CN210846216U

CN210846216U - Ultrasonic mixing device for preparing metal organic material

Info

Publication number: CN210846216U
Application number: CN201921632935.6U
Authority: CN
Inventors: 王新铭; 赵原青; 冯泽民; 马慧媛; 庞海军; 谭立超
Original assignee: Harbin University of Science and Technology
Current assignee: Harbin University of Science and Technology
Priority date: 2019-09-28
Filing date: 2019-09-28
Publication date: 2020-06-26
Anticipated expiration: 2029-09-28

Abstract

The utility model discloses an ultrasonic wave mixing arrangement is used in metal organic material preparation, including mixing box and four supporting legs, four the top outer wall of supporting leg is installed at the bottom four corners outer wall of mixing the box through the bolt respectively, the equal fixed mounting of both sides bottom outer wall of mixing box one end has first rotation motor, and the equal fixed mounting of output shaft of two first rotation motors has first rotation pole. The utility model provides a pair of ultrasonic wave mixing arrangement is used in metal organic material preparation is provided with four inlet pipes through the top at the mixed box to be provided with same passage in the bottom of four inlet pipes, can drop into two to four kinds of materials through the inlet pipe, rotate the motor by the second and drive second dwang and spiral puddler rotation, carry out preliminary effectual mixture to these materials, can also avoid the material to block up in the passage simultaneously, improved the smooth and easy nature of feeding.

Description

Ultrasonic mixing device for preparing metal organic material

Technical Field

The utility model relates to a metal organic material technical field especially relates to an ultrasonic wave mixing arrangement is used in metal organic material preparation.

Background

Organometallic compounds are used in a wide variety of applications in both production and life. For example, in the preparation of high molecular compounds, alkyl aluminum is commonly used as a catalyst, and in organic synthesis, organic metal compounds can provide active intermediates such as carbanions, radicals and carbenes, so that the organic metal compounds are a very useful synthetic reagent.

In the process of metal organic compound production preparation, need use mixing arrangement to carry out mixing treatment to the material, and current mixing arrangement is in the in-process that uses, all stirs the mixture to the material with simple puddler, and this kind of mixed mode has the insufficient problem of mixing, mixes the effect poor, consequently needs to design a neotype metal organic material preparation and solves above-mentioned problem with ultrasonic wave mixing arrangement.

Disclosure of Invention

The utility model aims at solving the defects existing in the prior art and providing an ultrasonic mixing device for preparing metal organic materials.

In order to achieve the above purpose, the utility model adopts the following technical scheme:

the utility model provides an ultrasonic wave mixing arrangement is used in metal organic material preparation, is including mixing box and four supporting legs, four the top outer wall of supporting leg is respectively through the bolt installation at the bottom four corners outer wall of mixing the box, the equal fixed mounting of both sides bottom outer wall of mixing box one end has first rotation motor, and the equal fixed mounting of output shaft of two first rotation motors has first rotation pole, and the equal fixed mounting of circumference outer wall of two first rotation poles has the stirring board that four annular array distribute, the central authorities outer wall fixed mounting who mixes box one end bottom has supersonic generator, and supersonic generator has ultrasonic emitter through spring coupling, and ultrasonic emitter's one end outer wall passes through the spring coupling at the inner wall of mixing the box other end, the equal fixed mounting of both sides outer wall at ultrasonic emitter top has the stock guide.

Preferably, the outer walls of four corners at the top of the mixing box body are fixedly provided with the feeding pipes, and the outer walls at the bottoms of the four feeding pipes are fixedly provided with the same vertically-arranged material guide pipes.

Preferably, the outer wall fixed mounting in the middle of the top of mixing box has the second to rotate the motor, and the output shaft fixed mounting that the second rotated the motor has the second dwang of vertical setting, and the circumference outer wall fixed mounting of second dwang has the spiral puddler.

Preferably, the outer wall of the bottom center of the mixing box body is fixedly provided with a discharging pipe, and the inner wall of the periphery of the top of the discharging pipe is fixedly provided with the same discharging valve.

Preferably, the first rotating motor, the second rotating motor and the ultrasonic generator are all electrically connected with a switch through a wire, and the switch is electrically connected with a power supply through a wire.

Preferably, the bottom outer wall of mixing box one side has seted up the maintenance mouth, and the outer wall of the one end of maintenance mouth has the maintenance lid through hinged joint, maintenance lid one side middle part outer wall fixed mounting has the handle.

The utility model has the advantages that:

1. the utility model provides a pair of ultrasonic wave mixing arrangement is used in metal organic material preparation is provided with four inlet pipes through the top at the mixed box to be provided with same passage in the bottom of four inlet pipes, can drop into two to four kinds of materials through the inlet pipe, rotate the motor by the second and drive second dwang and spiral puddler rotation, carry out preliminary effectual mixture to these materials, can also avoid the material to block up in the passage simultaneously, improved the smooth and easy nature of feeding.

2. The utility model provides a pair of ultrasonic wave mixing arrangement is used in metal organic material preparation, be provided with first rotation motor through the bottom at the mixed box, first rotation pole, the stirring board, supersonic generator and ultrasonic emitter, can produce ultrasonic vibration by supersonic generator, and transmit this vibration to the material by ultrasonic emitter, realize mixing the further vibration of preliminary mixed back material, the effect that the material mixes has been improved, it rotates to drive the stirring board by first rotation motor simultaneously, realize the mixing to mixing the bottom half material, further improve the sufficiency of mixing.

3. The utility model provides a pair of ultrasonic wave mixing arrangement is used in metal organic material preparation, in embodiment 2, through being provided with maintenance mouth and maintenance lid in one side of mixing the box, can maintain and clear up device inside through the maintenance mouth, improved the convenience of device maintenance clearance.

Drawings

Fig. 1 is a schematic structural view of an ultrasonic mixing device for preparing a metal organic material according to the present invention;

FIG. 2 is a schematic cross-sectional view of a mixing box of embodiment 1 of an ultrasonic mixing apparatus for preparing a metal-organic material according to the present invention;

FIG. 3 is a schematic view of a partial side structure of an ultrasonic transmitter of an ultrasonic mixing device for preparing metal organic materials according to the present invention;

fig. 4 is a schematic view of a partial cross-sectional structure of a mixing box in embodiment 2 of an ultrasonic mixing device for preparing a metal organic material according to the present invention.

In the figure: the device comprises a first rotating motor 1, an ultrasonic generator 2, a second rotating motor 3, a feeding pipe 4, a mixing box 5, a first rotating rod 6, a stirring plate 7, a spiral stirring rod 8, a second rotating rod 9, a material guide pipe 10, a material guide plate 11, an ultrasonic transmitting device 12, a material discharge pipe 13 and a maintenance cover 14.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.

Example 1

Referring to fig. 1 to 3, an ultrasonic mixing apparatus for preparing a metal organic material includes a mixing box 5 and four support legs, the top outer walls of the four support legs are respectively installed on the outer walls of the four corners of the bottom of the mixing box 5 through bolts, the outer walls of the bottoms of both sides of one end of the mixing box 5 are connected with a first rotating motor 1 through bolts, the output shafts of the two first rotating motors 1 are connected with first rotating rods 6 through bolts, the circumferential outer walls of the two first rotating rods 6 are connected with four stirring plates 7 distributed in an annular array through bolts, the central outer wall at the bottom of one end of the mixing box body 5 is connected with an ultrasonic generator 2 through bolts, and the ultrasonic generator 2 is connected with an ultrasonic transmitting device 12 through a spring, the outer wall of one end of the ultrasonic transmitting device 12 is connected with the inner wall of the other end of the mixing box body 5 through a spring, and the outer walls of two sides of the top of the ultrasonic transmitting device 12 are connected with a material guide plate 11 through bolts.

In the utility model, the outer walls of the four corners at the top of the mixing box body 5 are all connected with the feeding pipes 4 through bolts, and the outer walls at the bottom of the four feeding pipes 4 are connected with the same vertically arranged material guide pipe 10 through bolts;

the outer wall of the center of the top of the mixing box body 5 is connected with a second rotating motor 3 through a bolt, the output shaft of the second rotating motor 3 is connected with a second rotating rod 9 which is vertically arranged through a bolt, and the outer wall of the circumference of the second rotating rod 9 is connected with a spiral stirring rod 8 through a bolt;

the outer wall of the center of the bottom of the mixing box body 5 is connected with a discharge pipe 13 through bolts, and the inner walls of the tops of the periphery of the discharge pipe 13 are connected with the same discharge valve through bolts;

first rotating electrical machines 1, second rotating electrical machines 3 and supersonic generator 2 all have the switch through wire electric connection, and the switch has the power through wire electric connection.

Example 2

Referring to fig. 1-4, an ultrasonic wave mixing arrangement is used in metal organic material preparation still includes the maintenance mouth of seting up at mixing box 5 one side bottom outer wall, and the outer wall of the one end of maintenance mouth has maintenance lid 14 through hinged joint, and there is the handle maintenance lid 14 one side middle part outer wall through bolted connection, can maintain and clear up the device inside through the maintenance mouth, has improved the convenience of device maintenance clearance.

The working principle is as follows: when in use, all the driving parts, which refer to power elements, electric devices and adaptive power supplies, are connected through leads at idle positions of the device, the electric connection among the electric devices is completed sequentially by working sequence, the detailed connection means is a known technology in the field, the following main introduces working principles and processes without explaining electrical control, then two to four materials which need to be mixed are respectively put into a mixing box body 5 through a feeding pipe 4, simultaneously a second rotating motor 3, a first rotating motor 1 and an ultrasonic generator 2 are started, the second rotating motor 3 drives a second rotating rod 9 and a spiral stirring rod 8 to rotate, the materials are preliminarily and effectively mixed, the ultrasonic generator 2 generates ultrasonic vibration, the vibration is transmitted to the materials by an ultrasonic emitting device 12, and further vibration mixing of the preliminarily mixed materials is realized, the effect that the material was mixed is improved, is driven stirring board 7 by first rotation motor 1 simultaneously and rotates, realizes the mixing to 5 bottom materials of mixing box, further improves the sufficiency of mixing.

The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims

1. An ultrasonic mixing device for preparing metal organic materials comprises a mixing box body (5) and four supporting legs, and is characterized in that the top outer walls of the four supporting legs are respectively installed on the outer walls of the four corners of the bottom of the mixing box body (5) through bolts, the outer walls of the bottoms of the two sides of one end of the mixing box body (5) are respectively and fixedly provided with a first rotating motor (1), the output shafts of the two first rotating motors (1) are respectively and fixedly provided with a first rotating rod (6), the outer walls of the circumferences of the two first rotating rods (6) are respectively and fixedly provided with four stirring plates (7) distributed in an annular array, the outer wall of the center of the bottom of one end of the mixing box body (5) is fixedly provided with an ultrasonic generator (2), the ultrasonic generator (2) is connected with an ultrasonic emission device (12) through a spring, the outer wall of one end of the ultrasonic emission device, and material guide plates (11) are fixedly arranged on the outer walls of the two sides of the top of the ultrasonic transmitting device (12).

2. The ultrasonic mixing device for preparing the metal organic material according to claim 1, wherein the feeding pipes (4) are fixedly installed on the outer walls of four corners of the top of the mixing box body (5), and the same vertically-arranged material guiding pipe (10) is fixedly installed on the outer walls of the bottom of the four feeding pipes (4).

3. The ultrasonic mixing device for preparing the metal organic material according to claim 2, wherein a second rotating motor (3) is fixedly installed on the outer wall of the center of the top of the mixing box body (5), a second rotating rod (9) which is vertically arranged is fixedly installed on an output shaft of the second rotating motor (3), and a spiral stirring rod (8) is fixedly installed on the outer wall of the circumference of the second rotating rod (9).

4. The ultrasonic mixing device for preparing metal organic material according to claim 1, wherein a discharging pipe (13) is fixedly installed on the outer wall of the center of the bottom of the mixing box body (5), and the same discharging valve is fixedly installed on the inner wall of the top of the periphery of the discharging pipe (13).

5. The ultrasonic mixing device for preparing metal organic material according to claim 3, wherein the first rotating motor (1), the second rotating motor (3) and the ultrasonic generator (2) are electrically connected with a switch through a wire, and the switch is electrically connected with a power supply through a wire.

6. The ultrasonic mixing device for preparing the metal organic material as recited in claim 1, wherein a maintenance opening is formed in an outer wall of a bottom of one side of the mixing box body (5), a maintenance cover (14) is connected to an outer wall of one end of the maintenance opening through a hinge, and a handle is fixedly mounted on an outer wall of a middle of one side of the maintenance cover (14).