CN211216665U - Drum-type low mercury catalyst preparation facilities - Google Patents
Drum-type low mercury catalyst preparation facilities Download PDFInfo
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- CN211216665U CN211216665U CN201921904893.7U CN201921904893U CN211216665U CN 211216665 U CN211216665 U CN 211216665U CN 201921904893 U CN201921904893 U CN 201921904893U CN 211216665 U CN211216665 U CN 211216665U
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- fixedly connected
- reaction barrel
- crushing
- mercury catalyst
- rotating shaft
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Abstract
The utility model discloses a low mercury catalyst preparation facilities of drum-type, including the reaction barrel, the inner chamber bottom fixedly connected with of reaction barrel filters the fine mesh, the outer end fixedly connected with heating ring of reaction barrel, just the bottom fixedly connected with funnel of reaction barrel, the one end joint of funnel has the table body, just the bottom fixedly connected with discharging pipe of funnel, the top fixedly connected with agitator motor case of reaction barrel, be equipped with agitator motor in the inner chamber of agitator motor case, agitator motor's one end threaded connection has the puddler, the outer wall fixedly connected with stirring vane of puddler, just the upper left end fixedly connected with crushing case of reaction barrel, the inner chamber fixedly connected with rubbing crusher of crushing case constructs. This low mercury catalyst preparation facilities of drum-type can smash solid-state mercury catalyst, makes reaction mass and the abundant basis of mercury catalyst material to the heating collar of installation can heat the reaction barrel for reaction rate.
Description
Technical Field
The utility model relates to a low mercury catalyst preparation facilities technical field of drum-type specifically is a low mercury catalyst preparation facilities of drum-type.
Background
The mercury catalyst can change the chemical reaction rate of a reactant without changing chemical balance in a chemical reaction, and the substance of which the mass and the chemical property are not changed before and after the chemical reaction is called the catalyst. The solid catalyst is also called catalyst. The mercury catalyst is actually used in an organic synthesis reaction using mercury chloride as a catalyst.
The mercury catalyst is mostly solid, the solvent needs to be dissolved first to play a catalytic role in the reaction, the dissolution speed of the mercury catalyst solid in some dissolved solutions is slow, so the solid mercury catalyst needs to be crushed into powder to improve the catalytic speed, and some reaction solutions not only need the catalysis of the mercury catalyst, but also need to be heated to promote the reaction.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a low mercury catalyst preparation facilities of drum-type to solve the problem that proposes among the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: a drum-type low-mercury catalyst preparation device comprises a reaction barrel, wherein a filtering fine net is fixedly connected to the bottom end of an inner cavity of the reaction barrel, a heating ring is fixedly connected to the outer end of the reaction barrel, a funnel is fixedly connected to the bottom end of the reaction barrel, a table body is clamped at one end of the funnel, a discharging pipe is fixedly connected to the bottom end of the funnel, an agitating motor box is fixedly connected to the top end of the reaction barrel, an agitating motor is arranged in an inner cavity of the agitating motor box, an agitating rod is in threaded connection with one end of the agitating motor, an agitating sheet is fixedly connected to the outer wall of the agitating rod, a crushing box is fixedly connected to the upper left end of the reaction barrel, a crushing mechanism is fixedly connected to the inner cavity of the crushing box, a pushing mechanism is fixedly connected to the lower left end of the crushing box, an inlet pipe is fixedly connected to the right side of the bottom end of the crushing, a liquid tank is fixedly connected to the right end of the reaction barrel, a first liquid pumping pipe is inserted into an inner cavity of the liquid tank, one end of the first liquid pumping pipe penetrates through the liquid tank and extends to the outside, a water pump is fixedly connected to the other end of the first liquid pumping pipe, a second liquid pumping pipe is inserted into the other end of the water pump, the other end of the second liquid pumping pipe is fixedly connected to the right side of the top end of the reaction barrel, and a liquid supplementing pipe is fixedly connected to one end, away from the liquid tank, of the first liquid pumping pipe;
the crushing mechanism comprises a crushing motor, a motor rotating shaft, a fine gear, a first coarse gear, a second coarse gear, a first rotating shaft, a second rotating shaft, a first crushing disc and a second crushing disc, the grinding motor is fixedly connected with the outer end of the grinding box, the rotating shaft of the motor is in threaded connection with one end of the grinding motor, the thin gear is fixedly connected with the other end of the motor rotating shaft, the first coarse gear is clamped at one end of the thin gear, the first rotating shaft is fixedly connected to one side of the first coarse gear, the first grinding disc is fixedly connected to the other end of the first rotating shaft, and one end of the first coarse gear far away from the fine gear is clamped with a second coarse gear, the second rotating shaft is fixedly connected with one side of the second coarse gear, the second grinding disc is fixedly connected to the other end of the second rotating shaft, and the first grinding disc and the second grinding disc are arranged in an inner cavity of the grinding box;
the pushing mechanism comprises an air cylinder, a push rod and a push sheet, the air cylinder is fixedly connected to the lower left end of the crushing box, the push rod is sleeved at one end of the air cylinder, the push rod penetrates through the crushing box and extends to the inside, and the push sheet is fixedly connected to the other end of the push rod.
Preferably, the left side of the top end of the reaction barrel is fixedly connected with a pressure reduction hole.
Preferably, the left end of the reaction barrel is fixedly connected with a liquid pressure gauge.
Preferably, the top end of the crushing box is fixedly connected with a solid feeding hole.
Preferably, one end of the feeding pipe is fixedly connected with a powder filter screen.
Preferably, one side of the discharge pipe is in threaded connection with a flow control valve.
Compared with the prior art, the beneficial effects of the utility model are that:
(1) this low mercury catalyst preparation facilities of drum-type at the outside fixedly connected with heating ring of reaction barrel, the heating ring can heat the reaction for reaction rate, and the puddler of installation can stir the material in the reaction barrel, makes the reaction material fully contact with mercury catalyst, has accelerated the process of reaction.
(2) This low mercury catalyst preparation facilities of drum-type, the rubbing crusher of installation can pulverize solid-state mercury catalyst, make mercury catalyst and reactant contact more abundant, and the powder filter screen has been installed to the one end at the inlet pipe, can stay the large granule and continue smashing in smashing the case, prevent that the large granule from entering into the reaction barrel, the fine net of filtration of the installation of the inner chamber bottom of reaction barrel can be with the reaction in the solution mercury catalyst material of complete dissolution and impurity filtration obtain comparatively pure reactant.
Drawings
FIG. 1 is a sectional view of the present invention;
FIG. 2 is a sectional view of the structure of the crushing box of the present invention;
fig. 3 is a top view of the structure of the crushing box of the present invention.
In the figure: 1 reaction barrel, 2 fine filtering net, 3 heating ring, 4 funnel, 5 table body, 6 discharging pipe, 7 stirring motor box, 8 stirring motor, 9 stirring rod, 10 stirring sheet, 11 crushing box, 12 crushing mechanism, 121 crushing motor, 122 motor rotating shaft, 123 fine gear, 124 first coarse gear, 125 second coarse gear, 126 first rotating shaft, 127 second rotating shaft, 128 first crushing disk, 129 second crushing disk, 13 pushing mechanism, 131 cylinder, 132 push rod, 133 push sheet, 14 feeding pipe, 15 liquid tank, 16 first liquid pumping pipe, 17 water pump, 18 second liquid pumping pipe, 19 liquid replenishing pipe, 20 pressure gauge pressure reducing hole, 21 liquid, 22 solid feeding hole, 23 powder filtering net and 24 flow control valve.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution: a drum-type low-mercury catalyst preparation device comprises a reaction barrel 1, wherein the bottom end of an inner cavity of the reaction barrel 1 is fixedly connected with a filtering fine screen 2, the outer end of the reaction barrel 1 is fixedly connected with a heating ring 3, the bottom end of the reaction barrel 1 is fixedly connected with a funnel 4, one end of the funnel 4 is clamped with a table body 5, the bottom end of the funnel 4 is fixedly connected with a discharge pipe 6, the top end of the reaction barrel 1 is fixedly connected with a stirring motor box 7, a stirring motor 8 is arranged in the inner cavity of the stirring motor box 7, one end of the stirring motor 8 is in threaded connection with a stirring rod 9, the outer wall of the stirring rod 9 is fixedly connected with a stirring sheet 10, the left upper end of the reaction barrel 1 is fixedly connected with a crushing box 11, the inner cavity of the crushing box 11 is fixedly connected with a crushing mechanism 12, the left lower end of the crushing box 11 is fixedly connected with a pushing mechanism 13, the bottom end and the right side of, and the right-hand member fixedly connected with fluid reservoir 15 of reaction vessel 1, the inner chamber of fluid reservoir 15 is pegged graft and is had first liquid suction pipe 16, and the one end of first liquid suction pipe 16 runs through fluid reservoir 15 and extends to the outside, and the other end fixedly connected with water pump 17 of first liquid suction pipe 16, and the other end of water pump 17 is pegged graft and is had second liquid suction pipe 18, and the other end fixed connection of second liquid suction pipe 18 is on the top right side of reaction vessel 1, and the one end fixedly connected with fluid infusion pipe 19 of fluid reservoir 15 is kept away from to first liquid suction pipe 16.
The crushing mechanism 12 comprises a crushing motor 121, a motor rotating shaft 122, a fine gear 123, a first coarse gear 124, a second coarse gear 125, a first rotating shaft 126, a second rotating shaft 127, a first crushing disk 128 and a second crushing disk 129, wherein the crushing motor 121 is fixedly connected to the outer end of the crushing box 11, the motor rotating shaft 122 is in threaded connection with one end of the crushing motor 121, the fine gear 123 is fixedly connected to the other end of the motor rotating shaft 122, the first coarse gear 124 is clamped at one end of the fine gear 123, and a first rotating shaft 126 is fixedly coupled to one side of the first coarse gear 124, a first grinding plate 128 is fixedly coupled to the other end of the first rotating shaft 126, and the end of the first coarse gear 124 far from the fine gear 123 is clamped with a second coarse gear 125, the second rotating shaft 127 is fixedly connected to one side of the second coarse gear 125, the second grinding disc 129 is fixedly connected to the other end of the second rotating shaft 127, and the first grinding disc 128 and the second grinding disc 129 are arranged in the inner cavity of the grinding box.
When the mercury catalyst crusher is used, a solid mercury catalyst is placed into the crushing box 11 to be crushed, a reaction reagent is introduced into the liquid supplementing pipe 19, the water pump 17 is started, the reaction reagent is introduced into the reaction barrel 1 through the water pump 17, the powdered mercury catalyst material reacts with the reaction reagent, the reaction material is continuously stirred through the stirring rod 9, the reaction barrel 1 is heated through the heating ring 3, the reaction speed is accelerated, the reacted reagent is discharged through the discharging pipe 6, and the mercury catalyst material which is not completely reacted and impurities are filtered through the filtering fine net 2.
To sum up, this low mercury catalyst preparation facilities of drum-type at the outside fixedly connected with heating ring 3 of retort 1, heating ring 3 can heat the reaction for reaction rate, and the puddler 9 of installation can stir the material in the retort, makes reaction material and mercury catalyst fully contact, has accelerated the process of reaction.
And this low mercury catalyst preparation facilities of drum-type, rubbing crusher structure 12 of installation can pulverize solid-state mercury catalyst, make mercury catalyst and reactant contact more abundant, and installed powder filter screen 23 in the one end of inlet pipe 14, can stay the large granule and continue to smash in smashing case 11, prevent that the large granule from entering into reaction barrel 1, the fine net 2 of filtration of the installation of the inner chamber bottom of reaction barrel 1 can be with the reaction in the solution mercury catalyst material of complete dissolution and impurity filtration obtain comparatively pure reactant.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides a low mercury catalyst preparation facilities of drum-type, includes reaction barrel (1), its characterized in that: the inner cavity bottom fixedly connected with of reaction barrel (1) filters fine net (2), the outer end fixedly connected with heating collar (3) of reaction barrel (1), just the bottom fixedly connected with funnel (4) of reaction barrel (1), the one end joint of funnel (4) has the table body (5), just the bottom fixedly connected with discharging pipe (6) of funnel (4), the top fixedly connected with agitator motor case (7) of reaction barrel (1), be equipped with agitator motor (8) in the inner cavity of agitator motor case (7), the one end threaded connection of agitator motor (8) has puddler (9), the outer wall fixedly connected with stirring piece (10) of puddler (9), just the upper left end fixedly connected with of reaction barrel (1) smashes case (11), the inner cavity fixedly connected with crushing mechanism (12) of smashing case (11), the left lower end of the crushing box (11) is fixedly connected with a pushing mechanism (13), the right side of the bottom end of the crushing box (11) is fixedly connected with a feeding pipe (14), the other end of the feeding pipe (14) penetrates through the reaction barrel (1) and is fixedly connected with the top end of the left wall of the reaction barrel (1), a liquid tank (15) is fixedly connected at the right end of the reaction barrel (1), a first liquid pumping pipe (16) is inserted into the inner cavity of the liquid tank (15), one end of the first liquid extraction pipe (16) extends to the outside through the liquid tank (15), and the other end of the first liquid extracting pipe (16) is fixedly connected with a water pump (17), the other end of the water pump (17) is inserted with a second liquid pumping pipe (18), the other end of the second liquid pumping pipe (18) is fixedly connected with the right side of the top end of the reaction barrel (1), and one end of the first liquid pumping pipe (16) far away from the liquid tank (15) is fixedly connected with a liquid supplementing pipe (19);
the crushing mechanism (12) comprises a crushing motor (121), a motor rotating shaft (122), a fine gear (123), a first coarse gear (124), a second coarse gear (125), a first rotating shaft (126), a second rotating shaft (127), a first crushing disc (128) and a second crushing disc (129), the crushing motor (121) is fixedly connected to the outer end of the crushing box (11), the motor rotating shaft (122) is in threaded connection with one end of the crushing motor (121), the fine gear (123) is fixedly connected to the other end of the motor rotating shaft (122), the first coarse gear (124) is clamped at one end of the fine gear (123), the first rotating shaft (126) is fixedly connected to one side of the first coarse gear (124), the first crushing disc (128) is fixedly connected to the other end of the first rotating shaft (126), and the end, far away from the fine gear (123), of the first coarse gear (124) is clamped with the second coarse gear (125), the second rotating shaft (127) is fixedly connected to one side of the second coarse gear (125), the second grinding disc (129) is fixedly connected to the other end of the second rotating shaft (127), and the first grinding disc (128) and the second grinding disc (129) are arranged in the inner cavity of the crushing box;
push mechanism (13) include cylinder (131), push rod (132), push jack (133), cylinder (131) fixed connection is at the left lower extreme of smashing case (11), push rod (132) cup joint the one end at cylinder (131), just push rod (132) run through and smash case (11) and extend to inside, push jack (133) fixed connection is at the other end of push rod (132).
2. The apparatus of claim 1, wherein the drum-type low-mercury catalyst preparation apparatus comprises: the left side of the top end of the reaction barrel (1) is fixedly connected with a pressure reduction hole (20).
3. The apparatus of claim 1, wherein the drum-type low-mercury catalyst preparation apparatus comprises: the left end of the reaction barrel (1) is fixedly connected with a liquid pressure gauge (21).
4. The apparatus of claim 1, wherein the drum-type low-mercury catalyst preparation apparatus comprises: the top end of the crushing box (11) is fixedly connected with a solid feeding hole (22).
5. The apparatus of claim 1, wherein the drum-type low-mercury catalyst preparation apparatus comprises: one end of the feeding pipe (14) is fixedly connected with a powder filter screen (23).
6. The apparatus of claim 1, wherein the drum-type low-mercury catalyst preparation apparatus comprises: one side of the discharge pipe (6) is in threaded connection with a flow control valve (24).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921904893.7U CN211216665U (en) | 2019-11-06 | 2019-11-06 | Drum-type low mercury catalyst preparation facilities |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921904893.7U CN211216665U (en) | 2019-11-06 | 2019-11-06 | Drum-type low mercury catalyst preparation facilities |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN211216665U true CN211216665U (en) | 2020-08-11 |
Family
ID=71914168
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201921904893.7U Expired - Fee Related CN211216665U (en) | 2019-11-06 | 2019-11-06 | Drum-type low mercury catalyst preparation facilities |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN211216665U (en) |
-
2019
- 2019-11-06 CN CN201921904893.7U patent/CN211216665U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200811 Termination date: 20211106 |
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| CF01 | Termination of patent right due to non-payment of annual fee |