CN210965071U - Quinocetone reaction mother liquor recovery unit - Google Patents
Quinocetone reaction mother liquor recovery unit Download PDFInfo
- Publication number
- CN210965071U CN210965071U CN201920906296.1U CN201920906296U CN210965071U CN 210965071 U CN210965071 U CN 210965071U CN 201920906296 U CN201920906296 U CN 201920906296U CN 210965071 U CN210965071 U CN 210965071U
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- China
- Prior art keywords
- reaction
- box
- mother liquor
- quinocetone
- cooling
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 75
- 239000012452 mother liquor Substances 0.000 title claims abstract description 38
- IOKWXGMNRWVQHX-VAWYXSNFSA-N (e)-1-(3-methyl-4-oxido-1-oxoquinoxalin-1-ium-2-yl)-3-phenylprop-2-en-1-one Chemical compound O=[N+]1C2=CC=CC=C2N([O-])C(C)=C1C(=O)\C=C\C1=CC=CC=C1 IOKWXGMNRWVQHX-VAWYXSNFSA-N 0.000 title claims abstract description 29
- 238000011084 recovery Methods 0.000 title claims abstract description 8
- 230000005540 biological transmission Effects 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims description 41
- 230000000149 penetrating effect Effects 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000126 substance Substances 0.000 abstract description 10
- 239000013078 crystal Substances 0.000 abstract description 3
- 238000002425 crystallisation Methods 0.000 abstract description 2
- 230000008025 crystallization Effects 0.000 abstract description 2
- 238000009529 body temperature measurement Methods 0.000 abstract 2
- 230000010354 integration Effects 0.000 abstract 1
- 238000001914 filtration Methods 0.000 description 8
- 239000007788 liquid Substances 0.000 description 6
- 238000007599 discharging Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 241000220317 Rosa Species 0.000 description 3
- 230000004927 fusion Effects 0.000 description 3
- 239000011229 interlayer Substances 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000001142 anti-diarrhea Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- 239000000273 veterinary drug Substances 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a quinocetone reaction mother liquor recovery unit relates to quinocetone reaction mother liquor field, including the reaction furnace body, the top of reaction furnace body is fixed with the bell, the top of bell is provided with and runs through to the inside temperature measurement ware of bell, the top of bell is located one side of temperature measurement ware and installs the low-speed motor. The utility model discloses a set up reaction furnace body low-speed motor, transmission shaft and stirring leaf, quinocetone reaction mother liquor makes the reaction solution who fuses through several kinds of chemicals and produce mutually, through will concentrating the chemical and place reaction together, the heating, cool off the crystal that the crystallization and formed, drive the transmission shaft through low-speed motor and rotate, stir several kinds of chemicals through the stirring leaf of fixing in the transmission shaft outside, make the more even of the integration of several kinds of chemicals, make the reaction rate of quinocetone reaction mother liquor accelerate, the work efficiency of device has been improved.
Description
Technical Field
The utility model relates to a quinocetone reaction mother liquor field specifically is quinocetone reaction mother liquor recovery unit.
Background
Quinocetone is a new antibacterial, antidiarrheal and growth-promoting drug for livestock and poultry newly developed by the research institute of animal husbandry and veterinary drug of Lanzhou academy of agricultural sciences, and most of the existing quinocetone synthesis methods are formed by fusion reaction of several chemical solutions.
However, some enterprises can directly discharge the mother liquor after the mother liquor is reacted, and do not recycle the mother liquor, resulting in low utilization rate of the reaction mother liquor, when recycling several kinds of chemical solution fusion mother liquor, because the solution is fused unevenly, the reaction speed is slow, resulting in low working efficiency of the device, when filtering through the filter screen, because the filter screen of some devices is fixed with the device, after using a period of time, the filter effect of the filter screen can be reduced, resulting in poor filter effect of the device.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a: in order to solve the problems of low utilization rate of reaction mother liquor, low working efficiency of the device and poor filtering effect of the device, the quinocetone reaction mother liquor recovery device is provided.
In order to achieve the above object, the utility model provides a following technical scheme: the quinocetone reaction mother liquor recovery device comprises a reaction furnace body, wherein a furnace cover is fixed at the top end of the reaction furnace body, a temperature measurer penetrating into the furnace cover is arranged at the top end of the furnace cover, a low-speed motor is arranged at one side of the temperature measurer at the top end of the furnace cover, a feed inlet penetrating into the furnace cover is arranged at one side of the low-speed motor, the output end of the low-speed motor is connected with a transmission shaft, stirring blades are fixed on the outer side of the transmission shaft, an outer cover is arranged on the outer side of the reaction furnace body, a heating rod is arranged at the bottom end inside the outer cover, an auxiliary discharge port is arranged at the bottom end of the reaction furnace body, the bottom end of the auxiliary discharge port is connected with a cooling outer box, the interior of the cooling outer box is connected with a cooling inner box in a sliding way, one side of the reaction furnace body is provided with a filter box, the inboard of rose box is provided with main spout, the inboard sliding connection of main spout has square filter screen.
Preferably, the low-speed motor is rotatably connected with the transmission shaft through a rotating shaft, and the cooling inner box and the cooling outer box are slidably connected with the auxiliary sliding groove through a sliding block.
Preferably, a box cover is arranged at the top end of the cooling outer box, and a hole penetrating into the cooling outer box is formed in the top end of the box cover.
Preferably, the filter box and the square filter screen are in sliding connection through a main sliding groove, and a pipeline is arranged inside the cooling inner box.
Preferably, one side of the filter box is provided with a main discharge hole, and the filter box and the cooling inner box are connected with a pipeline through a water pump.
Preferably, the number of the heating rods is four, and the four groups of heating rods are uniformly distributed at the bottom end inside the heating rods.
Compared with the prior art, the beneficial effects of the utility model are that: the utility model discloses a set up reaction furnace body low-speed motor, transmission shaft and stirring leaf, quinocetone reaction mother liquor makes the reaction solution that produces through several kinds of chemical substance fuses mutually, through will concentrate chemical substance and place reaction together, the heating, cool the crystal that the crystallization formed, drive the transmission shaft through low-speed motor and rotate, stir several kinds of chemical substance through the stirring leaf of fixing outside the transmission shaft, make the fusion of several kinds of chemical substance more even, make the reaction rate of quinocetone reaction mother liquor accelerate, the work efficiency of device has been improved, retrieve reacted quinocetone reaction mother liquor through the reaction furnace body, and react quinocetone reaction mother liquor once more, refine remaining material in the quinocetone reaction mother liquor once more, improve the utilization ratio of quinocetone reaction mother liquor, through setting up square filter screen and main spout, after quinocetone reaction mother liquor cools off, carry out filtering separation through crystal and reaction mother liquor of square filter screen in to quinocetone reaction mother liquor, make square filter screen slide in the inside of rose box through main spout, after using a period, take out square filter screen through main spout and clear up or change, improve device's filter effect.
Drawings
Fig. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the connection between the outer cooling box and the inner cooling box of the present invention;
fig. 3 is the utility model discloses a schematic diagram is connected with the rose box to square filter screen.
In the figure: 1. a reaction furnace body; 2. a furnace cover; 3. a temperature measurer; 4. a low-speed motor; 5. a feed inlet; 6. a drive shaft; 7. stirring blades; 8. cooling the outer box; 9. an auxiliary discharge port; 10. a heating rod; 11. a filter box; 12. cooling the inner box; 13. a slider; 14. an auxiliary chute; 15. a main chute; 16. a square filter screen; 17. a housing; 18. and a main discharge hole.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The low-speed motors (41K25RGN-CF) mentioned in the utility model can be obtained by market or private ordering.
Referring to fig. 1-3, a quinocetone reaction mother liquor recovery device comprises a reaction furnace body 1, a furnace cover 2 is fixed at the top end of the reaction furnace body 1, a temperature measurer 3 penetrating into the furnace cover 2 is arranged at the top end of the furnace cover 2, a low-speed motor 4 is installed at one side of the temperature measurer 3 at the top end of the furnace cover 2, a feed inlet 5 penetrating into the furnace cover 2 is arranged at one side of the low-speed motor 4, a transmission shaft 6 is connected to the output end of the low-speed motor 4, a stirring blade 7 is fixed at the outer side of the transmission shaft 6, an outer cover 17 is arranged at the outer side of the reaction furnace body 1, a heating rod 10 is arranged at the bottom end of the inner part of the outer cover 17, an auxiliary discharge port 9 is arranged at the bottom end of the reaction furnace body 1, a cooling outer box 8 is connected to the bottom end of the auxiliary discharge port 9, an inner cooling inner, a square filter screen 16 is connected to the inner side of the main chute 15 in a sliding manner.
Please refer to fig. 1 and fig. 2, the low-speed motor 4 is rotatably connected to the transmission shaft 6 through a rotation shaft, so that the low-speed motor 4 can drive the transmission shaft 6 to rotate, and the inner cooling box 12 and the outer cooling box 8 are slidably connected to the auxiliary chute 14 through the sliding block 13, so that the inner cooling box 12 can be taken out from the outer cooling box 8.
Referring to fig. 2 in particular, a cover is disposed on the top of the cooling outer box 8, and a hole is disposed on the top of the cover and penetrates into the cooling outer box 8, so that cool air can be injected into the interlayer between the cooling outer box 8 and the cooling inner box 12 through the hole on the top of the cover.
Please refer to fig. 2 and fig. 3, the filter box 11 is slidably connected to the square filter screen 16 through the main chute 15, so as to facilitate the square filter screen 16 to be taken out from the inside of the filter box 11, and the cooling inner box 12 is provided with a pipeline inside, so as to facilitate the reaction mother liquid inside the cooling inner box 12 to be pumped out through the pipeline.
Please refer to fig. 1 and 3, a main discharging hole 18 is disposed at one side of the filtering box 11 for conveniently discharging the filtered reaction mother liquid through the main discharging hole 18, and the filtering box 11 and the cooling inner box 12 are connected with a pipeline through a water pump for conveniently discharging the reaction mother liquid in the cooling inner box 12 and injecting the reaction mother liquid into the filtering box 11.
Please refer to fig. 1, the number of the heating rods 10 is four, and the four groups of heating rods 10 are uniformly distributed at the bottom end of the interior of the heating rods 10, so as to facilitate the reaction mother liquor inside the reaction furnace body 1 to be heated more uniformly.
The working principle is as follows: firstly, when in use, the reaction furnace body 1 is connected with the furnace cover 2, the cooling inner box 12 is connected with the cooling outer box 8, the filter box 11 is connected with the square filter screen 16, and the filter box 11 is connected with the cooling inner box 12; then, the device is connected with an external power supply, a quinocetone reaction mother liquor is injected into the interior of the reaction furnace body 1 through the feed inlet 5, the transmission shaft 6 is driven to rotate through the low-speed motor 4, the quinocetone reaction mother liquor in the interior of the reaction furnace body 1 is stirred through the stirring blade 7 fixed on the outer side of the transmission shaft 6, a heat conduction liquid is injected through an interlayer between the outer cover 17 and the reaction furnace body 1, the heating rod 10 heats the reaction mother liquor in the interior of the reaction furnace body 1 through the heat conduction liquid, the temperature in the interior of the reaction furnace body 1 is measured through the temperature measurer 3 during heating, the temperature in the interior of the reaction furnace body 1 is controlled, after heating for a period of time, the reaction mother liquor in the interior of the reaction furnace body 1 is injected into the interior of the cooling inner box 12 through the auxiliary discharge outlet 9 for cooling, and after cooling for a period of time, filtering the reaction mother liquor by a square filter screen 16; finally, after filtration, the square screen 16 is taken out from the inside of the filter box 11 through the main chute 15, and the square screen 16 is cleaned or replaced.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (6)
1. Quinocetone reaction mother liquor recovery unit, including reaction furnace body (1), its characterized in that: the reaction furnace is characterized in that a furnace cover (2) is fixed at the top end of the reaction furnace body (1), a temperature measurer (3) penetrating into the furnace cover (2) is arranged at the top end of the furnace cover (2), a low-speed motor (4) is installed at one side, located at the temperature measurer (3), of the top end of the furnace cover (2), one side of the low-speed motor (4) is provided with a feed inlet (5) penetrating into the furnace cover (2), the output end of the low-speed motor (4) is connected with a transmission shaft (6), stirring blades (7) are fixed at the outer side of the transmission shaft (6), an outer cover (17) is arranged at the outer side of the reaction furnace body (1), a heating rod (10) is arranged at the bottom end of the inner part of the outer cover (17), an auxiliary discharge hole (9) is arranged at the bottom end of the reaction furnace body (1), a cooling outer box (8) is connected with a cooling inner box (12, one side of the reaction furnace body (1) is provided with a filter box (11), the inner side of the filter box (11) is provided with a main chute (15), and the inner side of the main chute (15) is connected with a square filter screen (16) in a sliding manner.
2. The apparatus for recovering a mother liquor of quinocetone reaction according to claim 1, characterized in that: the low-speed motor (4) is rotatably connected with the transmission shaft (6) through a rotating shaft, and the cooling inner box (12) and the cooling outer box (8) are slidably connected with the auxiliary sliding groove (14) through a sliding block (13).
3. The apparatus for recovering a mother liquor of quinocetone reaction according to claim 1, characterized in that: the top end of the cooling outer box (8) is provided with a box cover, and the top end of the box cover is provided with a hole penetrating into the cooling outer box (8).
4. The apparatus for recovering a mother liquor of quinocetone reaction according to claim 1, characterized in that: the filter box (11) is in sliding connection with the square filter screen (16) through a main sliding groove (15), and a pipeline is arranged inside the cooling inner box (12).
5. The apparatus for recovering a mother liquor of quinocetone reaction according to claim 1, characterized in that: one side of the filter box (11) is provided with a main discharge hole (18), and the filter box (11) and the cooling inner box (12) are connected with a pipeline through a water pump.
6. The apparatus for recovering a mother liquor of quinocetone reaction according to claim 1, characterized in that: the number of the heating rods (10) is four, and the four groups of heating rods (10) are uniformly distributed at the bottom end inside the heating rods (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920906296.1U CN210965071U (en) | 2019-08-15 | 2019-08-15 | Quinocetone reaction mother liquor recovery unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920906296.1U CN210965071U (en) | 2019-08-15 | 2019-08-15 | Quinocetone reaction mother liquor recovery unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210965071U true CN210965071U (en) | 2020-07-10 |
Family
ID=71412945
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920906296.1U Expired - Fee Related CN210965071U (en) | 2019-08-15 | 2019-08-15 | Quinocetone reaction mother liquor recovery unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210965071U (en) |
-
2019
- 2019-08-15 CN CN201920906296.1U patent/CN210965071U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200710 |