CN211216615U - A reation kettle for synthesizing macromolecular material - Google Patents

A reation kettle for synthesizing macromolecular material Download PDF

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CN211216615U
CN211216615U CN201921493963.4U CN201921493963U CN211216615U CN 211216615 U CN211216615 U CN 211216615U CN 201921493963 U CN201921493963 U CN 201921493963U CN 211216615 U CN211216615 U CN 211216615U
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reaction kettle
fixed
welding
kettle body
transmission shaft
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丁巍
赵越
戴咏川
宋官龙
王洪浩
朱智琦
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Liaoning Shihua University
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Abstract

本实用新型公开了化工设备技术领域的一种用于合成高分子材料的反应釜,包括反应釜体和搅拌装置,所述反应釜体的左侧壁通过焊接固定有进料管,所述反应釜体的顶部通过焊接安装有密封板,所述密封板的顶部焊接固定有U型架,所述U型架顶部的底面通过螺栓安装有电机,所述电机通过外接导线与外接电源连通,所述反应釜体的底部通过焊接固定有多个支撑架;该用于合成高分子材料的反应釜的设置,结构设计合理,通过在反应釜体的内部安装超声波探头,超声波利用空化在合成高分子的材料中形成微射流,微射流能显著提高物质分子运动频率和速度,进而能够有效的增加高分子材料之间的反应速率,提高合成高分子材料的纯度。

Figure 201921493963

The utility model discloses a reaction kettle for synthesizing polymer materials in the technical field of chemical equipment, comprising a reaction kettle body and a stirring device. A feed pipe is fixed on the left side wall of the reaction kettle body by welding. A sealing plate is installed on the top of the kettle body by welding, a U-shaped frame is welded and fixed on the top of the sealing plate, a motor is installed on the bottom surface of the top of the U-shaped frame by bolts, and the motor is connected with an external power supply through an external wire, so The bottom of the reaction kettle body is fixed with a plurality of support frames by welding; the setting of the reaction kettle for synthesizing polymer materials is reasonable in structure design. The micro-jet is formed in the molecular material, and the micro-jet can significantly increase the frequency and speed of the molecular motion of the substance, thereby effectively increasing the reaction rate between the polymer materials and improving the purity of the synthetic polymer material.

Figure 201921493963

Description

一种用于合成高分子材料的反应釜A kind of reactor for synthesizing polymer materials

技术领域technical field

本实用新型涉及化工设备技术领域,具体为一种用于合成高分子材料的反应釜。The utility model relates to the technical field of chemical equipment, in particular to a reaction kettle for synthesizing polymer materials.

背景技术Background technique

反应釜的广义理解即有物理或化学反应的容器,通过对容器的结构设计与参数配置,实现工艺要求的加热、蒸发、冷却及低高速的混配功能;反应釜广泛应用于石油、化工、橡胶、农药、染料、医药、食品行业。现有的反应釜存在一个严重的问题就是在合成的高分子材料时,由于是自由的进行反应,从而造成分子之间的反应速率较低,因此产生大量的副反应生成物,从而会影响合成高分子材料的纯度。The broad understanding of the reaction kettle is that there is a physical or chemical reaction container. Through the structural design and parameter configuration of the container, the heating, evaporation, cooling and low-speed mixing functions required by the process are realized; the reaction kettle is widely used in petroleum, chemical, Rubber, pesticide, dye, medicine, food industry. A serious problem in the existing reactor is that when synthesizing polymer materials, the reaction is carried out freely, resulting in a low reaction rate between molecules, so a large number of side reaction products are generated, which will affect the synthesis. The purity of the polymer material.

实用新型内容Utility model content

本实用新型的目的在于提供一种用于合成高分子材料的反应釜,以解决上述背景技术中提出的反应釜在合成的高分子材料时,由于是自由的进行反应,从而造成分子之间的反应速率较低,因此产生大量的副反应生成物,从而会影响合成高分子材料的纯度的问题。The purpose of this utility model is to provide a reaction kettle for synthesizing polymer materials, so as to solve the problem that the reaction kettle proposed in the above-mentioned background technology is free to react when synthesizing polymer materials, thereby causing the formation of inter-molecular interactions. The reaction rate is low, so a large number of side reaction products are produced, which will affect the purity of synthetic polymer materials.

为实现上述目的,本实用新型提供如下技术方案:一种用于合成高分子材料的反应釜,包括反应釜体和搅拌装置,所述反应釜体的左侧壁通过焊接固定有进料管,所述反应釜体的顶部通过焊接安装有密封板,所述密封板的顶部焊接固定有U型架,所述U型架顶部的底面通过螺栓安装有电机,所述电机通过外接导线与外接电源连通,所述反应釜体的底部通过焊接固定有多个支撑架,所述反应釜体底部中间位置通过焊接固定有出料管,所述搅拌装置焊接固定于传动轴的外侧壁,所述搅拌装置包括传动轴、搅拌桨和U型刮刀,所述传动轴的顶部通过轴承与所述密封板连接,所述传动轴贯穿所述密封板的顶部与所述电机啮合连接,所述传动轴的外侧壁通过螺纹连接有多个超声波探头,所述传动轴的内部开有空心腔,所述超声波探头的外接导线沿着所述空心腔与外接电源连通,所述搅拌桨焊接固定于所述传动轴下部外侧壁,所述U型刮刀通过焊接固定于所述传动轴的底部,所述U型刮刀与所述反应釜体的内侧壁接触。In order to achieve the above purpose, the utility model provides the following technical solutions: a reaction kettle for synthesizing polymer materials, comprising a reaction kettle body and a stirring device, the left side wall of the reaction kettle body is fixed with a feeding pipe by welding, A sealing plate is installed on the top of the reaction kettle body by welding, a U-shaped frame is welded and fixed on the top of the sealing plate, a motor is installed on the bottom surface of the top of the U-shaped frame through bolts, and the motor is connected to an external power supply through an external wire. The bottom of the reaction kettle body is fixed with a plurality of support frames by welding, the middle position of the bottom of the reaction kettle body is fixed with a discharge pipe by welding, and the stirring device is welded and fixed on the outer side wall of the transmission shaft. The device includes a transmission shaft, a stirring paddle and a U-shaped scraper, the top of the transmission shaft is connected with the sealing plate through a bearing, the transmission shaft penetrates through the top of the sealing plate and is engaged with the motor, and the transmission shaft is connected to the motor. The outer side wall is connected with a plurality of ultrasonic probes through threads, a hollow cavity is opened inside the transmission shaft, the external wire of the ultrasonic probe is connected with an external power supply along the hollow cavity, and the stirring paddle is welded and fixed to the transmission The outer side wall of the lower part of the shaft, the U-shaped scraper is fixed to the bottom of the transmission shaft by welding, and the U-shaped scraper is in contact with the inner side wall of the reaction kettle body.

优选的,所述进料管的左端通过螺纹连接有密封盖。Preferably, the left end of the feed pipe is connected with a sealing cover through a screw thread.

优选的,所述支撑架的数量为三个,三个所述支撑架呈现环形分布于所述反应釜体的底部。Preferably, the number of the support racks is three, and the three support racks are annularly distributed at the bottom of the reaction kettle body.

优选的,所述搅拌桨为曲形结构,所述搅拌桨的外侧壁通过焊接固定有多个三角板。Preferably, the stirring paddle has a curved structure, and a plurality of triangular plates are fixed on the outer side wall of the stirring paddle by welding.

与现有技术相比,本实用新型的有益效果是:该用于合成高分子材料的反应釜的设置,结构设计合理,通过在反应釜体的内部安装超声波探头,超声波利用空化在合成高分子的材料中形成微射流,微射流能显著提高物质分子运动频率和速度,进而能够有效的增加高分子材料之间的反应速率,提高合成高分子材料的纯度。Compared with the prior art, the beneficial effects of the present utility model are: the arrangement of the reaction kettle for synthesizing polymer materials, the structure design is reasonable, and the ultrasonic probe is installed inside the reaction kettle body, and the ultrasonic wave utilizes cavitation in the synthesis of high polymer materials. The micro-jet is formed in the molecular material, and the micro-jet can significantly increase the frequency and speed of the molecular motion of the substance, thereby effectively increasing the reaction rate between the polymer materials and improving the purity of the synthetic polymer material.

附图说明Description of drawings

图1为本实用新型结构示意图;Fig. 1 is the structural representation of the utility model;

图2为本实用新型反应釜体内部结构示意图;2 is a schematic diagram of the internal structure of the reactor body of the utility model;

图3为本实用新型第一传动轴内部结构示意图。3 is a schematic diagram of the internal structure of the first transmission shaft of the present invention.

图中:反应釜体100,进料管110,密封盖111,密封板120,支撑架130, U型架140,电机141,出料管150,搅拌装置200,传动轴210,超声波探头 211,空心腔212,搅拌桨220,三角板221,U型刮刀230。In the figure: the reactor body 100, the feeding pipe 110, the sealing cover 111, the sealing plate 120, the support frame 130, the U-shaped frame 140, the motor 141, the discharge pipe 150, the stirring device 200, the transmission shaft 210, the ultrasonic probe 211, Hollow cavity 212, stirring paddle 220, triangular plate 221, U-shaped scraper 230.

具体实施方式Detailed ways

下面将结合本实用新型实施例中的附图,对本实用新型实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本实用新型一部分实施例,而不是全部的实施例。基于本实用新型中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本实用新型保护的范围。The technical solutions in the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all the implementations. example. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative work fall within the protection scope of the present invention.

反应釜体100的左侧壁通过焊接固定有进料管110,反应釜体100的顶部通过焊接安装有密封板120,密封板120的顶部焊接固定有U型架140,U型架140顶部的底面通过螺栓安装有电机141,电机141通过外接导线与外接电源连通,反应釜体100的底部通过焊接固定有多个支撑架130,反应釜体100 底部中间位置通过焊接固定有出料管150,本实用新型提供一种用于合成高分子材料的反应釜,用于在合成高分子材料后,再对材料进行不断地搅动,以防止材料发生沉淀而影响出料地质量,请参阅图1-3,包括反应釜体100、搅拌装置200和防沉淀装置300。The left side wall of the reaction kettle body 100 is fixed with the feeding pipe 110 by welding, the top of the reaction kettle body 100 is installed with a sealing plate 120 by welding, the top of the sealing plate 120 is welded and fixed with a U-shaped frame 140, and the top of the U-shaped frame 140 is fixed with a U-shaped frame 140. A motor 141 is installed on the bottom surface through bolts, the motor 141 is connected to an external power supply through an external wire, a plurality of support frames 130 are fixed at the bottom of the reactor body 100 by welding, and a discharge pipe 150 is fixed at the middle position of the bottom of the reactor body 100 by welding, The utility model provides a reaction kettle for synthesizing polymer materials, which is used for continuously stirring the materials after synthesizing the polymer materials, so as to prevent the materials from precipitation and affecting the quality of the discharged materials, please refer to Fig. 1- 3, including the reaction kettle body 100 , the stirring device 200 and the anti-settling device 300 .

请再参阅图1-3,反应釜体100的左侧壁通过焊接固定有进料管110,反应釜体100的顶部通过焊接安装有密封板120,密封板120的顶部焊接固定有 U型架140,U型架140顶部的底面通过螺栓安装有电机141,电机141通过外接导线与外接电源连通,反应釜体100的底部通过焊接固定有多个支撑架 130,反应釜体100底部中间位置通过焊接固定有出料管150,反应釜体100 用于储存反应的材料,进料管110向反应釜体100的内腔中导入反应材料,电机141用于带动搅拌装置200的转动。Please refer to FIGS. 1-3 again, the left side wall of the reaction kettle body 100 is fixed with the feeding pipe 110 by welding, the top of the reaction kettle body 100 is mounted with the sealing plate 120 by welding, and the top of the sealing plate 120 is welded and fixed with a U-shaped frame 140, a motor 141 is installed on the bottom surface of the top of the U-shaped frame 140 through bolts, the motor 141 is connected with an external power supply through an external wire, the bottom of the reactor body 100 is fixed with a plurality of support frames 130 by welding, and the middle position of the bottom of the reactor body 100 passes through. A discharge pipe 150 is welded and fixed. The reaction kettle body 100 is used to store the reacted materials. The feed pipe 110 introduces the reaction material into the inner cavity of the reaction kettle body 100 . The motor 141 is used to drive the rotation of the stirring device 200 .

请再参阅图2,搅拌装置200焊接固定于传动轴210的外侧壁,搅拌装置 200包括传动轴210、搅拌桨220和U型刮刀230,传动轴210的顶部通过轴承与密封板120连接,传动轴210贯穿密封板120的顶部与电机141啮合连接,传动轴210的外侧壁通过螺纹连接有多个超声波探头211,传动轴210的内部开有空心腔212,超声波探头211的外接导线沿着空心腔212与外接电源连通,搅拌桨220焊接固定于传动轴210下部外侧壁,U型刮刀230通过焊接固定于传动轴210的底部,U型刮刀230与反应釜体100的内侧壁接触,搅拌桨220和U型刮刀230用于对反应釜体100内腔的反应的材料进行搅拌,使其混合的更加均匀,超声波探头211用于产生微射流,加快反应釜体100内腔中的反应分子间的运动频率和速度,提高最终合成高分子材料为纯度。Please refer to FIG. 2 again, the stirring device 200 is welded and fixed to the outer side wall of the transmission shaft 210. The stirring device 200 includes a transmission shaft 210, a stirring paddle 220 and a U-shaped scraper 230. The top of the transmission shaft 210 is connected to the sealing plate 120 through a bearing, and the transmission The shaft 210 penetrates through the top of the sealing plate 120 and is engaged with the motor 141 , the outer side wall of the transmission shaft 210 is connected with a plurality of ultrasonic probes 211 through threads, a hollow cavity 212 is opened inside the transmission shaft 210 , and the external wire of the ultrasonic probe 211 is along the hollow. The cavity 212 is communicated with an external power source, the stirring paddle 220 is welded and fixed to the lower outer wall of the transmission shaft 210, the U-shaped scraper 230 is fixed to the bottom of the transmission shaft 210 by welding, and the U-shaped scraper 230 is in contact with the inner wall of the reactor body 100, and the stirring paddle 220 and the U-shaped scraper 230 are used to stir the reacted materials in the inner cavity of the reactor body 100 to make the mixing more uniform, and the ultrasonic probe 211 is used to generate micro-jets to speed up the reaction molecules in the inner cavity of the reactor body 100. The frequency and speed of movement improve the purity of the final synthetic polymer material.

请再参阅图1,为了对加料后的进料管110进行密封,进料管110的左端通过螺纹连接有密封盖111,密封盖111用于对反应釜体100的内腔进行密封。Please refer to FIG. 1 again, in order to seal the feeding pipe 110 after feeding, the left end of the feeding pipe 110 is screwed with a sealing cover 111 , and the sealing cover 111 is used to seal the inner cavity of the reactor body 100 .

请再参阅图1,为了对反应釜体100进行支撑,支撑架130的数量为三个,三个支撑架130呈现环形分布于反应釜体100的底部,三个支撑架130呈现三角分布于反应釜体100的底部,支撑架130用于保持反应釜体100的水平。Please refer to FIG. 1 again, in order to support the reaction kettle body 100 , the number of the support frames 130 is three, the three support frames 130 are distributed in a ring shape at the bottom of the reaction kettle body 100 , and the three support frames 130 are distributed in a triangular shape at the bottom of the reaction kettle body 100 . At the bottom of the kettle body 100 , the support frame 130 is used to maintain the level of the reactor body 100 .

请再参阅图2,为了提高液体的搅拌效率,搅拌桨220为曲形结构,搅拌桨220的外侧壁通过焊接固定有多个三角板221,三角板221用于增大搅拌桨 220与反应物的接触面积,以提高搅拌效率。Please refer to FIG. 2 again, in order to improve the stirring efficiency of the liquid, the stirring paddle 220 has a curved structure, and the outer side wall of the stirring paddle 220 is fixed with a plurality of triangular plates 221 by welding, and the triangular plates 221 are used to increase the contact between the stirring paddle 220 and the reactant area to improve stirring efficiency.

上述的第一螺纹槽、第二螺纹槽、支撑架130并不仅限于本实施例记载的具体数量,本技术领域人员在本装置能完成其搅拌功能的前提下,可以根据需要增加或减少其数量。The above-mentioned first thread groove, second thread groove, and support frame 130 are not limited to the specific numbers recorded in this embodiment. Those skilled in the art can increase or decrease the number of them as required under the premise that the device can complete its stirring function. .

工作原理:打开密封盖111后将合成高分子的材料通过进料管110导进反应釜体100的内腔中,导进完成后再关闭密封盖111,打开电机141和超声波探头211的电源开关,电机141通过传动轴210带动超声波探头211、搅拌桨220、U型刮刀230进行转动,搅拌桨220在反应釜体100内腔的底部带动局部的反应材料转动使其产生水流,水流再依次向上传递进而达到对整体的材料搅拌,超声波探头211在材料中产生微射流,微射流增大反应材料分子运动频率和速度,促进材料的深度合成。Working principle: after opening the sealing cover 111, the synthetic polymer material is introduced into the inner cavity of the reactor body 100 through the feeding pipe 110, and after the introduction is completed, the sealing cover 111 is closed, and the power switches of the motor 141 and the ultrasonic probe 211 are turned on. , the motor 141 drives the ultrasonic probe 211, the stirring paddle 220, and the U-shaped scraper 230 to rotate through the transmission shaft 210, and the stirring paddle 220 drives the local reaction material to rotate at the bottom of the inner cavity of the reactor body 100 to generate water flow, and the water flow goes upward in turn. Transfer and then achieve overall material agitation, the ultrasonic probe 211 generates a micro-jet in the material, and the micro-jet increases the molecular motion frequency and speed of the reaction material and promotes the deep synthesis of the material.

虽然在上文中已经参考实施例对本实用新型进行了描述,然而在不脱离本实用新型的范围的情况下,可以对其进行各种改进并且可以用等效物替换其中的部件。尤其是,只要不存在结构冲突,本实用新型所披露的实施例中的各项特征均可通过任意方式相互结合起来使用,在本说明书中未对这些组合的情况进行穷举性的描述仅仅是出于省略篇幅和节约资源的考虑。因此,本实用新型并不局限于文中公开的特定实施例,而是包括落入权利要求的范围内的所有技术方案。Although the present invention has been described above with reference to the embodiments, various modifications may be made and equivalents may be substituted for parts thereof without departing from the scope of the invention. In particular, as long as there is no structural conflict, the various features in the disclosed embodiments of the present invention can be combined with each other in any way, and the description of these combinations is not exhaustive in this specification. For the sake of omitting space and saving resources. Therefore, the present invention is not limited to the specific embodiments disclosed herein, but includes all technical solutions falling within the scope of the claims.

Claims (4)

1.一种用于合成高分子材料的反应釜,其特征在于:包括反应釜体(100)和搅拌装置(200),所述反应釜体(100)的左侧壁通过焊接固定有进料管(110),所述反应釜体(100)的顶部通过焊接安装有密封板(120),所述密封板(120)的顶部焊接固定有U型架(140),所述U型架(140)顶部的底面通过螺栓安装有电机(141),所述电机(141)通过外接导线与外接电源连通,所述反应釜体(100)的底部通过焊接固定有多个支撑架(130),所述反应釜体(100)底部中间位置通过焊接固定有出料管(150),所述搅拌装置(200)焊接固定于传动轴(210)的外侧壁,所述搅拌装置(200)包括传动轴(210)、搅拌桨(220)和U型刮刀(230),所述传动轴(210)的顶部通过轴承与所述密封板(120)连接,所述传动轴(210)贯穿所述密封板(120)的顶部与所述电机(141)啮合连接,所述传动轴(210)的外侧壁通过螺纹连接有多个超声波探头(211),所述传动轴(210)的内部开有空心腔(212),所述超声波探头(211)的外接导线沿着所述空心腔(212)与外接电源连通,所述搅拌桨(220)焊接固定于所述传动轴(210)下部外侧壁,所述U型刮刀(230)通过焊接固定于所述传动轴(210)的底部,所述U型刮刀(230)与所述反应釜体(100)的内侧壁接触。1. a reaction kettle for synthesizing macromolecular materials is characterized in that: comprising a reaction kettle body (100) and a stirring device (200), and the left side wall of the reaction kettle body (100) is fixed with a feed by welding A pipe (110), a sealing plate (120) is installed on the top of the reaction kettle body (100) by welding, and a U-shaped frame (140) is fixed on the top of the sealing plate (120) by welding, and the U-shaped frame ( 140) A motor (141) is installed on the bottom surface of the top through bolts, the motor (141) is communicated with an external power supply through an external wire, and a plurality of support frames (130) are fixed on the bottom of the reactor body (100) by welding, A discharge pipe (150) is fixed by welding at the middle position of the bottom of the reaction kettle body (100), and the stirring device (200) is welded and fixed on the outer side wall of the transmission shaft (210), and the stirring device (200) includes a transmission A shaft (210), a stirring paddle (220) and a U-shaped scraper (230), the top of the transmission shaft (210) is connected with the sealing plate (120) through a bearing, and the transmission shaft (210) penetrates the sealing The top of the plate (120) is engaged with the motor (141), the outer side wall of the transmission shaft (210) is connected with a plurality of ultrasonic probes (211) through threads, and the transmission shaft (210) has a hollow inside a cavity (212), the external wire of the ultrasonic probe (211) is communicated with an external power source along the hollow cavity (212), and the stirring paddle (220) is welded and fixed to the lower outer wall of the transmission shaft (210), The U-shaped scraper (230) is fixed to the bottom of the transmission shaft (210) by welding, and the U-shaped scraper (230) is in contact with the inner wall of the reaction kettle body (100). 2.根据权利要求1所述的一种用于合成高分子材料的反应釜,其特征在于:所述进料管(110)的左端通过螺纹连接有密封盖(111)。2 . The reaction kettle for synthesizing polymer materials according to claim 1 , wherein the left end of the feed pipe ( 110 ) is connected with a sealing cover ( 111 ) through threads. 3 . 3.根据权利要求1所述的一种用于合成高分子材料的反应釜,其特征在于:所述支撑架(130)的数量为三个,三个所述支撑架(130)呈现环形分布于所述反应釜体(100)的底部。3 . The reactor for synthesizing polymer materials according to claim 1 , wherein the number of the support frames ( 130 ) is three, and the three support frames ( 130 ) are distributed in an annular shape. 4 . at the bottom of the reactor body (100). 4.根据权利要求1所述的一种用于合成高分子材料的反应釜,其特征在于:所述搅拌桨(220)为曲形结构,所述搅拌桨(220)的外侧壁通过焊接固定有多个三角板(221)。4. The reactor for synthesizing polymer materials according to claim 1, wherein the stirring paddle (220) has a curved structure, and the outer wall of the stirring paddle (220) is fixed by welding There are multiple triangular plates (221).
CN201921493963.4U 2019-09-09 2019-09-09 A reation kettle for synthesizing macromolecular material Expired - Fee Related CN211216615U (en)

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