CN210522508U - Reaction kettle for synthesis of nano material - Google Patents

Reaction kettle for synthesis of nano material Download PDF

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Publication number
CN210522508U
CN210522508U CN201921339004.7U CN201921339004U CN210522508U CN 210522508 U CN210522508 U CN 210522508U CN 201921339004 U CN201921339004 U CN 201921339004U CN 210522508 U CN210522508 U CN 210522508U
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China
Prior art keywords
reaction kettle
heating
heat conduction
top cover
heating outer
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Expired - Fee Related
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CN201921339004.7U
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Chinese (zh)
Inventor
刘建波
尚永辉
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Xianyang Normal University
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Xianyang Normal University
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Priority to CN201921339004.7U priority Critical patent/CN210522508U/en
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Publication of CN210522508U publication Critical patent/CN210522508U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a belong to reation kettle technical field, specifically be a synthetic reation kettle that uses of nano-material, it includes: reation kettle main part, top cap, motor, heating outer container and connecting pipe, reation kettle main part top fixed mounting top cap, the equal fixed mounting in top cap top left and right sides has the inlet pipe, the inlet pipe top all is provided with sealed lid, top cap top right side is provided with the thermometer, top cap top left side is provided with the manometer, top cap top left side is provided with the relief valve, the top cap top sets up the motor, can filter the steam of heating, avoids heating the outer box in impurity pile up influence reation kettle life, and connecting pipe can dismantle, conveniently clears up the heating outer container, improves the inside heat conduction speed of heating outer container, and the heat conduction and the cooling of being convenient for are convenient for detect inside reflection pressure, improve the security of reaction process.

Description

Reaction kettle for synthesis of nano material
Technical Field
The utility model relates to a reation kettle technical field specifically is a synthetic reation kettle that uses of nano-material.
Background
The broad understanding of the reaction kettle is that the reaction kettle is a container for physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container. The material of the reaction kettle generally comprises carbon manganese steel, stainless steel, zirconium, nickel-based (Hastelloy and Monel) alloy and other composite materials. The reaction kettle can be made of stainless steel materials such as SUS304, SUS316L, etc. The stirrer has anchor type, frame type, paddle type, turbine type, scraper type and combined type, and the rotating mechanism can adopt a cycloidal pin gear speed reducer, a stepless speed reducer or variable frequency speed regulation and the like, so that the special reaction requirements of various materials can be met. The sealing device can adopt sealing structures such as mechanical sealing, packing sealing and the like. The heating, cooling can adopt structure such as press from both sides cover, half pipe, coil pipe, miller board, and the heating method has: steam, electric heating and heat conducting oil, so as to meet the technological requirements of different working environments of acid resistance, high temperature resistance, wear resistance, corrosion resistance and the like. And can be designed and manufactured according to the technological requirements of users.
At present, current steam heating formula reation kettle can't filter steam, piles up impurity in making the pipeline easily, uses easy corrosion reation kettle for a long time, connects the inconvenient dismantlement of trachea, and is inconvenient to reation kettle clears up, can't detect internal reaction pressure, can not in time release pressure, explodes easily, and the security is lower.
SUMMERY OF THE UTILITY MODEL
This section is for the purpose of summarizing some aspects of embodiments of the invention and to briefly introduce some preferred embodiments. Some simplifications or omissions may be made in this section and in the abstract of the specification and the title of the application to avoid obscuring the purpose of this section, the abstract of the specification and the title of the application, and such simplifications or omissions are not intended to limit the scope of the invention.
In view of the above and/or the problems existing in the existing reaction kettle for synthesizing nano materials, the utility model is provided.
Therefore, the utility model aims at providing a synthetic reation kettle that uses of nano-material can filter the steam of heating, avoids in the heating outer box impurity pile up influence reation kettle life, and the connecting tube can be dismantled, conveniently clears up the heating outer box, improves the inside heat conduction speed of heating outer box, is convenient for heat conduction and cooling, is convenient for detect inside reflection pressure, improves the security of reaction process. For solving the technical problem, according to the utility model discloses an aspect, the utility model provides a following technical scheme:
a reaction kettle for synthesizing nano materials comprises: the reaction kettle comprises a reaction kettle main body, a top cover, a motor, a heating outer box and a connecting air pipe, wherein the top cover is fixedly arranged at the top of the reaction kettle main body, the left side and the right side of the top cover are fixedly provided with feeding pipes, the top of each feeding pipe is provided with a sealing cover, the right side of the top cover is provided with a thermometer, the left side of the top cover is provided with a pressure gauge, the left side of the top cover is provided with a pressure relief valve, the top of the top cover is provided with the motor, the bottom of the motor is connected with a speed reducer, the bottom of the speed reducer is connected with a shaft rod extending into an inner cavity of the reaction kettle main body, the bottom of the shaft rod is fixedly provided with a stirring rod, the top of the stirring rod is fixedly provided with a stirring auxiliary rod, the outer side of the bottom of, the heat conduction cavity inner chamber is provided with the circulation heat pipe, the equal fixed mounting in heating outer container left and right sides connects the trachea, it all is provided with the filter screen to connect the trachea inner chamber.
As the utility model discloses a synthetic reation kettle of using of nano-material a preferred scheme, wherein: the bottom of the reaction kettle main body is provided with a discharge pipe, and a discharge valve is arranged on the discharge pipe.
As the utility model discloses a synthetic reation kettle of using of nano-material a preferred scheme, wherein: and the connecting position of the connecting air pipe and the heating outer box is provided with threads matched with each other.
As the utility model discloses a synthetic reation kettle of using of nano-material a preferred scheme, wherein: the equal fixed mounting in heating outer container bottom left and right sides has the landing leg, the equal fixed mounting in landing leg bottom has the gyro wheel.
As the utility model discloses a synthetic reation kettle of using of nano-material a preferred scheme, wherein: sealing gaskets are arranged between the connecting air pipes and the heating outer box and are made of rubber.
Compared with the prior art: the temperature inside the reaction kettle main body is detected through a thermometer, the pressure inside the reaction kettle main body is detected through a pressure gauge, redundant pressure inside the reaction kettle main body is discharged through a pressure release valve, explosion is avoided, the use safety is improved, under the power of a motor, a shaft rod rotates, materials in an inner cavity of the reaction kettle main body are stirred through a stirring rod and a stirring auxiliary rod, the reaction speed is improved, steam circulates through a heat conduction cavity and transfers heat, a steam outlet pipe is used for flowing out steam, a condensate outlet pipe is used for flowing out condensate and transferring heat through a circulating heat conduction pipe, the propagation speed of the steam temperature is improved, when cooling is carried out, the steam temperature inside the heat conduction cavity can quickly reach a uniform state, a right connecting air pipe is used for circulating hot steam to heat the reaction kettle main body, and a left connecting air pipe is used for circulating cold air to, the filter screen is used for filtering the impurity that lets in the inside gas of heat conduction intracavity, avoid heat conduction intracavity impurity to pile up corruption reation kettle main part and heating outer container, can filter the steam of heating, avoid in the heating outer container impurity pile up influence reation kettle life, connect the trachea and can dismantle, conveniently clear up the heating outer container, improve the inside heat conduction velocity of heating outer container, be convenient for heat conduction and cooling, be convenient for detect inside reflection pressure, improve the security of reaction process.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the present invention will be described in detail with reference to the accompanying drawings and detailed embodiments, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without inventive labor. Wherein:
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an enlarged schematic view of the structure of the reaction kettle for synthesizing nano-materials according to the present invention;
fig. 3 is the schematic view of the structure of the circulation heat conduction pipe of the present invention.
Detailed Description
In order to make the above objects, features and advantages of the present invention more comprehensible, embodiments of the present invention are described in detail below with reference to the accompanying drawings.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention, but the present invention may be implemented in other ways than those specifically described herein, and one skilled in the art may similarly generalize the present invention without departing from the spirit of the present invention, and therefore the present invention is not limited to the specific embodiments disclosed below.
Next, the present invention will be described in detail with reference to the schematic drawings, and in the detailed description of the embodiments of the present invention, for convenience of explanation, the sectional view showing the device structure will not be enlarged partially according to the general scale, and the schematic drawings are only examples, and should not limit the scope of the present invention. In addition, the three-dimensional dimensions of length, width and depth should be included in the actual fabrication.
In order to make the objects, technical solutions and advantages of the present invention clearer, embodiments of the present invention will be described in further detail below with reference to the accompanying drawings.
The utility model provides a synthetic reation kettle that uses of nano-material can filter the steam of heating, avoids in the heating outer tank impurity to pile up influence reation kettle life, and connecting pipe can dismantle, conveniently clears up the heating outer tank, improves the inside heat conduction speed of heating outer tank, and the heat conduction and the cooling of being convenient for are convenient for detect inside reflection pressure, improve the security of reaction process, please refer to and draw back to figure 1, include: the reaction kettle comprises a reaction kettle main body 100, a top cover 200, a motor 300, a heating outer box 400 and a connecting air pipe 500;
referring to fig. 1 again, the reaction vessel body 100 contains the nano-material to provide a space for the synthesis of the nano-material.
Referring to fig. 1 again, the top cover 200 includes a feeding pipe 210, a sealing cover 211, a thermometer 220, a pressure gauge 230 and a pressure relief valve 240, and specifically, the top cover 200 is mounted on the top of the reaction vessel body 100 by being fastened by screws, the reaction kettle main body 100 is sealed, the feeding pipes 210 are welded at the left side and the right side of the top cover 200, the material is fed through the feeding pipe 210, the top of the feeding pipe 210 is provided with a sealing cover 211, the sealing cover 211 is used for sealing the feeding pipe 210 to prevent the main body 100 of the reaction kettle from spraying during reaction, the right side of the top cover 200 is embedded with a thermometer 220, the temperature inside the reaction kettle main body 100 is detected through the temperature gauge 220, the pressure gauge 230 is embedded at the left side of the top cover 200, the pressure gauge 230 is used for detecting the internal pressure of the reaction kettle main body 100, the pressure relief valve 240 is embedded and installed on the left side of the top cover 200, the excessive pressure in the reaction kettle main body 100 is discharged through the pressure release valve 240, so that explosion is avoided, and the use safety is improved.
Referring to fig. 1 again, the motor 300 includes a speed reducer 310, a shaft rod 320, a stirring rod 330 and a stirring auxiliary rod 340, specifically, the motor 300 is disposed on the top of the top cover 200, the bottom of the motor 300 is connected to the speed reducer 310, the speed reducer 310 is locked and installed on the top of the top cover 200 by screws, the speed reducer 310 is used for limiting the transmission of the rotation speed of the motor 300, the bottom of the speed reducer 310 is connected to the shaft rod 320 extending into the inner cavity of the reaction kettle main body 100, the stirring rod 330 is welded to the bottom of the shaft rod 320, the stirring rods 330 are distributed on the left side and the right side of the shaft rod 320, the stirring auxiliary rod 340 is welded to the stirring rod 330, under the power of the motor 300, the shaft rod 320 rotates, the materials in the inner cavity.
Referring to fig. 1 and 3, the heating outer box 400 includes a heat conduction cavity 410, a steam outlet pipe 420, a condensate outlet pipe 430 and a circulation heat pipe 440, specifically, the heating outer box 400 is welded on the outer wall of the reaction kettle main body 100, the heat conduction cavity 410 is arranged between the heating outer box 400 and the reaction kettle main body 100, steam flows through the heat conduction cavity 410, heat is transferred, the steam outlet pipe 420 is arranged at the top of the left side of the heat conduction cavity 410, the steam outlet pipe 420 is used for flowing steam out, the condensate outlet pipes 430 are arranged on the left side and the right side of the bottom of the heat conduction cavity 410, the condensate outlet pipes 430 are used for flowing out condensate, the circulation heat pipe 440 is arranged in the inner cavity of the heat conduction cavity 410, heat is transferred through the circulation heat pipe 440, the propagation speed of steam temperature.
Referring to fig. 1 and 2, the connecting air pipe 500 includes a filter screen 510, specifically, the connecting air pipe 500 is installed at the left and right sides of the heating outer box 400 in an embedded manner, the right connecting air pipe 500 is used for circulating hot steam to heat the reaction kettle main body 100, the left connecting air pipe 500 is used for circulating cold air to cool the reaction kettle main body 100, the filter screen 510 is installed in the connecting air pipe 500 in an embedded manner, the filter screen 510 is used for filtering impurities introduced into the gas inside the heat conduction cavity 410, and the impurities in the inner cavity of the heat conduction cavity 410 are prevented from being accumulated to corrode the reaction kettle main body 100 and the heating outer box 400.
When the temperature-measuring device is used specifically, the temperature inside the reaction kettle main body 100 is detected through the thermometer 220, the pressure inside the reaction kettle main body 100 is detected through the pressure gauge 230, redundant pressure inside the reaction kettle main body 100 is discharged through the pressure release valve 240, explosion is avoided, the use safety is improved, under the power of the motor 300, the shaft lever 320 rotates, materials in the inner cavity of the reaction kettle main body 100 are stirred through the stirring rod 330 and the stirring auxiliary rod 340, the reaction rate is improved, steam flows through the heat conduction cavity 410 to transfer heat, the steam outlet pipe 420 is used for flowing out steam, the condensate outlet pipe 430 is used for flowing out condensate, heat is transferred through the circulating heat conduction pipe 440 to improve the propagation speed of steam temperature, when cooling is carried out, the steam temperature inside the heat conduction cavity 410 can quickly reach a uniform state, the right connecting air pipe 500 is used for flowing through the hot steam to heat the reaction kettle main, connecting trachea 500 is used for circulating cold air and cooling down reation kettle main part 100 on the left side, and filter screen 510 is used for filtering the impurity that lets in the inside gas of heat conduction chamber 410, avoids heat conduction chamber 410 inner chamber impurity to pile up corruption reation kettle main part 100 and heating outer container 400.
Referring to fig. 1 again, for convenience of use, a discharge pipe 110 is disposed at the bottom of the reaction vessel main body 100, and a discharge valve 120 is disposed on the discharge pipe 110.
For convenience of installation, the connecting position of the connecting air pipe 500 and the heating outer box 400 is provided with mutually matched threads.
Referring to fig. 1 again, for convenience of use, the left and right sides of the bottom of the heating outer box 400 are fixedly provided with support legs 450, and the bottoms of the support legs 450 are fixedly provided with rollers 460.
Referring to fig. 1 and 2 again, in order to improve air tightness, a gasket 520 is disposed between the connecting air pipe 500 and the heating outer box 400, and the gasket 520 is made of rubber.
While the invention has been described above with reference to an embodiment, various modifications may be made and equivalents may be substituted for elements thereof without departing from the scope of the invention. In particular, as long as there is no structural conflict, the various features of the disclosed embodiments of the present invention can be used in any combination with each other, and the non-exhaustive description of these combinations in this specification is merely for the sake of brevity and resource conservation. Therefore, it is intended that the invention not be limited to the particular embodiments disclosed, but that the invention will include all embodiments falling within the scope of the appended claims.

Claims (5)

1. A reaction kettle for synthesizing nano materials is characterized by comprising: the reaction kettle comprises a reaction kettle main body (100), a top cover (200), a motor (300), a heating outer box (400) and a connecting air pipe (500), wherein the top cover (200) is fixedly installed at the top of the reaction kettle main body (100), feeding pipes (210) are fixedly installed on the left side and the right side of the top cover (200), sealing covers (211) are arranged on the tops of the feeding pipes (210), a thermometer (220) is arranged on the right side of the top cover (200), a pressure gauge (230) is arranged on the left side of the top cover (200), a pressure release valve (240) is arranged on the left side of the top cover (200), the motor (300) is arranged on the top of the top cover (200), a speed reducer (310) is connected to the bottom of the motor (300), a shaft lever (320) extending into, stirring rod (330) top fixed mounting has stirring auxiliary rod (340), reation kettle main part (100) bottom outside sets up heating outer container (400), be provided with between heating outer container (400) and reation kettle main part (100) heat conduction chamber (410), heat conduction chamber (410) left side top is provided with steam outlet pipe (420), heat conduction chamber (410) bottom left and right sides all is provided with condensate outlet pipe (430), heat conduction chamber (410) inner chamber is provided with circulation heat pipe (440), the equal fixed mounting in heating outer container (400) left and right sides connects trachea (500), it all is provided with filter screen (510) to connect trachea (500) inner chamber.
2. The reactor for synthesizing nano-materials according to claim 1, wherein a discharge pipe (110) is disposed at the bottom of the reactor main body (100), and a discharge valve (120) is disposed on the discharge pipe (110).
3. The reaction kettle for synthesizing nano-materials according to claim 1, wherein the connecting position of the connecting air pipe (500) and the heating outer box (400) is provided with mutually matched screw threads.
4. The reactor as claimed in claim 1, wherein the left and right sides of the bottom of the outer heating box (400) are fixedly provided with legs (450), and the bottoms of the legs (450) are fixedly provided with rollers (460).
5. The reaction kettle for synthesizing nano-materials according to claim 1, wherein a sealing gasket (520) is arranged between the connecting air pipe (500) and the heating outer box (400), and the sealing gasket (520) is made of rubber.
CN201921339004.7U 2019-08-16 2019-08-16 Reaction kettle for synthesis of nano material Expired - Fee Related CN210522508U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201921339004.7U CN210522508U (en) 2019-08-16 2019-08-16 Reaction kettle for synthesis of nano material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921339004.7U CN210522508U (en) 2019-08-16 2019-08-16 Reaction kettle for synthesis of nano material

Publications (1)

Publication Number Publication Date
CN210522508U true CN210522508U (en) 2020-05-15

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CN201921339004.7U Expired - Fee Related CN210522508U (en) 2019-08-16 2019-08-16 Reaction kettle for synthesis of nano material

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111701554A (en) * 2020-05-26 2020-09-25 江苏益通流体科技有限公司 Mechanical seal assembly capable of measuring internal pressure for carbon steel reaction kettle
CN112010688A (en) * 2020-09-03 2020-12-01 盘锦华晨石油装备制造有限公司 Constant temperature biodegradation tank

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111701554A (en) * 2020-05-26 2020-09-25 江苏益通流体科技有限公司 Mechanical seal assembly capable of measuring internal pressure for carbon steel reaction kettle
CN112010688A (en) * 2020-09-03 2020-12-01 盘锦华晨石油装备制造有限公司 Constant temperature biodegradation tank

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20200515

Termination date: 20210816