CN210856357U - Electrochemical synthesis equipment for metal organic framework material - Google Patents

Electrochemical synthesis equipment for metal organic framework material Download PDF

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Publication number
CN210856357U
CN210856357U CN201921669361.XU CN201921669361U CN210856357U CN 210856357 U CN210856357 U CN 210856357U CN 201921669361 U CN201921669361 U CN 201921669361U CN 210856357 U CN210856357 U CN 210856357U
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CN
China
Prior art keywords
cooling device
reaction chamber
organic framework
framework material
electrochemical synthesis
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Expired - Fee Related
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CN201921669361.XU
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Chinese (zh)
Inventor
陈勇强
田源
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Jinzhong University
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Jinzhong University
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Priority to CN201921669361.XU priority Critical patent/CN210856357U/en
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Publication of CN210856357U publication Critical patent/CN210856357U/en
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Abstract

The utility model discloses a metal organic framework material electrochemical synthesis equipment, comprising a main body, the lower extreme surface of main part is provided with the bracing piece, the upper end surface of bracing piece is provided with the base, the front end surface of base is provided with the switch, the upper end surface of base is provided with the reaction chamber stove, the front end surface of reaction chamber stove is provided with visual panel, one side of visual panel is provided with the moisture removal device, the lower extreme that removes the moisture device is provided with the chamber door switch, one side surface that removes the moisture device is provided with cooling device. A metal organic framework material electrochemical synthesis equipment, be equipped with cooling device and remove damp device, can finish the back in equipment synthesis, reduce the inside temperature of reaction chamber stove fast, the person of facilitating the use takes out the material after will synthesizing, can also reduce the inside comdenstion water of reaction chamber stove, bring better use prospect.

Description

Electrochemical synthesis equipment for metal organic framework material
Technical Field
The utility model relates to an electrochemical synthesis equipment field, in particular to metal organic framework material electrochemical synthesis equipment.
Background
The electrochemical synthesis equipment for the metal organic framework material is equipment for electrochemically synthesizing the metal organic framework material, can be used by people conveniently, and is simple in structure and convenient to operate.
The existing metal organic framework material electrochemical synthesis equipment has certain disadvantages in use, firstly, in the use process, the inside of a reaction furnace chamber is cooled slowly, the use of a user is influenced, and certain inconvenience is caused.
SUMMERY OF THE UTILITY MODEL
The main object of the utility model is to provide a metal organic framework material electrochemical synthesis equipment can effectively solve the problem in the background art.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
an electrochemical synthesis device of metal organic framework material comprises a main body, wherein a support rod is arranged on the outer surface of the lower end of the main body, the outer surface of the upper end of the supporting rod is provided with a base, the outer surface of the front end of the base is provided with a switch, the outer surface of the upper end of the base is provided with a reaction cavity furnace, the outer surface of the front end of the reaction cavity furnace is provided with a visual panel, a moisture removal device is arranged on one side of the visual panel, a cavity door switch is arranged at the lower end of the moisture removal device, the outer surface of one side of the dehumidifying device is provided with a cooling device, the outer surface of the upper end of the reaction cavity furnace is provided with a control panel, a display screen is arranged at one end of the control panel, a bracket is arranged in the reaction cavity furnace, parallel reaction kettles are arranged outside the support, fixing holes are formed in the middle of the support, and mounting holes are formed between the fixing holes and the parallel reaction kettles.
The cooling device is mainly beneficial to quickly cooling the inside of the reaction furnace chamber.
The dehumidifying device mainly reduces the condensed water after the synthesis reaction in the reaction furnace chamber.
Preferably, cooling device includes semiconductor refrigeration piece, radiating groove, cooling fan, power cord and heat dissipation fan, cooling device's upper end surface is provided with the power cord, the lower extreme surface of power cord is provided with the cooling fan, one side surface of cooling fan is provided with the semiconductor refrigeration piece, one side surface of semiconductor refrigeration piece is provided with the heat dissipation fan, one side surface of heat dissipation fan is provided with the radiating groove.
Preferably, the dehumidifying device comprises a ventilating groove, a dry silica gel storage bin, a threaded connecting piece, a replacement cover and an upper cover, the ventilating groove is formed in the outer surface of the lower end of the dehumidifying device, the dry silica gel storage bin is arranged on the outer surface of the upper end of the ventilating groove, the threaded connecting piece is arranged on the outer surface of the upper end of the dry silica gel storage bin, the upper cover is arranged on the outer surface of the upper end of the threaded connecting piece, and the replacement cover is arranged on the outer surface of the upper end of the upper cover.
Preferably, be provided with the cross screw between radiating groove and the cooling device, one side surface of radiating groove passes through the cross screw and is connected with one side surface fixed connection of cooling device, be provided with the mounting bracket No. one between heat dissipation fan and the cooling device, the lower extreme surface of heat dissipation fan is through the inside fixed connection of a mounting bracket and cooling device, be provided with the mounting bracket No. two between cooling fan and the cooling device, the lower extreme surface of cooling fan is through the inside fixed connection of mounting bracket No. two and cooling device.
Preferably, a hinge is arranged between the replacing cover and the upper cover, the outer surface of one side of the replacing cover is movably connected with the outer surface of the upper end of the upper cover through the hinge, and the outer surface of the lower end of the upper cover is fixedly connected with the outer surface of the upper end of the threaded connecting piece.
Preferably, be provided with the set screw between cooling device and the reaction chamber stove, one side surface of cooling device passes through the set screw and is connected with one side surface fixed connection of reaction chamber stove, the outer wall of dehumidification device passes through threaded connection spare and can dismantle with the front end surface of reaction chamber stove and be connected.
Compared with the prior art, the utility model discloses following beneficial effect has: this a metal organic framework material electrochemical synthesis equipment, cooling device through setting up, after equipment synthesis reaction, the semiconductor refrigeration piece that the accessible set up reduces reaction chamber stove inside temperature fast, the cooling fan can improve the convection current of cold air, the heat dissipation fan can reduce the heat that the semiconductor refrigeration piece produced, prevent that reaction chamber stove inside high temperature from influencing people and taking out, be favorable to people's use, remove damp device through setting up, can be after equipment synthesis reaction, through the inside dry silica gel of dry silica gel storage bin, absorb the water gas, prevent that the comdenstion water from polluting inside the reaction chamber stove, be favorable to the maintenance of equipment, whole metal organic framework material electrochemical synthesis equipment simple structure, high durability and convenient operation, the effect of use is better for traditional mode.
Drawings
Fig. 1 is a schematic diagram of the overall structure of the electrochemical synthesis equipment for metal organic framework materials of the present invention.
FIG. 2 is an enlarged view of the parallel reaction vessel 13 inside the reaction chamber furnace 6 of the metal organic framework material electrochemical synthesis apparatus of the present invention.
Fig. 3 is an enlarged view of the cooling device 11 in fig. 1 of the electrochemical synthesis apparatus for metal-organic framework material according to the present invention.
Fig. 4 is an enlarged view of the moisture removing device 10 shown in fig. 1 of the electrochemical synthesis apparatus for metal-organic framework material according to the present invention.
In the figure: 1. a main body; 2. a support bar; 3. a switch; 4. a cavity door switch; 5. a base; 6. a reaction chamber furnace; 7. a display screen; 8. a visual panel; 9. a control panel; 10. a moisture removal device; 11. a cooling device; 12. a support; 13. parallel reaction kettles; 14. a fixing hole; 15. mounting holes; 16. a semiconductor refrigeration sheet; 17. a heat sink; 18. a cooling fan; 19. a power line; 20. a heat dissipation fan; 21. a ventilation groove; 22. drying the silica gel storage bin; 23. a threaded connection; 24. replacing the cover; 25. and (7) covering.
Detailed Description
In order to make the technical means, creation features, achievement purposes and functions of the present invention easy to understand, the present invention is further described below with reference to the following embodiments.
As shown in fig. 1-4, an electrochemical synthesis apparatus for metal organic framework material comprises a main body 1, a support rod 2 is disposed on the outer surface of the lower end of the main body 1, a base 5 is disposed on the outer surface of the upper end of the support rod 2, a switch 3 is disposed on the outer surface of the front end of the base 5, a reaction chamber furnace 6 is disposed on the outer surface of the upper end of the base 5, a visible panel 8 is disposed on the outer surface of the front end of the reaction chamber furnace 6, a dehumidifying device 10 is disposed on one side of the visible panel 8, a chamber door switch 4 is disposed on the lower end of the dehumidifying device 10, a cooling device 11 is disposed on the outer surface of one side of the dehumidifying device 10, a control panel 9 is disposed on the outer surface of the upper end of the reaction chamber furnace 6, a display 7 is disposed on one end of the control panel 9, a support 12 is, a mounting hole 15 is arranged between the fixing hole 14 and the parallel reaction kettle 13.
Further, cooling device 11 includes semiconductor refrigeration piece 16, radiating groove 17, cooling fan 18, power cord 19 and heat dissipation fan 20, cooling device 11's upper end surface is provided with power cord 19, power cord 19's lower extreme surface is provided with cooling fan 18, one side surface of cooling fan 18 is provided with semiconductor refrigeration piece 16, one side surface of semiconductor refrigeration piece 16 is provided with heat dissipation fan 20, one side surface of heat dissipation fan 20 is provided with radiating groove 17, be favorable to the inside temperature of reaction chamber stove 6 to reduce fast.
Further, remove damp device 10 including ventilative groove 21, dry silica gel storehouse 22, threaded connection spare 23, replace lid 24 and upper cover 25, the lower extreme surface of removing damp device 10 is provided with ventilative groove 21, the upper end surface of ventilative groove 21 is provided with dry silica gel storehouse 22, the upper end surface of dry silica gel storehouse 22 is provided with threaded connection spare 23, the upper end surface of threaded connection spare 23 is provided with upper cover 25, the upper end surface of upper cover 25 is provided with replacement lid 24, be favorable to reducing the inside comdenstion water of reaction chamber stove 6.
Further, be provided with the cross screw between radiating groove 17 and cooling device 11, one side surface of radiating groove 17 passes through the cross screw and is connected with one side surface fixed connection of cooling device 11, be provided with the mounting bracket No. one between heat dissipation fan 20 and the cooling device 11, the lower extreme surface of heat dissipation fan 20 is through the inside fixed connection of a mounting bracket and cooling device 11, be provided with the mounting bracket No. two between cooling fan 18 and the cooling device 11, the lower extreme surface of cooling fan 18 is through the inside fixed connection of mounting bracket No. two and cooling device 11, be favorable to cooling device 11's structural temperature.
Furthermore, a hinge is arranged between the replacing cover 24 and the upper cover 25, the outer surface of one side of the replacing cover 24 is movably connected with the outer surface of the upper end of the upper cover 25 through the hinge, and the outer surface of the lower end of the upper cover 25 is fixedly connected with the outer surface of the upper end of the threaded connecting piece 23, so that the structural temperature of the dehumidifying device 10 is facilitated.
Further, be provided with the set screw between cooling device 11 and the reaction chamber stove 6, one side surface of cooling device 11 passes through the set screw and is connected with one side surface fixed connection of reaction chamber stove 6, and the outer wall that removes damp device 10 passes through threaded connection 23 and can dismantle with the front end surface of reaction chamber stove 6 and be connected, is favorable to the overall structure stability of equipment.
It should be noted that the utility model relates to a metal organic framework material electrochemical synthesis device, before using, the user connects the device with the power line, open the reaction chamber furnace 6 through the chamber door switch 4, take out the parallel reaction kettle 13, put the reactant into the parallel reaction kettle 13, then put the parallel reaction kettle 13 on the bracket 12 to close the reaction chamber furnace 6, open the switch 3, adjust the numerical value on the control panel 9, wait for the reactant to finish synthesizing, the cooling device 11 is arranged, after the device synthesis reaction, the temperature inside the reaction chamber furnace 6 can be rapidly reduced through the arranged semiconductor refrigeration piece 16, the cooling fan 18 can improve the convection of cold air, the heat generated by the semiconductor refrigeration piece 16 can be reduced by the heat dissipation fan 20, prevent the temperature inside the reaction chamber furnace 6 from being too high to influence people to take out, which is beneficial for people's use, the dehumidifying device 10 is arranged, can be after equipment synthesis reaction, through the inside dry silica gel of dry silica gel storehouse 22, with the gas absorption of congealing water, prevent that the comdenstion water from polluting inside reaction chamber stove 6, be favorable to the maintenance of equipment, it is comparatively practical.
The basic principles and the main features of the invention and the advantages of the invention have been shown and described above. It will be understood by those skilled in the art that the present invention is not limited to the above embodiments, and that the foregoing embodiments and descriptions are provided only to illustrate the principles of the present invention without departing from the spirit and scope of the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (6)

1. A metal organic framework material electrochemical synthesis device, comprising a main body (1), characterized in that: the outer surface of the lower end of the main body (1) is provided with a supporting rod (2), the outer surface of the upper end of the supporting rod (2) is provided with a base (5), the outer surface of the front end of the base (5) is provided with a switch (3), the outer surface of the upper end of the base (5) is provided with a reaction chamber furnace (6), the outer surface of the front end of the reaction chamber furnace (6) is provided with a visible panel (8), one side of the visible panel (8) is provided with a dehumidifying device (10), the lower end of the dehumidifying device (10) is provided with a chamber door switch (4), the outer surface of one side of the dehumidifying device (10) is provided with a cooling device (11), the outer surface of the upper end of the reaction chamber furnace (6) is provided with a control panel (9), one end of the control panel (9) is provided with a display screen (7), the, parallel reaction kettles (13) are arranged outside the support (12), a fixing hole (14) is formed in the middle of the support (12), and a mounting hole (15) is formed between the fixing hole (14) and the parallel reaction kettles (13).
2. The metal-organic framework material electrochemical synthesis device of claim 1, wherein: cooling device (11) include semiconductor refrigeration piece (16), radiating groove (17), cooling fan (18), power cord (19) and heat dissipation fan (20), the upper end surface of cooling device (11) is provided with power cord (19), the lower extreme surface of power cord (19) is provided with cooling fan (18), one side surface of cooling fan (18) is provided with semiconductor refrigeration piece (16), one side surface of semiconductor refrigeration piece (16) is provided with heat dissipation fan (20), one side surface of heat dissipation fan (20) is provided with radiating groove (17).
3. The metal-organic framework material electrochemical synthesis device of claim 1, wherein: remove damp device (10) including ventilative groove (21), dry silica gel storehouse (22), threaded connection spare (23), replacement lid (24) and upper cover (25), the lower extreme surface that removes damp device (10) is provided with ventilative groove (21), the upper end surface of ventilative groove (21) is provided with dry silica gel storehouse (22), the upper end surface of dry silica gel storehouse (22) is provided with threaded connection spare (23), the upper end surface of threaded connection spare (23) is provided with upper cover (25), the upper end surface of upper cover (25) is provided with replacement lid (24).
4. The metal-organic framework material electrochemical synthesis device of claim 2, wherein: be provided with the cross screw between radiating groove (17) and cooling device (11), one side surface of radiating groove (17) passes through the cross screw and is connected with one side surface fixed connection of cooling device (11), be provided with the mounting bracket No. one between heat dissipation fan (20) and cooling device (11), the lower extreme surface of heat dissipation fan (20) is through the inside fixed connection of a mounting bracket and cooling device (11), be provided with the mounting bracket No. two between cooling fan (18) and cooling device (11), the lower extreme surface of cooling fan (18) is through the inside fixed connection of mounting bracket No. two and cooling device (11).
5. The metal-organic framework material electrochemical synthesis device of claim 3, wherein: a hinge is arranged between the replacing cover (24) and the upper cover (25), the outer surface of one side of the replacing cover (24) is movably connected with the outer surface of the upper end of the upper cover (25) through the hinge, and the outer surface of the lower end of the upper cover (25) is fixedly connected with the outer surface of the upper end of the threaded connecting piece (23).
6. The metal-organic framework material electrochemical synthesis device of claim 1, wherein: be provided with the fixed screw between cooling device (11) and reaction chamber stove (6), one side surface of cooling device (11) passes through the fixed screw and is connected with one side surface fixed connection of reaction chamber stove (6), the outer wall of dehumidification device (10) passes through threaded connection spare (23) and can dismantle with the front end surface of reaction chamber stove (6) and be connected.
CN201921669361.XU 2019-10-08 2019-10-08 Electrochemical synthesis equipment for metal organic framework material Expired - Fee Related CN210856357U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201921669361.XU CN210856357U (en) 2019-10-08 2019-10-08 Electrochemical synthesis equipment for metal organic framework material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921669361.XU CN210856357U (en) 2019-10-08 2019-10-08 Electrochemical synthesis equipment for metal organic framework material

Publications (1)

Publication Number Publication Date
CN210856357U true CN210856357U (en) 2020-06-26

Family

ID=71288476

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201921669361.XU Expired - Fee Related CN210856357U (en) 2019-10-08 2019-10-08 Electrochemical synthesis equipment for metal organic framework material

Country Status (1)

Country Link
CN (1) CN210856357U (en)

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Granted publication date: 20200626

Termination date: 20211008