CN210915898U

CN210915898U - Synthesizer of high-purity methyl silicone oil of anti-oxidation

Info

Publication number: CN210915898U
Application number: CN201921936181.3U
Authority: CN
Inventors: 李卓瑾
Original assignee: Zhejiang Rongli High Tech Materials Co ltd
Current assignee: Zhejiang Rongli High Tech Materials Co ltd
Priority date: 2019-11-11
Filing date: 2019-11-11
Publication date: 2020-07-03
Anticipated expiration: 2029-11-11

Abstract

The utility model discloses a synthesizer of high-purity methyl silicon oil of oxytolerant, including base, first pole setting, second pole setting and third pole setting, install reation kettle through branch between second pole setting and the third pole setting, install step motor through the mounting groove between the branch, the rolling disc is installed through the rotary trough to the bottom in the reation kettle, step motor's power take off end connects the rolling disc bottom, the reation kettle upper end is provided with the top cap, the heating pipe is installed through the reservation tank in the top cap bottom, install the feeding hard tube through the mounting hole between the heating pipe, the temperature controller is installed through the screw in top cap one side. The utility model discloses can conveniently carry out the ratio to the raw materials and get the material, can conveniently carry out the even heating to reation kettle's material, can also conveniently rotate the mixing to the material in the reation kettle, be convenient for detect the pH value of the material after the reaction, be fit for being extensively promoted and used.

Description

Synthesizer of high-purity methyl silicone oil of anti-oxidation

Technical Field

The utility model relates to a chemical production technical field, in particular to synthesizer of anti-oxidation high-purity methyl silicone oil.

Background

Methyl silicone oil is a chemical substance, has excellent heat resistance, electrical insulation, weather resistance, hydrophobicity, physiological inertia and smaller surface tension, also has low viscosity-temperature coefficient and higher compression resistance, is widely applied to the industries of surface treatment, cosmetic addition and textile sewing, and is necessary for synthesizing the methyl silicone oil.

Patent No. CN201721532510.9 discloses a production device of methyl silicone oil with different viscosities, which is simple in device, less in investment, wide in viscosity range of producible high-purity methyl silicone oil, can be used for producing dimethyl silicone oil with the viscosity ranging from 30cp to 1000000cs, can meet the national standard requirements in quality, and can realize industrial production.

Although the device can produce methyl silicone oil with different viscosities, the following disadvantages exist: 1. The raw materials cannot be conveniently proportioned and taken; 2. the materials in the reaction kettle cannot be heated uniformly conveniently; 3. materials in the reaction kettle cannot be conveniently rotated and uniformly mixed; 4. the pH value of the reacted material cannot be conveniently detected.

SUMMERY OF THE UTILITY MODEL

The main object of the utility model is to provide a synthesizer of anti-oxidation high-purity methyl silicone oil can effectively solve the problem in the technical background.

In order to achieve the above purpose, the utility model adopts the following technical scheme:

a synthesizer of high-purity methyl silicone oil of anti-oxidation comprises a base, a first vertical rod, a second vertical rod and a third vertical rod, wherein a reaction kettle is installed between the second vertical rod and the third vertical rod through a supporting rod, a stepping motor is installed between the supporting rods through a mounting groove, a rotating disc is installed at the inner bottom end of the reaction kettle through a rotating groove, the power output end of the stepping motor is connected with the bottom of the rotating disc, a top cover is arranged at the upper end of the reaction kettle, a heating pipe is installed at the bottom of the top cover through a reserved groove, a feeding hard pipe is installed between the heating pipes through a mounting hole, a temperature controller is installed on one side of the top cover through screws, a top plate is welded on one side of the top end of the third vertical rod, an electric hydraulic cylinder is installed at the bottom of the top plate through bolts, the output end, the utility model discloses a sampling device, including storage tank, first pole setting top, second pole setting top has a multi-way valve through mounting panel and mounting screw installation, the discharge port of storage tank passes through the feed inlet that the conveying pipeline connects the multi-way valve, the discharge gate of multi-way valve has force pump and pressure pump to send the material end through feeding hose connection feeding hard tube top through the pipe connection, sample jar is installed through the mounting groove to third pole setting one end, sample tank deck portion one end has the pH value tester through the screw installation, the sense terminal of pH value tester is located the interior bottom of sample jar.

Furthermore, the input end of the heating pipe is electrically connected with the output end of the temperature controller through a lead.

Further, the quantity of storage tank specifically sets up to the multiunit, be close to storage tank one end on the conveying pipeline and all be provided with flow control valve.

Furthermore, the number of the heating pipes is specifically set to be multiple groups, and the heating pipes are uniformly distributed on the circumference of the lower end of the top cover.

Furthermore, a stepping motor controller is installed on one side of the stepping motor through a screw, and the input end of the stepping motor is electrically connected with the output end of the stepping motor controller through a wire.

Further, a sampling suction pump is installed at one end of the top of the sampling tank through a screw, the feeding end of the suction pump is connected with the discharge port of the reaction kettle through a suction pipe, and the discharge end of the suction pump is connected with the inner side of the sampling tank through a pipeline.

Compared with the prior art, the utility model discloses following beneficial effect has:

1. through setting up the multiunit storage tank, conveniently load the raw materials of multiple difference, the rethread sets up flow control valve, utilizes flow control valve convenience to adjust the flow size via the conveying pipeline to make things convenient for personnel to carry out the ratio to the raw materials and get the material.

2. Through setting up heating pipe and temperature controller, the personnel are with heating pipe and external power source switch-on, and the raw materials of heating pipe during operation convenience in to reation kettle heats, utilizes the convenient heating temperature who controls the heating pipe of temperature controller, prevents that the heating pipe from rising temperature too high, utilizes multiunit heating pipe to be circumference evenly distributed at the top cap lower extreme, conveniently promotes the homogeneity of heating pipe to raw materials heating in the reation kettle.

3. Through setting up step motor and step motor controller, open step motor, the during operation power take off end conveniently drives the rolling disc and rotates, and personnel adjust step motor controller's setting value, conveniently adjust step motor's slew velocity as required to adjust the slew velocity of rolling disc, and then be convenient for drive the interior raw materials mixing of reation kettle.

4. Through setting up sample suction pump and pH value tester, after the reaction was accomplished, personnel opened the sample suction pump, and the during operation is convenient inhales the material in reation kettle via inhaling the material pipe, via the pipe-line transportation to the sample jar in, utilizes the detection end that the pH tester is located the sample jar bottom, conveniently detects the pH value of the material of reaction completion, and the personnel of being convenient for know.

Drawings

FIG. 1 is a schematic diagram of the overall structure of an oxidation-resistant high-purity methyl silicone oil synthesizer according to the present invention.

FIG. 2 is a schematic top view of the top cover of the apparatus for synthesizing oxidation-resistant high-purity methyl silicone oil according to the present invention.

FIG. 3 is a schematic diagram of the electrical connection of an electrical appliance of the oxidation-resistant high-purity methyl silicone oil synthesizer of the present invention.

In the figure: 1. a base; 2. a first upright rod; 3. a fixing plate; 4. a material storage tank; 5. a delivery pipe; 6. a flow regulating valve; 7. a multi-way valve; 8. a second upright stanchion; 9. a pressure pump; 10. A feed hose; 11. a top cover; 12. heating a tube; 13. feeding a hard pipe; 14. a reaction kettle; 15. rotating the disc; 16. a strut; 17. a stepping motor; 18. a third upright stanchion; 19. an electric hydraulic cylinder; 20. a sampling suction pump; 21. a material suction pipe; 22. a sampling tank; 23. a pH value tester; 24. a temperature controller; 25. a stepper motor controller.

Detailed Description

In order to make the technical means, creation features, achievement purposes and functions of the present invention easy to understand, the present invention is further described below with reference to the following embodiments.

As shown in fig. 1-3, a synthesizer of oxidation-resistant high-purity methyl silicone oil comprises a base 1, a first vertical rod 2, a second vertical rod 8 and a third vertical rod 18, a reaction kettle 14 is installed between the second vertical rod 8 and the third vertical rod 18 through a supporting rod 16, a stepping motor 17 is installed between the supporting rods 16 through a mounting groove, a rotating disc 15 is installed at the inner bottom end of the reaction kettle 14 through a rotating groove, the power output end of the stepping motor 17 is connected with the bottom of the rotating disc 15, a top cover 11 is arranged at the upper end of the reaction kettle 14, a heating pipe 12 is installed at the bottom of the top cover 11 through a reserved groove, a feeding hard pipe 13 is installed between the heating pipes 12 through a mounting hole, a temperature controller 24 is installed on one side of the top cover 11 through screws, a top plate is welded on one side of the top end of the third vertical rod 18, an electric

hydraulic cylinder

19 and, 2 one end welding of first pole setting has fixed plate and fixed plate top to install storage tank 4 through the fixed lantern ring, there is multi-way valve 7 at 8 tops of second pole setting through mounting panel and screw mounting, the discharge port of storage tank 4 passes through conveying pipeline 5 and connects the feed inlet of multi-way valve 7, there is force pump 9 and force pump 9 discharge end to connect feeding hard tube 13 top through feeding hose 10 through the pipe connection of multi-way valve 7, sample jar 22 is installed through the mounting groove to 18 one ends of third pole setting, pH value tester 23 is installed through the screw in sample jar 22 top one end, the sense terminal of pH value tester 23 is located the interior bottom of sample jar 22.

Wherein, the input end of the heating pipe 12 is electrically connected with the output end of the temperature controller 24 through a conducting wire.

In this embodiment, as shown in fig. 1 and 3, the temperature controller 24 is used to conveniently control the heating temperature of the heating pipe 12, so as to prevent the heating pipe 12 from being heated too high.

Wherein, the quantity of storage tank 4 specifically sets up to the multiunit, be close to storage tank 4 one end on the conveying pipeline 5 and all be provided with flow control valve 6.

In this embodiment, as shown in fig. 1, a plurality of groups of material storage tanks 4 are used to conveniently fill a plurality of different raw materials, and a flow control valve 6 is used to conveniently adjust the flow through a material conveying pipe 5, so that the personnel can conveniently mix the raw materials to obtain the materials.

The number of the heating pipes 12 is specifically set to be multiple groups, and the heating pipes 12 are circumferentially and uniformly distributed at the lower end of the top cover 11.

In this embodiment, as shown in fig. 1 and 2, a plurality of groups of heating pipes 12 are uniformly distributed on the lower end of the top cover 11 in a circumferential manner, so as to facilitate the uniformity of heating the raw materials in the reaction kettle 14 by the heating pipes 12.

Wherein, step motor controller 25 is installed through the screw in step motor 17 one side, step motor 17's input constitutes the electricity with step motor controller 25's output through the wire and is connected.

In this embodiment, as shown in fig. 1 and 3, a person adjusts the setting value of the stepping motor controller 25, which facilitates the adjustment of the rotation speed of the stepping motor 17 as needed, thereby adjusting the rotation speed of the rotary disk 15.

Wherein, a sampling suction pump 20 is installed at one end of the top of the sampling tank 22 through a screw, the feed end of the suction pump 20 is connected with the discharge port of the reaction kettle 14 through a suction pipe 21, and the discharge end of the suction pump 20 is connected with the inner side of the sampling tank 22 through a pipeline.

In this embodiment, as shown in fig. 1, after the reaction is completed, a person opens the sampling suction pump 20, so that the material in the reaction kettle 14 is conveniently sucked through the suction pipe 21 and conveyed to the sampling tank 22 through a pipeline during operation.

It should be noted that the utility model relates to a synthesizer of high-purity methyl silicone oil of anti-oxidation, during operation, personnel open force pump 9, during operation conveniently convey the raw materials to feeding hose 10 via conveying pipeline 5 and multi-way valve 7, and then convey to reation kettle 14 via feeding hard tube 13 and react, utilize multiunit storage tank 4 to conveniently load multiple different raw materials, reuse flow control valve 6 to conveniently adjust the flow size via conveying pipeline 5, thereby make things convenient for personnel to match the raw materials and get the material, personnel open electric hydraulic cylinder 19, during operation conveniently drive top cap 11 and reciprocate, personnel switch on heating pipe 12 with external power supply, heating pipe 12 conveniently heats the raw materials in reation kettle 14 during operation, utilize temperature controller 24 (produced by xu zhou ruide electrical apparatus limited, model AC-112) to conveniently control the heating temperature of heating pipe 12, the heating pipes 12 are prevented from being heated too high, a plurality of groups of heating pipes 12 are uniformly distributed at the lower end of the top cover 11 in a circumferential manner, so that the uniformity of heating the raw materials in the reaction kettle 14 by the heating pipes 12 is conveniently improved, the stepping motor 17 is started, the power output end conveniently drives the rotating disc 15 to rotate during working, a worker adjusts the set value of a stepping motor controller 25 (model ZBLD. C20-400 LR) and conveniently adjusts the rotating speed of the stepping motor 17 according to needs, so as to adjust the rotating speed of the rotating disc 15 and further conveniently drive the raw materials in the reaction kettle 14 to be uniformly mixed, after the reaction is finished, the worker starts the sampling suction pump 20, conveniently sucks the materials in the reaction kettle 14 through the suction pipe 21 and conveys the materials into the sampling tank 22 through a pipeline, and utilizes a pH tester 23 (produced by Guangzhou Jia instrument precision instruments, JY model-P H160) to be positioned at the detection end of the inner bottom end of the sampling tank 22, the p h value of the material after the reaction is finished is conveniently detected, and the personnel can conveniently know the value.

The basic principles and the main features of the invention and the advantages of the invention have been shown and described above. It will be understood by those skilled in the art that the present invention is not limited to the above embodiments, and that the foregoing embodiments and descriptions are provided only to illustrate the principles of the present invention without departing from the spirit and scope of the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims

1. The utility model provides a synthesizer of high-purity methyl silicone oil of anti-oxidation, includes base (1), first pole setting (2), second pole setting (8) and third pole setting (18), its characterized in that: install reation kettle (14) through branch (16) between second pole setting (8) and third pole setting (18), install step motor (17) through the mounting groove between branch (16), rolling disc (15) are installed through the turn trough in reation kettle (14) bottom, step motor's (17) power take off end connects rolling disc (15) bottom, reation kettle (14) upper end is provided with top cap (11), heating pipe (12) are installed through the reserve tank in top cap (11) bottom, install feeding hard tube (13) through the mounting hole between heating pipe (12), top cap (11) one side is installed temperature controller (24) through the screw, the welding of third pole setting (18) top one side has the roof, the output that installs electric hydraulic cylinder (19) and electric hydraulic cylinder (19) through the bolt bottom the roof connects top cap (11) top, first pole setting (2) one end welding has fixed plate and fixed plate top to install storage tank (4) through the fixed lantern ring, there are multi-ported valve (7) at second pole setting (8) top through mounting panel and screw mounting, the discharge port of storage tank (4) passes through conveying pipeline (5) and connects the feed inlet of multi-ported valve (7), the discharge gate of multi-ported valve (7) has force pump (9) and force pump (9) discharge end to pass through feeding hose (10) and connects feeding hard tube (13) top, sample jar (22) is installed through the mounting groove to third pole setting (18) one end, pH value tester (23) are installed through the screw to sample jar (22) top one end, the sense terminal of pH value tester (23) is located sample jar (22) bottom in.

2. The synthesis device of oxidation-resistant high-purity methyl silicone oil according to claim 1, characterized in that: the input end of the heating pipe (12) is electrically connected with the output end of the temperature controller (24) through a lead.

3. The synthesis device of oxidation-resistant high-purity methyl silicone oil according to claim 1, characterized in that: the quantity of storage tank (4) specifically sets up to the multiunit, be close to storage tank (4) one end on conveying pipeline (5) and all be provided with flow control valve (6).

4. The synthesis device of oxidation-resistant high-purity methyl silicone oil according to claim 1, characterized in that: the number of the heating pipes (12) is specifically set to be multiple groups, and the heating pipes (12) are uniformly distributed on the circumference of the lower end of the top cover (11).

5. The synthesis device of oxidation-resistant high-purity methyl silicone oil according to claim 1, characterized in that: step motor controller (25) is installed through the screw in step motor (17) one side, the input of step motor (17) and the output of step motor controller (25) constitute the electricity through the wire and are connected.

6. The synthesis device of oxidation-resistant high-purity methyl silicone oil according to claim 1, characterized in that: sampling suction pump (20) is installed through the screw in sampling jar (22) top one end, suction pump's (20) feed end is through inhaling the discharge gate of material pipe (21) connection reation kettle (14), suction pump's (20) discharge end is inboard through pipe connection sampling jar (22).