25 2021-04-16 贵州省钛材料研发中心有限公司 Reactor big cover for titanium sponge reduction distillation production

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20200818

Termination date: 20210108

CF01 Termination of patent right due to non-payment of annual fee