CN211070103U

CN211070103U - Combined stirring reaction container for gluconolactone

Info

Publication number: CN211070103U
Application number: CN201922096241.1U
Authority: CN
Inventors: 李应生
Original assignee: Jiangxi New Huanghai Food Co ltd
Current assignee: Jiangxi New Huanghai Food Co ltd
Priority date: 2019-11-29
Filing date: 2019-11-29
Publication date: 2020-07-24
Anticipated expiration: 2029-11-29

Abstract

The utility model discloses a combination formula stirring reaction vessel is used to gluconolactone, including reation kettle and stirred tank, the welding of reation kettle top middle part has the motor, the welding of motor bottom has the motor shaft, reation kettle and stirred tank are run through in proper order to the motor shaft. The utility model discloses a setting of reation kettle and stirred tank drives single motor shaft through single motor and rotates, runs through reation kettle and stirred tank through the motor shaft, stirs reation kettle and stirred tank, saves the cost, can drive through single motor, saves the cost effectively, and is comparatively practical, is fit for extensively promoting and using.

Description

Combined stirring reaction container for gluconolactone

Technical Field

The utility model relates to a combined stirring technical field for gluconolactone, in particular to a combined stirring reaction container for gluconolactone.

Background

Decomposing calcium gluconate with inorganic acid or decalcifying with ion exchange resin to obtain gluconic acid solution. If 100 parts of concentrated sulfuric acid is added into 500 parts of water, then calcium gluconate is added, and the temperature is kept at 60-85 ℃ for 1.5 h; standing for 12h, filtering, adding oxalic acid into the filtrate, and keeping the temperature at 50 ℃ for 1 h; standing, filtering to obtain glucose acid solution, and post-treating to obtain lactone.

The existing patent (publication number is CN201120485693.X) and a combined stirring reaction container for calcium gluconate, the discharge port of the condensation reaction kettle and the feed inlet of the hydrolysis reaction are connected by a vacuum pump pipeline, so that the operation process is simplified, a large amount of manpower is saved, but the structure is complex, and the vacuum pump leads gluconolactone with poor fluidity from bottom to top, and needs large electric energy.

Therefore, the combined stirring reaction container for the gluconolactone is provided, and drainage is carried out in a direct current mode, so that the flowing distance of the gluconolactone is reduced, and the energy consumption is also reduced.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a gluconolactone is with combination formula stirring reaction vessel has solved the problem that proposes in the background art.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a gluconic acid lactone is with combination formula stirring reaction vessel, includes reation kettle and stirred tank, reation kettle top middle part welding has the motor, the welding of motor bottom has the motor shaft, reation kettle and stirred tank are run through in proper order to the motor shaft.

As the utility model discloses a preferred embodiment, motor shaft top equidistance welding has zigzag's reaction leaf, the reaction leaf is located reation kettle, motor shaft bottom equidistance welding has the stirring leaf of screw thread form, the stirring leaf is located reation kettle.

As an optimal implementation mode of the utility model, there is main material mouth in the welding of reation kettle top left side through the cutting, there is supplementary material mouth in the welding of reation kettle top right side through the cutting.

As the utility model discloses a preferred embodiment, the welding of reation kettle bottom left side has the support column, support column bottom welding stirred tank top left side, reation kettle bottom right side welding intercommunication has the connecting valve, the connecting valve other end intercommunication has stirred tank top right side.

As the utility model discloses a preferred embodiment, stirred tank bottom left side intercommunication bleeder valve, the welding of stirred tank bottom both sides has the supporting legs.

Compared with the prior art, the beneficial effects of the utility model are as follows:

1. the utility model discloses a gluconolactone is with combination formula stirring reaction vessel, through the setting of reation kettle and stirred tank, drive single motor shaft through single motor and rotate, run through reation kettle and stirred tank through the motor shaft, stir reation kettle and stirred tank, save the cost, can drive through single motor, save the cost effectively.

2. The utility model discloses a gluconolactone is with combination formula stirring reaction vessel, through the setting of connecting valve, make after-reaction gluconolactone get into the stirred tank through opening the connecting valve, the mode that adopts the direct current is more quick, and the line square is shorter, and rethread reation kettle and stirred tank carry out simultaneous working for the effect is higher.

Drawings

Other features, objects and advantages of the invention will become more apparent upon reading of the detailed description of non-limiting embodiments with reference to the following drawings:

FIG. 1 is a schematic view of the overall structure of a combined stirred tank reactor for gluconolactone according to the present invention;

fig. 2 is a sectional view of the structure of the combined stirred tank reactor for gluconolactone of the present invention.

In the figure: a support leg 1; a discharge port 2; a stirred tank 3; a support column 4; a reaction kettle 5; reaction leaves 6; a main material port 7; a motor 8; an auxiliary material port 9; a motor shaft 10; a connection valve 11; the stirring blade 12.

Detailed Description

In order to make the technical means, creation features, achievement purposes and functions of the present invention easy to understand, the present invention is further described below with reference to the following embodiments.

In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.

In the description of the present invention, it should be noted that, unless explicitly stated or limited otherwise, the terms "mounted," "connected" and "disposed" are to be interpreted broadly, and may be, for example, fixedly connected, disposed, detachably connected, disposed, or integrally connected and disposed; the utility model discloses in provide only supply the reference with the model of electrical apparatus. For those skilled in the art, different types of electrical appliances with the same function can be replaced according to actual use conditions, and for those skilled in the art, the specific meaning of the above terms in the present invention can be understood in specific situations.

Referring to fig. 1-2, the present invention provides a technical solution: the utility model provides a gluconic acid lactone is with combination formula stirring reaction vessel, includes reation kettle 5 and stirred

tank

3, 5 top middle parts of reation kettle have welded

motor

8, 8 bottom welds of motor have motor shaft 10, motor shaft 10 runs through reation kettle 5 and stirred tank 3 in proper order.

In this embodiment, referring to fig. 1 and fig. 2, the single motor 8 drives the single motor shaft 10 to rotate, the motor shaft 10 penetrates through the reaction kettle 5 and the stirring kettle 3 to stir the reaction kettle 5 and the stirring kettle 3, so as to save cost, and the single motor 8 can drive the reaction kettle and the stirring kettle, so as to effectively save cost.

Wherein, motor shaft 10 top equidistance welding has zigzag shaped reaction leaf 6, reaction leaf 6 is located reation kettle 5, motor shaft 10 bottom equidistance welding has screw thread form stirring leaf 12, stirring leaf 12 is located stirred tank 3.

In the embodiment, referring to fig. 2, the reaction blade 6 is welded on the top of the motor shaft 10, and the stirring blade 12 is welded on the bottom of the motor shaft 10, the motor 8 is started to drive the motor shaft to rotate, and the reaction blade 6 and the stirring blade 12 rotate accordingly.

Wherein, 5 top left sides of reation kettle have main material mouth 7 through cutting and welding, 5 top right sides of reation kettle have supplementary material mouth 9 through cutting and welding.

In this embodiment, referring to fig. 2, the main material is added through the main material port 7, and the auxiliary material is added through the auxiliary material port 9.

The left side of the bottom of the reaction kettle 5 is welded with a support column 4, the left side of the top of the stirring kettle 3 is welded with the bottom of the support column 4, the right side of the bottom of the reaction kettle 5 is welded and communicated with a connecting valve 11, and the other end of the connecting valve 11 is communicated with the right side of the top of the stirring kettle 3.

In this embodiment, please refer to fig. 2, the gluconolactone enters the stirred tank 3 after the reaction by opening the connection valve 11, the direct current is adopted more quickly, the running moment is shorter, and then the reaction tank 5 and the stirred tank 3 work simultaneously, so that the effect is higher.

Wherein, 3 bottom left sides intercommunication bleeder valve 2 of stirred tank, 3 bottom both sides welding of stirred tank have supporting legs 1.

In this embodiment, please refer to fig. 2, the gluconolactone is discharged through the discharging valve 2.

It should be noted that the utility model relates to a combined stirring reaction vessel for gluconolactone, which comprises a support leg 1, a discharge port 2, a stirring kettle 3, a support column 4, a reaction kettle 5, a reaction blade 6, a main material port 7, a motor 8, an auxiliary material port 9, a motor shaft 10, a connecting valve 11 and a stirring blade 12, all of which are universal standard parts or parts known by those skilled in the art, the structure and principle of which are known by technical manuals or conventional experimental methods, during operation, the single motor 8 drives the single motor shaft 10 to rotate, the motor shaft 10 penetrates through the reaction kettle 5 and the stirring kettle 3 to stir the reaction kettle 5 and the stirring kettle 3, the reaction blade 6 is welded on the top of the motor shaft 10, the stirring blade 12 is welded on the bottom of the motor shaft 10, the motor 8 is started to drive the motor shaft to rotate, and the reaction blade 6 and the stirring blade 12 rotate therewith, open connecting valve 11 and make the post-reaction gluconolactone get into stirred tank 3, the mode that adopts the direct current is faster, and the line moment is shorter, and rethread reation kettle 5 and stirred tank 3 carry out simultaneous working, discharge gluconolactone through bleeder valve 2.

The basic principles and the main features of the invention and the advantages of the invention have been shown and described above, it will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, but that the invention may be embodied in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims

1. The utility model provides a gluconolactone is with combination formula stirring reaction vessel, includes reation kettle (5) and stirred tank (3), its characterized in that: the welding of reation kettle (5) top middle part has motor (8), the welding of motor (8) bottom has motor shaft (10), reation kettle (5) and stirred tank (3) are run through in proper order in motor shaft (10).

2. The modular mixing reactor vessel for gluconolactone as claimed in claim 1, wherein: motor shaft (10) top equidistance welding has broken line shape reaction leaf (6), reaction leaf (6) are located reation kettle (5), motor shaft (10) bottom equidistance welding has stirring leaf (12) of screw thread form, stirring leaf (12) are located stirred tank (3).

3. The modular mixing reactor vessel for gluconolactone as claimed in claim 1, wherein: reation kettle (5) top left side has main material mouth (7) through cutting and welding, reation kettle (5) top right side has supplementary material mouth (9) through cutting and welding.

4. The modular mixing reactor vessel for gluconolactone as claimed in claim 1, wherein: the welding of reation kettle (5) bottom left side has support column (4), support column (4) bottom welding stirred tank (3) top left side, reation kettle (5) bottom right side welding intercommunication has connecting valve (11), connecting valve (11) other end intercommunication has stirred tank (3) top right side.

5. The modular mixing reactor vessel for gluconolactone as claimed in claim 1, wherein: stirred tank (3) bottom left side intercommunication bleeder valve (2), stirred tank (3) bottom both sides welding has supporting legs (1).