CN210875275U - Jacketed reaction kettle - Google Patents

Jacketed reaction kettle Download PDF

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Publication number
CN210875275U
CN210875275U CN201921058361.6U CN201921058361U CN210875275U CN 210875275 U CN210875275 U CN 210875275U CN 201921058361 U CN201921058361 U CN 201921058361U CN 210875275 U CN210875275 U CN 210875275U
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CN
China
Prior art keywords
jacket
kettle
reaction kettle
heater
heat exchange
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Withdrawn - After Issue
Application number
CN201921058361.6U
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Chinese (zh)
Inventor
姚婉平
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Shanghai Pu Jie Fragrance Co ltd
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Shanghai Pu Jie Fragrance Co ltd
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Priority to CN201921058361.6U priority Critical patent/CN210875275U/en
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Abstract

The utility model discloses a jacketed reaction kettle, which comprises a kettle body and a jacket, wherein the jacket is arranged at the outer side of the kettle body, and an accommodating space is formed between the jacket and the kettle body; the jacket is provided with an outlet and an inlet, the jacket type reaction kettle further comprises a pipeline heater, the pipeline heater is arranged outside the jacket and is connected with the outlet and the inlet through a pipeline, so that the accommodating space, the outlet, the pipeline heater and the inlet form a heat exchange loop, and the heat exchange loop is used for circulating flow of heat exchange fluid, so that heat of the pipeline heater is transferred to the kettle body. The utility model discloses a be connected pipe heater and the export and the entry that press from both sides the cover, shortened pipe heater and jacket formula reation kettle's distance, avoided heat transfer circuit's heat to run off, also avoided jacket formula reation kettle's body high temperature, avoided the internal enamel layer of cauldron to be destroyed, improved heat exchange efficiency, reduced jacket formula reation kettle's use cost.

Description

Jacketed reaction kettle
Technical Field
The utility model relates to a chemical industry field, in particular to double-layered shell type reation kettle.
Background
The broad understanding of the reaction kettle is that the reaction kettle is a container for physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container.
The jacketed reaction kettle generally comprises a kettle body, a kettle cover, a jacket, a stirrer, a transmission device, a shaft seal device, a support and the like. The jacket is arranged outside the auxiliary kettle body. Typically, a heating liquid is provided within the jacket, which receives external heat and transfers the heat to the reactants within the kettle body.
The current oil bath heating type jacketed reaction kettle generally has two forms.
One is to set up a dedicated oil heating boiler at a place remote from the production plant. The biggest disadvantage of this form is that the heated oil must be at a high temperature at the boiler, because of heat losses during transport and high production costs.
The other is to arrange a heating resistor in the jacket of the sleeve type reaction kettle, and the most advantage of the form is to solve the above disadvantages. Then, in actual production, because the heating resistor is too close to the inner layer of the sleeve-type reaction kettle and is influenced by the high temperature of the heating resistor, the enamel layer on the inner surface of the sleeve-type reaction kettle is particularly easy to be damaged, and the sleeve-type reaction kettle is subjected to enamel surface treatment again, as well as the pipeline is time-consuming, labor-consuming and expensive, so that the production cost is greatly increased.
In summary, the heating oil of the jacketed reaction kettle has the following disadvantages during heating: the heating boiler is too far away from the sleeve type reaction kettle, and the heat loss of the heating oil in the transmission process is too large; or the heating resistor arranged in the jacket layer is too close to the enamel layer of the jacket type reaction kettle, so that the enamel layer is easily damaged.
SUMMERY OF THE UTILITY MODEL
The to-be-solved technical problem of the utility model is to overcome the above-mentioned defect among the prior art, provide a jacketed reation kettle.
The utility model discloses an above-mentioned technical problem is solved through following technical scheme:
a jacketed reaction kettle comprises a kettle body and a jacket, wherein the jacket is arranged on the outer side of the kettle body, and an accommodating space is formed between the jacket and the kettle body; the jacketed reaction kettle is characterized in that the jacketed reaction kettle further comprises a pipeline heater, the pipeline heater is arranged outside the jacket and connected with the outlet and the inlet through pipelines, so that the accommodating space, the outlet, the pipeline heater and the inlet form a heat exchange loop, and the heat exchange loop is used for circulating flow of heat exchange fluid, so that heat of the pipeline heater is transferred to the kettle body.
In this scheme, through adopting above structure, be connected through the export and the entry with pipe heater and clamp cover, shortened pipe heater and clamp cover formula reation kettle's distance, avoided heat transfer loop's heat to run off, also avoided clamp cover formula reation kettle's body high temperature, avoided the internal enamel layer of cauldron to be destroyed, improved heat exchange efficiency, reduced clamp cover formula reation kettle's use cost.
Preferably, the jacketed reaction kettle further comprises a first heat-insulating layer and a second heat-insulating layer, the first heat-insulating layer is arranged on the outer side of the jacket, and the second heat-insulating layer is arranged on the outer side of the pipe heater.
In this scheme, through adopting above structure, utilize first heat preservation and second heat preservation, avoided jacketed reation kettle's heat to run off, reduced jacketed reation kettle's use cost.
Preferably, the first heat-insulating layer and the second heat-insulating layer are made of one of glass wool, mineral wool and composite silicate.
Preferably, the jacketed reaction kettle further comprises a circulating pump, and the circulating pump is arranged in the heat exchange loop.
In this scheme, through adopting above structure, utilize the circulating pump to improve the interior heat transfer fluid's of jacketed reation kettle velocity of flow, and then improved heat transfer fluid's heat exchange efficiency.
Preferably, the circulation pump is disposed between the outlet and the pipe heater.
Preferably, the distance between the outer wall of the pipe heater and the outer wall of the jacket is not more than 0.5 m.
In this scheme, through adopting above structure, through setting up pipe heater at the 0.5m within range that presss from both sides the cover, further shortened heat transfer pipeline's length, avoided the heat to run off, improved heat exchange efficiency.
Preferably, the outlet is provided at a lower portion of the jacket, and the inlet is provided at an upper portion of the jacket.
Preferably, the jacketed reaction kettle further comprises a control device and a measuring device; the measuring device is arranged in the jacket and is used for measuring the temperature of the accommodating space; the control device is used for controlling the power and the heating time of the pipeline heater; one end of the control device is in communication connection with the measuring device, and the other end of the control device is in communication connection with the pipeline heater.
In this scheme, through adopting above structure, utilize measuring device to realize the implementation of the interior temperature of double-layered cover formula reation kettle and detect, utilize controlling means to realize the timely accurate adjustment of the interior temperature of double-layered cover formula reation kettle. The temperature stability in the jacketed reaction kettle is improved, the overhigh or overlow temperature in the jacketed reaction kettle is avoided, and the reaction environment in the jacketed reaction kettle is improved.
On the basis of the common knowledge in the field, the above preferred conditions can be combined at will to obtain the preferred embodiments of the present invention.
The utility model discloses an actively advance the effect and lie in:
the utility model discloses a be connected pipe heater and the export and the entry that press from both sides the cover, shortened pipe heater and jacket formula reation kettle's distance, avoided heat transfer circuit's heat to run off, also avoided jacket formula reation kettle's body high temperature, avoided the internal enamel layer of cauldron to be destroyed, improved heat exchange efficiency, reduced jacket formula reation kettle's use cost.
Drawings
Fig. 1 is a schematic structural diagram of a jacketed reaction kettle according to embodiment 1 of the present invention.
Fig. 2 is a schematic structural view of a jacketed reaction kettle according to embodiment 2 of the present invention.
Fig. 3 is a schematic structural view of a jacketed reaction kettle according to embodiment 3 of the present invention.
Description of reference numerals:
jacketed reaction kettle 100
Kettle body 11
Jacket 12
An outlet 13
Inlet 14
Pipe heater 20
Circulating pump 30
Control device 40
Measuring device 50
Detailed Description
The present invention will be more clearly and completely described below by way of examples and with reference to the accompanying drawings, but the present invention is not limited thereto.
Example 1
As shown in fig. 1, the present embodiment is a jacketed reaction kettle 100, the jacketed reaction kettle 100 includes a kettle body 11 and a jacket 12, the jacket 12 is disposed outside the kettle body 11, and an accommodating space is formed between the jacket 12 and the kettle body 11; the jacket 12 is provided with an outlet 13 and an inlet 14, the jacketed reaction kettle 100 further comprises a pipe heater 20, the pipe heater 20 is arranged outside the jacket 12, the pipe heater 20 is connected with the outlet 13 and the inlet 14 through a pipe, so that the accommodating space, the outlet 13, the pipe heater 20 and the inlet 14 form a heat exchange loop, and the heat exchange loop is used for circulating a heat exchange fluid, so that the heat of the pipe heater 20 is transferred to the kettle body 11. This embodiment is connected through export 13 and the entry 14 with pipe heater 20 and clamp cover 12, has shortened pipe heater 20 and the distance of clamp cover formula reation kettle 100, has avoided heat transfer loop's heat to run off, has also avoided clamp cover formula reation kettle 100's body high temperature, has avoided the enamel layer in the cauldron body 11 to be destroyed, has improved heat exchange efficiency, has reduced clamp cover formula reation kettle 100's use cost.
As an embodiment, the jacketed reaction kettle 100 may further include a first heat-insulating layer disposed outside the jacket 12 and a second heat-insulating layer disposed outside the pipe heater 20. In this embodiment, the first heat insulating layer and the second heat insulating layer are utilized, so that heat loss of the jacketed reaction kettle 100 is avoided, and the use cost of the jacketed reaction kettle 100 is reduced. Preferably, the first heat-insulating layer and the second heat-insulating layer are made of one of glass wool, mineral wool and composite silicate. Generally, the first insulating layer and the second insulating layer are laid after the jacketed reaction kettle 100 is installed in place. The periphery of the related pipeline is also paved with an insulating layer.
As an embodiment, the distance between the outer wall of the pipe heater 20 and the outer wall of the jacket 12 may be designed to be not more than 0.5 m. This embodiment further shortens the length of heat transfer pipeline through setting up pipe heater 20 in the 0.5m within range of pressing from both sides cover 12, has avoided the heat loss, has improved heat exchange efficiency. In the present embodiment, the distance is designed to be 0.3 m.
As a preferred embodiment, the outlet 13 is provided at a lower portion of the jacket 12, and the inlet 14 is provided at an upper portion of the jacket 12. In other embodiments, the positions of the outlet 13 and the inlet 14 may be different from those of the present embodiment.
Example 2
As shown in fig. 2, this embodiment is a jacketed reaction kettle 100, and is substantially the same as embodiment 1 except that:
jacketed kettle 100 further comprises a circulation pump 30, and circulation pump 30 is disposed in the heat exchange loop. In this embodiment, the circulating pump 30 is used to increase the flowing speed of the heat exchange fluid in the jacketed reaction kettle 100, so as to increase the heat exchange efficiency of the heat exchange fluid. In the present embodiment, the circulation pump 30 is disposed between the outlet 13 and the duct heater 20. In other embodiments, the circulation pump 30 may be disposed at other locations in the heat exchange loop.
Example 3
As shown in fig. 3, this embodiment is a jacketed reaction kettle 100, and is substantially the same as embodiment 2 except that:
the jacketed reaction kettle 100 of the present embodiment further includes a control device 40 and a measuring device 50; a measuring device 50 is provided in the jacket 12, the measuring device 50 being for measuring the temperature of the accommodating space; the control device 40 is used for controlling the power and the heating time of the pipeline heater 20; one end of the control device 40 is communicatively connected to the measuring device 50, and the other end of the control device 40 is communicatively connected to the duct heater 20.
Specifically, the measuring device 50 is configured to measure the temperature of the heat exchange fluid within a preset time, and send a temperature signal to the control device 40;
the control device 40 receives the temperature signal and compares the temperature signal with a preset value;
when the temperature signal is greater than the preset value, the control device 40 sends a heating stop signal to the pipe heater 20, and the pipe heater 20 stops heating after receiving the heating stop signal;
when the temperature signal is smaller than the preset value, the control device 40 sends a heating power increasing signal to the pipe heater 20, and the pipe heater 20 increases the heating power after receiving the heating power increasing signal;
when the temperature signal is equal to the preset value, the control device 40 sends a heating power invariable signal to the pipe heater 20, and the pipe heater 20 continues to heat according to the original heating power after receiving the heating power invariable signal.
The predetermined time ranges from 2 minutes to 24 hours. The predetermined time is selected to be 0.5 hour in this embodiment. In this embodiment, the measurement device 50 is used to implement and detect the temperature in the jacketed reaction kettle 100, and the control device 40 is used to implement the timely and accurate adjustment of the temperature in the jacketed reaction kettle 100. The temperature stability in the jacketed reaction kettle 100 can be improved, the phenomenon that the temperature in the jacketed reaction kettle 100 is too high or too low can be avoided, and the improvement of the reaction environment in the jacketed reaction kettle 100 can be facilitated.
In addition, according to the relevant test data, compared with the jacket type reaction kettle with the built-in heating resistor in the jacket, the heating power of the pipe heater 20 of the jacket type reaction kettle 100 of the embodiment only needs to adopt one fourth of the heating power of the jacket type reaction kettle, and the heating effect similar to the jacket type reaction kettle can be achieved, and the jacket type reaction kettle 100 of the embodiment reduces the load of electricity utilization and improves the heat exchange efficiency.
Although specific embodiments of the present invention have been described above, it will be understood by those skilled in the art that this is by way of example only and that the scope of the invention is defined by the appended claims. Various changes and modifications to these embodiments may be made by those skilled in the art without departing from the spirit and the principles of the present invention, and these changes and modifications are all within the scope of the present invention.

Claims (7)

1. A jacketed reaction kettle comprises a kettle body and a jacket, wherein the jacket is arranged on the outer side of the kettle body, and an accommodating space is formed between the jacket and the kettle body; the jacketed reaction kettle is characterized by further comprising a pipeline heater, wherein the pipeline heater is arranged outside the jacket and is connected with the outlet and the inlet through a pipeline, so that the accommodating space, the outlet, the pipeline heater and the inlet form a heat exchange loop, and the heat exchange loop is used for circulating flow of heat exchange fluid, so that heat of the pipeline heater is transferred to the kettle body;
the jacketed reaction kettle further comprises a control device and a measuring device; the measuring device is arranged in the jacket and is used for measuring the temperature of the accommodating space; the control device is used for controlling the power and the heating time of the pipeline heater; one end of the control device is in communication connection with the measuring device, and the other end of the control device is in communication connection with the pipeline heater.
2. The jacketed reaction kettle of claim 1, further comprising a first insulation layer disposed on the outside of the jacket and a second insulation layer disposed on the outside of the pipe heater.
3. The jacketed reaction kettle according to claim 2, wherein the first and second insulation layers are made of one of glass wool, mineral wool and composite silicate.
4. The jacketed kettle of claim 1, further comprising a circulation pump disposed in the heat exchange loop.
5. The jacketed kettle of claim 4, wherein the circulation pump is disposed between the outlet and the pipe heater.
6. The jacketed reactor of claim 1 wherein the outer wall of the pipe heater is spaced from the outer wall of the jacket by a distance of no more than 0.5 m.
7. The jacketed reactor according to claim 1 wherein the outlet is located at the lower portion of the jacket and the inlet is located at the upper portion of the jacket.
CN201921058361.6U 2019-07-05 2019-07-05 Jacketed reaction kettle Withdrawn - After Issue CN210875275U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201921058361.6U CN210875275U (en) 2019-07-05 2019-07-05 Jacketed reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921058361.6U CN210875275U (en) 2019-07-05 2019-07-05 Jacketed reaction kettle

Publications (1)

Publication Number Publication Date
CN210875275U true CN210875275U (en) 2020-06-30

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201921058361.6U Withdrawn - After Issue CN210875275U (en) 2019-07-05 2019-07-05 Jacketed reaction kettle

Country Status (1)

Country Link
CN (1) CN210875275U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115569627A (en) * 2022-11-21 2023-01-06 烟台福川化工有限公司 Salifying reaction kettle for trimethyl orthoacetate

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115569627A (en) * 2022-11-21 2023-01-06 烟台福川化工有限公司 Salifying reaction kettle for trimethyl orthoacetate
CN115569627B (en) * 2022-11-21 2023-02-07 烟台福川化工有限公司 Salifying reaction kettle for trimethyl orthoacetate

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Granted publication date: 20200630

Effective date of abandoning: 20210615

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Effective date of abandoning: 20210615