CN211216615U - A reation kettle for synthesizing macromolecular material - Google Patents
A reation kettle for synthesizing macromolecular material Download PDFInfo
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- CN211216615U CN211216615U CN201921493963.4U CN201921493963U CN211216615U CN 211216615 U CN211216615 U CN 211216615U CN 201921493963 U CN201921493963 U CN 201921493963U CN 211216615 U CN211216615 U CN 211216615U
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- 239000000463 material Substances 0.000 title claims abstract description 15
- 230000002194 synthesizing effect Effects 0.000 title claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 47
- 238000003756 stirring Methods 0.000 claims abstract description 33
- 238000003466 welding Methods 0.000 claims abstract description 25
- 238000007789 sealing Methods 0.000 claims abstract description 24
- 239000002861 polymer material Substances 0.000 claims abstract description 22
- 230000005540 biological transmission Effects 0.000 claims description 27
- 239000000523 sample Substances 0.000 claims description 12
- 239000000126 substance Substances 0.000 abstract description 5
- 229920001059 synthetic polymer Polymers 0.000 abstract description 5
- 230000033001 locomotion Effects 0.000 abstract description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000003786 synthesis reaction Methods 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000007086 side reaction Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 206010024769 Local reaction Diseases 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000009878 intermolecular interaction Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
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Abstract
本实用新型公开了化工设备技术领域的一种用于合成高分子材料的反应釜,包括反应釜体和搅拌装置,所述反应釜体的左侧壁通过焊接固定有进料管,所述反应釜体的顶部通过焊接安装有密封板,所述密封板的顶部焊接固定有U型架,所述U型架顶部的底面通过螺栓安装有电机,所述电机通过外接导线与外接电源连通,所述反应釜体的底部通过焊接固定有多个支撑架;该用于合成高分子材料的反应釜的设置,结构设计合理,通过在反应釜体的内部安装超声波探头,超声波利用空化在合成高分子的材料中形成微射流,微射流能显著提高物质分子运动频率和速度,进而能够有效的增加高分子材料之间的反应速率,提高合成高分子材料的纯度。
The utility model discloses a reaction kettle for synthesizing polymer materials in the technical field of chemical equipment, comprising a reaction kettle body and a stirring device. A feed pipe is fixed on the left side wall of the reaction kettle body by welding. A sealing plate is installed on the top of the kettle body by welding, a U-shaped frame is welded and fixed on the top of the sealing plate, a motor is installed on the bottom surface of the top of the U-shaped frame by bolts, and the motor is connected with an external power supply through an external wire, so The bottom of the reaction kettle body is fixed with a plurality of support frames by welding; the setting of the reaction kettle for synthesizing polymer materials is reasonable in structure design. The micro-jet is formed in the molecular material, and the micro-jet can significantly increase the frequency and speed of the molecular motion of the substance, thereby effectively increasing the reaction rate between the polymer materials and improving the purity of the synthetic polymer material.
Description
技术领域technical field
本实用新型涉及化工设备技术领域,具体为一种用于合成高分子材料的反应釜。The utility model relates to the technical field of chemical equipment, in particular to a reaction kettle for synthesizing polymer materials.
背景技术Background technique
反应釜的广义理解即有物理或化学反应的容器,通过对容器的结构设计与参数配置,实现工艺要求的加热、蒸发、冷却及低高速的混配功能;反应釜广泛应用于石油、化工、橡胶、农药、染料、医药、食品行业。现有的反应釜存在一个严重的问题就是在合成的高分子材料时,由于是自由的进行反应,从而造成分子之间的反应速率较低,因此产生大量的副反应生成物,从而会影响合成高分子材料的纯度。The broad understanding of the reaction kettle is that there is a physical or chemical reaction container. Through the structural design and parameter configuration of the container, the heating, evaporation, cooling and low-speed mixing functions required by the process are realized; the reaction kettle is widely used in petroleum, chemical, Rubber, pesticide, dye, medicine, food industry. A serious problem in the existing reactor is that when synthesizing polymer materials, the reaction is carried out freely, resulting in a low reaction rate between molecules, so a large number of side reaction products are generated, which will affect the synthesis. The purity of the polymer material.
实用新型内容Utility model content
本实用新型的目的在于提供一种用于合成高分子材料的反应釜,以解决上述背景技术中提出的反应釜在合成的高分子材料时,由于是自由的进行反应,从而造成分子之间的反应速率较低,因此产生大量的副反应生成物,从而会影响合成高分子材料的纯度的问题。The purpose of this utility model is to provide a reaction kettle for synthesizing polymer materials, so as to solve the problem that the reaction kettle proposed in the above-mentioned background technology is free to react when synthesizing polymer materials, thereby causing the formation of inter-molecular interactions. The reaction rate is low, so a large number of side reaction products are produced, which will affect the purity of synthetic polymer materials.
为实现上述目的,本实用新型提供如下技术方案:一种用于合成高分子材料的反应釜,包括反应釜体和搅拌装置,所述反应釜体的左侧壁通过焊接固定有进料管,所述反应釜体的顶部通过焊接安装有密封板,所述密封板的顶部焊接固定有U型架,所述U型架顶部的底面通过螺栓安装有电机,所述电机通过外接导线与外接电源连通,所述反应釜体的底部通过焊接固定有多个支撑架,所述反应釜体底部中间位置通过焊接固定有出料管,所述搅拌装置焊接固定于传动轴的外侧壁,所述搅拌装置包括传动轴、搅拌桨和U型刮刀,所述传动轴的顶部通过轴承与所述密封板连接,所述传动轴贯穿所述密封板的顶部与所述电机啮合连接,所述传动轴的外侧壁通过螺纹连接有多个超声波探头,所述传动轴的内部开有空心腔,所述超声波探头的外接导线沿着所述空心腔与外接电源连通,所述搅拌桨焊接固定于所述传动轴下部外侧壁,所述U型刮刀通过焊接固定于所述传动轴的底部,所述U型刮刀与所述反应釜体的内侧壁接触。In order to achieve the above purpose, the utility model provides the following technical solutions: a reaction kettle for synthesizing polymer materials, comprising a reaction kettle body and a stirring device, the left side wall of the reaction kettle body is fixed with a feeding pipe by welding, A sealing plate is installed on the top of the reaction kettle body by welding, a U-shaped frame is welded and fixed on the top of the sealing plate, a motor is installed on the bottom surface of the top of the U-shaped frame through bolts, and the motor is connected to an external power supply through an external wire. The bottom of the reaction kettle body is fixed with a plurality of support frames by welding, the middle position of the bottom of the reaction kettle body is fixed with a discharge pipe by welding, and the stirring device is welded and fixed on the outer side wall of the transmission shaft. The device includes a transmission shaft, a stirring paddle and a U-shaped scraper, the top of the transmission shaft is connected with the sealing plate through a bearing, the transmission shaft penetrates through the top of the sealing plate and is engaged with the motor, and the transmission shaft is connected to the motor. The outer side wall is connected with a plurality of ultrasonic probes through threads, a hollow cavity is opened inside the transmission shaft, the external wire of the ultrasonic probe is connected with an external power supply along the hollow cavity, and the stirring paddle is welded and fixed to the transmission The outer side wall of the lower part of the shaft, the U-shaped scraper is fixed to the bottom of the transmission shaft by welding, and the U-shaped scraper is in contact with the inner side wall of the reaction kettle body.
优选的,所述进料管的左端通过螺纹连接有密封盖。Preferably, the left end of the feed pipe is connected with a sealing cover through a screw thread.
优选的,所述支撑架的数量为三个,三个所述支撑架呈现环形分布于所述反应釜体的底部。Preferably, the number of the support racks is three, and the three support racks are annularly distributed at the bottom of the reaction kettle body.
优选的,所述搅拌桨为曲形结构,所述搅拌桨的外侧壁通过焊接固定有多个三角板。Preferably, the stirring paddle has a curved structure, and a plurality of triangular plates are fixed on the outer side wall of the stirring paddle by welding.
与现有技术相比,本实用新型的有益效果是:该用于合成高分子材料的反应釜的设置,结构设计合理,通过在反应釜体的内部安装超声波探头,超声波利用空化在合成高分子的材料中形成微射流,微射流能显著提高物质分子运动频率和速度,进而能够有效的增加高分子材料之间的反应速率,提高合成高分子材料的纯度。Compared with the prior art, the beneficial effects of the present utility model are: the arrangement of the reaction kettle for synthesizing polymer materials, the structure design is reasonable, and the ultrasonic probe is installed inside the reaction kettle body, and the ultrasonic wave utilizes cavitation in the synthesis of high polymer materials. The micro-jet is formed in the molecular material, and the micro-jet can significantly increase the frequency and speed of the molecular motion of the substance, thereby effectively increasing the reaction rate between the polymer materials and improving the purity of the synthetic polymer material.
附图说明Description of drawings
图1为本实用新型结构示意图;Fig. 1 is the structural representation of the utility model;
图2为本实用新型反应釜体内部结构示意图;2 is a schematic diagram of the internal structure of the reactor body of the utility model;
图3为本实用新型第一传动轴内部结构示意图。3 is a schematic diagram of the internal structure of the first transmission shaft of the present invention.
图中:反应釜体100,进料管110,密封盖111,密封板120,支撑架130, U型架140,电机141,出料管150,搅拌装置200,传动轴210,超声波探头 211,空心腔212,搅拌桨220,三角板221,U型刮刀230。In the figure: the
具体实施方式Detailed ways
下面将结合本实用新型实施例中的附图,对本实用新型实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本实用新型一部分实施例,而不是全部的实施例。基于本实用新型中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本实用新型保护的范围。The technical solutions in the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all the implementations. example. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative work fall within the protection scope of the present invention.
反应釜体100的左侧壁通过焊接固定有进料管110,反应釜体100的顶部通过焊接安装有密封板120,密封板120的顶部焊接固定有U型架140,U型架140顶部的底面通过螺栓安装有电机141,电机141通过外接导线与外接电源连通,反应釜体100的底部通过焊接固定有多个支撑架130,反应釜体100 底部中间位置通过焊接固定有出料管150,本实用新型提供一种用于合成高分子材料的反应釜,用于在合成高分子材料后,再对材料进行不断地搅动,以防止材料发生沉淀而影响出料地质量,请参阅图1-3,包括反应釜体100、搅拌装置200和防沉淀装置300。The left side wall of the
请再参阅图1-3,反应釜体100的左侧壁通过焊接固定有进料管110,反应釜体100的顶部通过焊接安装有密封板120,密封板120的顶部焊接固定有 U型架140,U型架140顶部的底面通过螺栓安装有电机141,电机141通过外接导线与外接电源连通,反应釜体100的底部通过焊接固定有多个支撑架 130,反应釜体100底部中间位置通过焊接固定有出料管150,反应釜体100 用于储存反应的材料,进料管110向反应釜体100的内腔中导入反应材料,电机141用于带动搅拌装置200的转动。Please refer to FIGS. 1-3 again, the left side wall of the
请再参阅图2,搅拌装置200焊接固定于传动轴210的外侧壁,搅拌装置 200包括传动轴210、搅拌桨220和U型刮刀230,传动轴210的顶部通过轴承与密封板120连接,传动轴210贯穿密封板120的顶部与电机141啮合连接,传动轴210的外侧壁通过螺纹连接有多个超声波探头211,传动轴210的内部开有空心腔212,超声波探头211的外接导线沿着空心腔212与外接电源连通,搅拌桨220焊接固定于传动轴210下部外侧壁,U型刮刀230通过焊接固定于传动轴210的底部,U型刮刀230与反应釜体100的内侧壁接触,搅拌桨220和U型刮刀230用于对反应釜体100内腔的反应的材料进行搅拌,使其混合的更加均匀,超声波探头211用于产生微射流,加快反应釜体100内腔中的反应分子间的运动频率和速度,提高最终合成高分子材料为纯度。Please refer to FIG. 2 again, the stirring
请再参阅图1,为了对加料后的进料管110进行密封,进料管110的左端通过螺纹连接有密封盖111,密封盖111用于对反应釜体100的内腔进行密封。Please refer to FIG. 1 again, in order to seal the
请再参阅图1,为了对反应釜体100进行支撑,支撑架130的数量为三个,三个支撑架130呈现环形分布于反应釜体100的底部,三个支撑架130呈现三角分布于反应釜体100的底部,支撑架130用于保持反应釜体100的水平。Please refer to FIG. 1 again, in order to support the
请再参阅图2,为了提高液体的搅拌效率,搅拌桨220为曲形结构,搅拌桨220的外侧壁通过焊接固定有多个三角板221,三角板221用于增大搅拌桨 220与反应物的接触面积,以提高搅拌效率。Please refer to FIG. 2 again, in order to improve the stirring efficiency of the liquid, the
上述的第一螺纹槽、第二螺纹槽、支撑架130并不仅限于本实施例记载的具体数量,本技术领域人员在本装置能完成其搅拌功能的前提下,可以根据需要增加或减少其数量。The above-mentioned first thread groove, second thread groove, and
工作原理:打开密封盖111后将合成高分子的材料通过进料管110导进反应釜体100的内腔中,导进完成后再关闭密封盖111,打开电机141和超声波探头211的电源开关,电机141通过传动轴210带动超声波探头211、搅拌桨220、U型刮刀230进行转动,搅拌桨220在反应釜体100内腔的底部带动局部的反应材料转动使其产生水流,水流再依次向上传递进而达到对整体的材料搅拌,超声波探头211在材料中产生微射流,微射流增大反应材料分子运动频率和速度,促进材料的深度合成。Working principle: after opening the
虽然在上文中已经参考实施例对本实用新型进行了描述,然而在不脱离本实用新型的范围的情况下,可以对其进行各种改进并且可以用等效物替换其中的部件。尤其是,只要不存在结构冲突,本实用新型所披露的实施例中的各项特征均可通过任意方式相互结合起来使用,在本说明书中未对这些组合的情况进行穷举性的描述仅仅是出于省略篇幅和节约资源的考虑。因此,本实用新型并不局限于文中公开的特定实施例,而是包括落入权利要求的范围内的所有技术方案。Although the present invention has been described above with reference to the embodiments, various modifications may be made and equivalents may be substituted for parts thereof without departing from the scope of the invention. In particular, as long as there is no structural conflict, the various features in the disclosed embodiments of the present invention can be combined with each other in any way, and the description of these combinations is not exhaustive in this specification. For the sake of omitting space and saving resources. Therefore, the present invention is not limited to the specific embodiments disclosed herein, but includes all technical solutions falling within the scope of the claims.
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