CN211159238U - CO with detection function2Removing device - Google Patents

CO with detection function2Removing device Download PDF

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Publication number
CN211159238U
CN211159238U CN201921230449.1U CN201921230449U CN211159238U CN 211159238 U CN211159238 U CN 211159238U CN 201921230449 U CN201921230449 U CN 201921230449U CN 211159238 U CN211159238 U CN 211159238U
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China
Prior art keywords
pipe
air outlet
valve
removing device
detection
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Active
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CN201921230449.1U
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Chinese (zh)
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陈奇
潘云辉
李想
金玉平
项葛浚
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Hangzhou lanran Technology Co.,Ltd.
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Hangzhou Lanran Environmental Technology Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02CCAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00Capture or disposal of greenhouse gases
    • Y02C20/40Capture or disposal of greenhouse gases of CO2

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  • Gas Separation By Absorption (AREA)

Abstract

The utility model discloses a CO that area detected2The removing device, the purifying device mainly includes: feed pipe, air outlet pipe, air inlet pipe, absorption tank and CO2Detection device, safeties and prevent suck-back device. The device removes CO in air contacting with materials2To solve the problem of CO adsorption of materials in the experiment or production process2Resulting in impure or deteriorated materials. At the same time, the device is provided with CO2A detection device, canTimely reminding of replacing the adsorbent, convenient replacement of the adsorbent, and capability of preventing reverse absorption2Pollution, and meeting the requirements of experiments and production.

Description

CO with detection function2Removing device
Technical Field
The utility model relates to a carbon dioxide remove device, especially an experiment remove device that is applied to and requires extremely low to in-process carbon dioxide concentration.
Background
Carbon dioxide is a carbon oxide, is a colorless and odorless gas at normal temperature and pressure, is one of the components of air, and accounts for about 0.03-0.04% of the total volume of air. Carbon dioxide belongs to acidic oxides, and is carbonic acid and carbonic anhydride generated by reaction with water, so that the alkali liquor can easily absorb CO2Therefore, CO in the air was used in the experiment of the high purity solution2May cause the impurity of the feed liquid and even the deterioration, such as the adsorption of excessive CO in the lithium hydroxide concentration experiment2Easy to form L i2CO3Precipitation caused the failure of the experiment. Therefore, necessary measures are taken to prevent CO2The impact on experimentation and production is also a very critical step.
Common CO at present2The removing means is that a gas washing bottle containing NaOH concentrated solution is introduced for gas washing, and CO cannot be ensured in the process2The problems of clean removal and when to change the solution, as well as the occurrence of suck-back when the scrubbing is stopped. Existing CO2As a removing device, for example, a CO disclosed in Chinese patent 201610167846.32The removing device is characterized in that: comprises an air inlet module and CO2Purification module and the module of giving vent to anger. The purification device improves the biological bulk density and the light energy utilization rate.
In practical applications, part of the experimental or production process requires CO2The concentration is maintained at a very low level, and the above patent fails to make CO into a solution by biological purification2To extremely low levels and no detection means to ensure CO2The level of the concentration of the active ingredient,the experiment is easy to fail or qualified products cannot be produced.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the technical problem existing in the prior art and providing a CO with detection2A removing device for ensuring CO by adding an aeration device and a safety device at the tail end of the air inlet pipe2Removal effect, with addition of CO before the safety device2An alarm device is detected to determine when the absorbent is replaced.
The utility model discloses concrete scheme is as follows:
CO with detection function2The removing device comprises a feeding pipe, an air inlet pipe and CO2The device comprises a detection device, a safety device, an air outlet pipe, a discharge pipe, a microporous aerator, an absorption tank, a feed valve, a drain valve, a first one-way exhaust valve and a second one-way intake valve; the absorption tank is connected with the inlet pipe, a feed valve for controlling the on-off of the pipeline is arranged on the inlet pipe, a liquid discharge pipe is arranged at the bottom of the absorption tank, a liquid discharge valve for controlling the liquid discharge is arranged on the liquid discharge pipe, the air inlet pipe extends into the absorption tank, the tail end of the air inlet pipe is connected with a microporous aerator, and the CO outlet pipe is sequentially connected with a CO outlet pipe2The device comprises a detection device, a safety device and a first one-way exhaust valve, wherein one end of an air outlet pipe is communicated with the headspace of an absorption tank, the other end of the air outlet pipe is an air outlet, a pipeline between the first one-way exhaust valve and the air outlet is connected with a pressure relief branch, and a second one-way air inlet valve is arranged at the upstream of a pressure relief port at the tail end of the pressure relief branch; the one-way exhaust direction of the first one-way exhaust valve is from the safety device to the air outlet, and the one-way exhaust direction of the second one-way intake valve is from the air outlet to the pressure relief port.
Preferably, said CO is2The pipeline material used by the removing device is acid-resistant and alkali-resistant material.
Preferably, the safety device is a closed container with an inlet and an outlet, and the container is filled with solid CO2Adsorbing the particles.
Furthermore, the closed container is a spherical or cylindrical glass container.
Further, the solid CO2Adsorption particlesIs one or more of solid NaOH, CaO and soda lime particles.
Preferably, the height of the microporous aerator in the absorption tank is lower than that of the air inlet at one end of the air outlet pipe.
Furthermore, the air inlet pipe is connected with an air pump device.
Preferably, the absorption tank is stored with alkali liquor, and the liquid level of the alkali liquor is higher than the microporous aerator but lower than the air inlet of the air outlet pipe.
Preferably, the microporous aerator is a hollow glass tube with a plurality of micropores with the aperture of 1-1.5 mm formed on the tube wall.
Preferably, said CO is2The detection device adopts infrared CO2Detection device or chemical CO2And (4) a detection device.
The device removes CO in air contacting with materials2To solve the problem of CO adsorption of materials in the experiment or production process2Resulting in impure or deteriorated materials, and the device is provided with CO2The detection device can prompt the absorption liquid in the absorption tank to be replaced in time, is convenient to replace by combining the absorption liquid, and has the characteristic of preventing reverse absorption, so that the safety of the material is ensured not to be influenced by CO2Pollution, and meeting the requirements of experiments and production.
Drawings
FIG. 1 shows a CO with detection2Structure of removing device
The reference numbers in the figures illustrate: feed pipe 1, inlet pipe 2, CO2The device comprises a detection device 3, a safety device 4, an air outlet pipe 5, a discharge pipe 6, a microporous aerator 7, an absorption tank 8, a feeding valve 9, a liquid discharge valve 10, a first one-way exhaust valve 11 and a second one-way intake valve 12.
Detailed Description
The present invention will be further described with reference to the accompanying drawings and the following detailed description.
As shown in FIG. 1, it is a kind of CO with detection2The structure of the removing device is schematically shown, and the main structure of the removing device comprises a feeding pipe 1, an air inlet pipe 2 and CO2Detection device 3, safety device 4, air outlet pipe 5, discharge pipe 6, microporous aerator 7, absorption tank 8 and feeding materialA valve 9, a drain valve 10, a first one-way exhaust valve 11 and a second one-way intake valve 12, wherein the feed pipe 1 is connected with the absorption tank 8, the feed pipe 1 is provided with the feed valve 9 for controlling the on-off of the pipeline, carbon dioxide absorption liquid can be introduced into the absorption tank 8 through the feed pipe 1, and the carbon dioxide absorption liquid can be NaOH or KOH solution or Ca (OH) solution with the concentration of more than 0.5 mol/L2One or more of alkaline concentrated solutions such as suspension. The bottom of the absorption tank 8 is provided with a liquid discharge pipe 6, and the liquid discharge pipe 6 is provided with a liquid discharge valve 10 for controlling liquid discharge. The air inlet pipe 2 extends into the absorption tank 8, and the tail end of the air inlet pipe is connected with a microporous aerator 7 so as to reduce the size of bubbles and strengthen the absorption and removal of carbon dioxide. The tail end of the air inlet pipe 2 can be connected with an air pump device for blowing air into the absorption tank 8 to remove CO2. In the invention, the microporous aerator 7 can adopt a hollow glass tube with a plurality of micropores with the aperture of 1-1.5 mm on the tube wall. The gas outlet pipe 5 is sequentially connected with CO2The detection device 3, the safety device 4 and the first one-way exhaust valve 11. One end of the air outlet pipe 5 is communicated with the headspace of the absorption tank 8 to ensure that the headspace does not extend below the liquid level, and the other end is an air outlet. The height of the microporous aerator 7 in the absorption tank 8 is lower than the air inlet at one end of the air outlet pipe 5 by a certain distance. The carbon dioxide absorbing liquid stored in the absorption tank 8 should be kept at a proper height, and the liquid level should be kept to submerge the microporous aerator 7 but be lower than the air inlet of the air outlet pipe 5. In order to ensure that the fluctuating liquid level does not touch the air inlet during aeration, the liquid level is preferably 0.5-1 cm lower than the air inlet of the air outlet pipe 5.
CO in the present invention2The detection device 3 adopts infrared CO2Detection device or chemical CO2The detection device can adopt any CO in the prior art2The detection equipment is realized, and equipment capable of directly displaying digital is preferably adopted, so that real-time viewing is facilitated. The safety device 4 is a closed container with an inlet and an outlet, and the container is filled with solid CO2Adsorbing particles, wherein the closed container is a spherical or cylindrical glass container, and solid CO is filled in the glass container2The adsorption particles can be one or more of solid NaOH, CaO and soda lime particles, as long as CO can be efficiently adsorbed2And (4) finishing.
A pressure relief branch is connected to the pipeline between the first one-way exhaust valve 11 and the air outlet, and a second one-way intake valve 12 is arranged at the upstream of the pressure relief opening at the tail end of the pressure relief branch. The purpose of the pressure relief branch is to prevent liquid in the experimental equipment from flowing back when the air pressure in the experimental equipment is large, and to avoid polluting the safety device 4. The one-way exhaust direction of the first one-way exhaust valve 11 is from the safety device 4 to the air outlet, and the exhaust cannot be performed in the opposite direction; the second unidirectional air intake valve 12 is configured to exhaust air in a unidirectional direction from the air outlet to the pressure relief port and not to exhaust air in the opposite direction.
To ensure the life of the entire plant, CO2The pipeline material and the valve used by the removing device are acid-resistant and alkali-resistant materials. One method of use of the device is described below:
before operation, the safety device 4 is filled with CaO solid particles and is installed according to the figure 1. And opening a feed valve 9, closing a liquid discharge valve 10, injecting about half of the volume of NaOH concentrated solution into the absorption tank 8, and closing the feed valve 9 when the liquid level is better to submerge 3cm above the microporous aerator 7 and is 0.5-1 cm below the air inlet of the air outlet pipe 5. The air inlet pipe 2 is connected with a small air pump to blow air into the equipment, and the air is uniformly dispersed in NaOH concentrated solution through the microporous aerator 7 from the air inlet pipe 2 at the moment to remove CO2The air passes through CO2The detection device 3 detects CO therein2The content is pumped into the experimental equipment from the air outlet of the air outlet pipe 5 through the safety device 4 along the air outlet pipe 5, and the ventilation ensures that no CO exists in the experimental equipment2Then the subsequent experiment can be carried out.
If the adsorption saturation of the NaOH concentrated solution occurs in the experimental process, CO2The detection device 3 will detect CO2The component is mixed and the alarm is given, and the equipment can still purify CO because CaO filled in the safety device 4 has the adsorption function2. The feed valve 9 and the drain valve 10 are opened to replace the absorption liquid, and the experiment can be normally and continuously carried out without suspending in the process of replacing the absorption liquid.
After the experiment is finished, the air pump is closed after the connection between the air outlet and the experimental equipment is cut off, and suck-back is prevented. If the air pump is stopped carelessly, the experimental equipment may have a backflow condition with a large air pressure, and due to the action of the first one-way exhaust valve 11 and the second one-way exhaust valve 12, the backflow fluid can be discharged from the first one-way exhaust valve 11 through the pressure relief opening, and cannot pass through the second one-way exhaust valve 12 to react with CaO in the safety device 4 to pollute the experimental material liquid.
The above-mentioned embodiments are only used for explaining the present invention, and are not intended to limit the present invention in any form, and any modifications, equivalent replacements, improvements, etc. made by the present invention are within the protection scope of the present invention without exceeding the technical solutions recorded in the claims.

Claims (10)

1. CO with detection function2The removing device is characterized by comprising a feeding pipe (1), an air inlet pipe (2) and CO2The device comprises a detection device (3), a safety device (4), an air outlet pipe (5), a discharge pipe (6), a microporous aerator (7), an absorption tank (8), a feeding valve (9), a liquid discharge valve (10), a first one-way exhaust valve (11) and a second one-way intake valve (12); inlet pipe (1) connect absorption tank (8), be equipped with feed valve (9) of control pipeline break-make on inlet pipe (1), absorption tank (8) bottom is equipped with row material pipe (6), is equipped with flowing back valve (10) of control flowing back on arranging material pipe (6), intake pipe (2) stretch into in absorption tank (8) and end-to-end connection has micropore aerator (7), connect gradually CO on outlet duct (5)2The device comprises a detection device (3), a safety device (4) and a first one-way exhaust valve (11), wherein one end of an air outlet pipe (5) is communicated with the headspace of an absorption tank (8), the other end of the air outlet pipe is an air outlet, a pipeline between the first one-way exhaust valve (11) and the air outlet is connected with a pressure relief branch, and a second one-way intake valve (12) is arranged at the upstream of a pressure relief opening at the tail end of the pressure relief branch; the one-way exhaust direction of the first one-way exhaust valve (11) flows from the safety device (4) to the air outlet, and the one-way exhaust direction of the second one-way intake valve (12) flows from the air outlet to the pressure relief opening.
2. CO with detection according to claim 12The removing device is characterized in that the CO is removed2The pipeline material used by the removing device is acid-resistant and alkali-resistant material.
3. CO with detection according to claim 12The removing device is characterized in that the safety device (4) is a closed container with an inlet and an outlet, and solid CO is filled in the container2Adsorbing the particles.
4. CO with detection according to claim 32The removing device is characterized in that the closed container is a spherical or cylindrical glass container.
5. CO with detection according to claim 32The removing device is characterized in that the solid CO is2The adsorption particles are one or more of solid NaOH, CaO and soda lime particles.
6. CO with detection according to claim 12The removing device is characterized in that the height of the microporous aerator (7) in the absorption tank (8) is lower than that of the air inlet at one end of the air outlet pipe (5).
7. CO with detection according to claim 62The removing device is characterized in that the air inlet pipe (2) is connected with an air pump device.
8. CO with detection according to claim 12The removing device is characterized in that carbon dioxide absorption liquid is stored in the absorption tank (8), and the liquid level is higher than the microporous aerator (7) but lower than the air inlet of the air outlet pipe (5).
9. CO with detection according to claim 12The removing device is characterized in that the microporous aerator (7) is a hollow glass tube with a plurality of micropores with the aperture of 1-1.5 mm formed on the tube wall.
10. CO with detection according to claim 12The removing device is characterized in that the CO is removed2The detection device (3) adopts infrared CO2Detection device or chemical CO2And (4) a detection device.
CN201921230449.1U 2019-07-31 2019-07-31 CO with detection function2Removing device Active CN211159238U (en)

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Application Number Priority Date Filing Date Title
CN201921230449.1U CN211159238U (en) 2019-07-31 2019-07-31 CO with detection function2Removing device

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Application Number Priority Date Filing Date Title
CN201921230449.1U CN211159238U (en) 2019-07-31 2019-07-31 CO with detection function2Removing device

Publications (1)

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CN211159238U true CN211159238U (en) 2020-08-04

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116099326A (en) * 2023-03-14 2023-05-12 惠州市华达通气体制造股份有限公司 Adsorbent management method based on hydrogen production purification and electronic equipment
CN117205718A (en) * 2023-08-21 2023-12-12 青岛理工大学 Capturing and fixing CO 2 Composite material of (2), preparation method and CO 2 Absorption device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116099326A (en) * 2023-03-14 2023-05-12 惠州市华达通气体制造股份有限公司 Adsorbent management method based on hydrogen production purification and electronic equipment
CN117205718A (en) * 2023-08-21 2023-12-12 青岛理工大学 Capturing and fixing CO 2 Composite material of (2), preparation method and CO 2 Absorption device
CN117205718B (en) * 2023-08-21 2024-05-14 青岛理工大学 Capturing and fixing CO2Composite material of (2), preparation method and CO2Absorption device

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Address after: 310012 Building 5, Hang Seng Science Park, 1218 Wenyi West Road, Yuhang District, Hangzhou City, Zhejiang Province

Patentee after: Hangzhou lanran Technology Co.,Ltd.

Address before: 310012 Building 5, Hang Seng Science Park, 1218 Wenyi West Road, Yuhang District, Hangzhou City, Zhejiang Province

Patentee before: HANGZHOU LANRAN ENVIRONMENTAL TECHNOLOGY Co.,Ltd.