CN210495325U - Filtering bottle filling device - Google Patents

Filtering bottle filling device Download PDF

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Publication number
CN210495325U
CN210495325U CN201921295374.5U CN201921295374U CN210495325U CN 210495325 U CN210495325 U CN 210495325U CN 201921295374 U CN201921295374 U CN 201921295374U CN 210495325 U CN210495325 U CN 210495325U
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China
Prior art keywords
cylinder body
plate
waste liquid
bottle
sample injection
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CN201921295374.5U
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Chinese (zh)
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宋薇
王文娟
李闯
李佳
冯辉
邢东
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Pony Test Group Jilin Co ltd
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Pony Test Group Jilin Co ltd
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Abstract

The utility model relates to a filter bottling device relates to laboratory utensil technical field, has solved because some detection methods often can establish ties two and purify the post, and ordinary solid phase extraction device can't satisfy the experiment requirement, often needs to carry out twice purification, not only wastes time but also hard technical problem. The device is technically characterized by comprising a cylinder body, wherein detection equipment is placed in the cylinder body, a plurality of through holes are formed in a top plate of the cylinder body and used for inserting purification columns, a glass door is rotatably connected in front of the cylinder body, and a glass baffle is arranged at the front end of the cylinder body and used for preventing organic waste liquid in the cylinder body from flowing out; the detection device includes: waste liquid groove, color comparison pipe support, advance kind bottle frame, balanced support, purification column adapter with adjustable. The device has the effects of simple structure, convenience in operation and high practicability.

Description

Filtering bottle filling device
Technical Field
The utility model relates to a laboratory apparatus technical field, in particular to filter bottling device.
Background
With the rapid development of the detection industry, various national, industrial and local standards are more and more, many new detection standards are continuously generated, the control requirements of the various standards on the pretreatment process are continuously updated, the detection accuracy is higher and higher, due to the higher and higher complexity of the sample matrix, the purification column for the sample pretreatment is gradually converted into a commercial finished product from the original manual filling, the traditional single purification process is also converted into a plurality of substances for purification, and thus, higher requirements are provided for the solid phase extraction device.
The solid phase extraction device widely used at present has certain limitation. The waste liquid tank is inconvenient to replace, so that organic reagents are often poured to pollute an experiment table; the effluent receiving rack is not standard, and the sample injection bottle cannot be used for receiving effluent; because some detection methods can be connected with two purifying columns in series, a common solid phase extraction device can not meet the experimental requirements, and two times of purification is required, so that the time and the labor are wasted.
Moreover, the existing solid phase extraction device is integrated, cannot be disassembled and replaced, and the cylinder body cannot be cleaned up, so that various pollutants are left, and a test object is polluted.
Based on this, it is very necessary to design a novel multifunctional filtering bottle filling device which can be suitable for different receiving bottles and is relatively convenient, flexible and changeable.
SUMMERY OF THE UTILITY MODEL
The utility model discloses it is inconvenient to solve waste liquid groove among the prior art and change, often lead to organic reagent to spill, pollute the laboratory bench, because some detection methods often can establish ties two and purify the post, ordinary solid phase extraction device can't satisfy the experiment requirement, often need carry out twice purification, it is both time-consuming and hard, present solid phase extraction device is all integrative, can't dismantle the change, the cylinder body is clean not cleaned, will cause various pollutants to remain, thereby pollute test object's technical problem, a filtration bottling device is provided.
In order to solve the technical problem, the technical scheme of the utility model is specifically as follows:
a filter bottle filling apparatus comprising: the device comprises a cylinder body, a plurality of through holes are formed in the top plate of the cylinder body and used for inserting purification columns, a glass door is rotatably connected in front of the cylinder body, and a glass baffle is arranged in front of the cylinder body and used for preventing organic waste liquid in the cylinder body from flowing out;
the detection device includes: the device comprises a waste liquid tank, a colorimetric tube stand, a sample injection bottle stand, an adjustable balance support and a purifying column adapter;
the waste liquid tank is used for collecting waste liquid flowing out of the purification column;
the colorimetric tube frame is an upper three-layer plate, a middle three-layer plate and a lower three-layer plate, the upper three-layer plate, the middle three-layer plate and the lower three-layer plate are fixed by fixing columns, mounting holes are formed in the upper three-layer plate and the middle three-layer plate and used for placing colorimetric tubes, the positions of the mounting holes correspond to the positions of through holes in a top plate of the cylinder body one by one, and the lower three;
the sample injection bottle rack is a fixed plate with the thickness of 1cm, a plurality of sample injection bottle holes are formed in the sample injection bottle rack and used for placing sample injection bottles, and the positions of the sample injection bottle holes correspond to the positions of the through holes in the top plate of the cylinder body one by one;
the adjustable balance support is a normal lifting support and is used for adjusting the heights of the waste liquid tank, the colorimetric tube stand and the sample injection bottle stand;
the purification column adapter is used for connecting two purification columns in series.
Preferably, a sealing sleeve is detachably mounted at the through hole on the top plate of the cylinder body, the purification column is divided into a first cylinder body and a second cylinder body, and the second cylinder body of the purification column penetrates through the sealing sleeve and extends into the cylinder body.
Preferably, the bottom side of the cylinder body is provided with a vacuum tube, the vacuum tube is connected with a pressure gauge, one end of the vacuum tube is connected with a vacuum pump, and the bottom surface of the cylinder body is also provided with four nylon anchor feet.
Preferably, the periphery of the glass door is provided with a sealing ring, and the sealing ring is attached to the outer wall of the cylinder body.
Preferably, the bottom of the cylinder body is provided with three positioning plates, the positioning plates are used for positioning the waste liquid tank, the colorimetric pipe frame, the sample injection bottle frame and the adjustable balance support, a nylon plate is laid in the interior surrounded by the positioning plates, the detection equipment is placed above the nylon plate, and the nylon plate is used for isolating the detection equipment from the cylinder body.
Preferably, a second positioning plate is arranged on the lifting plate above the adjustable balance support and is used for positioning the waste liquid tank, the colorimetric tube frame and the sample injection bottle frame;
the top of the purifying column adapter is in a plane circular shape, the middle of the purifying column adapter is provided with a hollow design with round holes, and the purifying column adapter is a circular platform with the diameter gradually reduced from top to bottom and is used for being matched with purifying columns of different models.
The utility model discloses following beneficial effect has:
the utility model discloses a filter bottling device selects different mounting means, convenient, the light purification mode that changes according to different purification mode. This filter bottling device has the effect that the structure is succinct, convenient operation, and the practicality is strong. By arranging the waste liquid tank and the glass baffle, the organic reagent can be prevented from spilling to pollute the experiment table; the problem of series connection of two purification columns is solved by arranging the purification column adapter, and the technical problems that an ordinary solid phase extraction device cannot meet experimental requirements and needs to be purified twice frequently, so that time and labor are wasted due to the fact that two purification columns are often connected in series in some detection methods are solved; the sealing sleeve is installed through the colorimetric tube support, the sample injection bottle support, the adjustable balance support and the detachable which are movably installed, the problem that the existing solid-phase extraction device is integrated, cannot be disassembled and replaced, and the cylinder body cannot be cleaned up, so that various pollutants are remained, and the technical problem that a test object is polluted is solved.
Drawings
The present invention will be described in further detail with reference to the accompanying drawings and specific embodiments.
FIG. 1 is a schematic structural view of a filtering bottle-filling device of the present invention for collecting waste liquid;
fig. 2 is a schematic view of a filtering bottle filling device of the present invention collecting waste liquid by using an adjustable balance bracket;
fig. 3 is a schematic view of a bottle filter filling device of the present invention collecting liquid through a colorimetric tube stand by using an adjustable balance stand;
FIG. 4 is a schematic view of the operation of the filtration bottle filling device in series with the purification column of the present invention;
fig. 5 is a schematic view of the purification column adapter of the filtration bottle filling device of the present invention connecting in series with the purification column;
fig. 6 is the installation schematic diagram of the purification column of the filtration bottle filling device and the sealing sleeve on the cylinder body top plate of the utility model.
The reference numerals in the figures denote:
1. a cylinder body; 2. a vacuum tube; 3. a pressure gauge; 4. sealing sleeves; 5. purifying the column; 6. a seal ring; 7. a glass door; 8. a glass baffle; 9. a waste liquid tank; 10. positioning a plate; 11. a nylon plate; 12. an adjustable balance support; 13. a second positioning plate; 14. a colorimetric tube stand; 15. a colorimetric cylinder; 16. a purifying column adapter; 17. nylon anchor feet; 18. a sample injection bottle holder; 19. and (4) sampling bottles.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-6, a filtering bottle filling apparatus includes: the detection device comprises a cylinder body 1, wherein detection equipment is placed in the cylinder body 1, a plurality of through holes are formed in the top plate of the cylinder body 1 and used for inserting purification columns 5, a glass door 7 is rotatably connected in front of the cylinder body 1, a glass baffle 8 is arranged in front of the cylinder body 1, and the glass baffle 8 is used for preventing organic waste liquid in the cylinder body 1 from flowing out;
the detection device includes: a waste liquid tank 9, a colorimetric tube frame 14, a sample injection bottle frame 18, an adjustable balance bracket 12 and a purifying column adapter 16;
the waste liquid tank 9 is used for collecting waste liquid flowing out of the purifying column 5; the colorimetric tube frame 14 is an upper, middle and lower three-layer plate, the upper, middle and lower three-layer plates are fixed by fixing columns, the upper and middle three-layer plates are provided with mounting holes for placing the colorimetric tubes 15, the positions of the mounting holes correspond to the positions of through holes of a top plate of the cylinder body 1 one by one, and the lower layer plate is a flat plate; the sample bottle rack 18 is a fixing plate with the thickness of 1cm and is provided with a plurality of sample bottle holes, the sample bottle holes are used for placing sample bottles 19, and the positions of the sample bottle holes correspond to the positions of through holes on a top plate of the cylinder body 1 one by one; the adjustable balance support 12 is a normal lifting support, a second positioning plate 13 is arranged on a lifting plate above the adjustable balance support 12, and the second positioning plate 13 is used for positioning the waste liquid tank 9, the colorimetric tube support 14 and the sample injection bottle support 18; the top of the purifying column adapter 16 is a plane circular, the middle part of the purifying column adapter is provided with a hollow design with a round hole, the diameter of the purifying column adapter 16 is a circular platform which is reduced in sequence from top to bottom, and the purifying column adapter 16 is used for connecting two purifying columns 5 in series.
The working principle is as follows: as shown in fig. 1 to 5, a waste liquid tank 9 is disposed at the bottom of the cylinder 1 and serves to collect waste liquid flowing out from the purification column 5; the colorimetric tube frame 14 is used for placing the colorimetric tube 15, and the positions of the mounting holes on the colorimetric tube frame 14 correspond to the positions of the through holes on the top plate of the cylinder body 1 one by one, so that the purifying columns 5 can be smoothly inserted into the colorimetric tube 15; the sample injection bottle rack 18 is used for placing the sample injection bottles 19, and the positions of the sample injection bottle holes correspond to the positions of the through holes on the top plate of the cylinder body 1 one by one, so that the purifying columns 5 can be smoothly inserted into the sample injection bottles 19; the second positioning plate 13 is arranged on the lifting plate above the adjustable balance support 12, and when the waste liquid tank 9, the colorimetric pipe support 14 and the sample injection bottle support 18 are installed, the waste liquid tank 9, the colorimetric pipe support 14 and the sample injection bottle support 18 can be effectively positioned through the second positioning plate 13, so that the installation by an operator is facilitated, and the working efficiency is improved; connect one-level purification post 5 on the seal cover 4 of cylinder body 1 top, open glass door 7, connect second grade purification post 5 in one-level purification post 5 below through purifying column adapter 16, put waste liquid groove 9 into cylinder body 1 earlier, close glass door 7, with vacuum pump pressure regulation and to purifying post 5 cleaning process. Taking out the waste liquid tank 9, replacing the colorimetric tube frame 14 or the sample bottle frame 18, if necessary, placing the adjustable balance support 12, and carrying out purification operation. The problem of two purification columns establish ties is solved, because some detection methods often can establish ties two purification columns, ordinary solid phase extraction device can't satisfy the experimental requirement, often needs to carry out twice and purifies, both time-consuming and hard technical problem has been solved.
This filtration bottling device can regard as the purification process alone and use: as shown in fig. 1-3, the purifying column 5 is inserted into the through hole of the top plate of the cylinder 1, the glass door 7 is opened, the waste liquid tank 9 is first put into the cylinder 1, the glass door 7 is closed, the cleaning liquid is poured into the purifying column 5, the purifying column 5 is pretreated by using a vacuum pump to adjust the pressure, in the process, the cleaning liquid in the purifying column 5 is sucked out by the suction force of the vacuum pump, and the cleaning liquid flows into the waste liquid tank 9, and in the actual operation process, the vacuum pump is closed when the cleaning liquid is still left at a certain height in the purifying column 5 through manual control. The glass door 7 is opened, the waste liquid tank 9 is taken out, the waste liquid in the waste liquid tank 9 is poured out and is treated in a centralized mode, the colorimetric tube rack 14 or the sample injection bottle rack 18 is replaced, if the height is not enough, the adjustable balance support 12 is placed inside the cylinder body 1, then the colorimetric tube rack 14 or the sample injection bottle rack 18 is placed above the adjustable balance support 12, the height of the colorimetric tube rack 14 or the sample injection bottle rack 18 is adjusted by adjusting the height of the adjustable balance support 12, and the colorimetric tube 15 or the sample injection bottle 19 on the colorimetric tube rack 14 or the sample injection bottle rack 18 is sleeved below the purification column 5 to carry out purification operation.
This filter bottling device can freely adjust the height of color comparison pipe support 14 or advance kind bottle rack 18, changes convenient and fast such as waste liquid groove 9, and each part all can freely be dismantled, convenient washing.
Seal cover 4 is installed to the through-hole department detachable on the roof of cylinder body 1, and purification post 5 divide into first barrel and second barrel, and the diameter of first barrel is greater than the diameter of second barrel, and wherein the second barrel of purification post 5 passes seal cover 4 and extends to inside 1 of cylinder body. The bottom side of cylinder body 1 is equipped with vacuum tube 2, is connected with manometer 3 on the vacuum tube 2, and the one end and the vacuum pump of vacuum tube 2 are connected, and the bottom surface of cylinder body 1 still is equipped with four nylon lower margin 17.
The working principle is as follows: as shown in fig. 6, seal cover 4 can be dismantled, conveniently change or clear seal cover 4, seal cover 4 installs the through-hole department on the roof of cylinder body 1, the thinner barrel of purification post 5 passes seal cover 4, and extend to inside the cylinder body 1, seal cover 4 reliably seals the through-hole of cylinder body 1 and purification post 5, the vacuum pump is at the during operation, can guarantee that the washing liquid in the purification post 5 flows out smoothly, prevent that outside air from getting into in the cylinder body 1 from the through-hole department on the roof of cylinder body 1, influence the use of vacuum pump. The vacuum pump passes through vacuum tube 2 and to evacuation in the cylinder body 1, can make things convenient for operating personnel to observe the pressure value of vacuum pump in real time through observing manometer 3, makes things convenient for operating personnel in time to adjust the pressure of vacuum pump. The cylinder body 1 is placed on the experiment table through the nylon anchor 17, so that the experiment table is prevented from being scratched by the cylinder body 1 or anchors made of other materials; meanwhile, the nylon anchor 17 has small relative friction, and an operator can conveniently adjust the position of the cylinder body 1 according to the experimental requirement.
And sealing rings 6 are arranged around the glass door 7, and the sealing rings 6 are attached to the outer wall of the cylinder body 1.
The working principle is as follows: by arranging the sealing ring 6, the effective sealing of the glass door 7 on the cylinder body 1 can be ensured, and the normal work of the vacuum pump is ensured; in the course of the work, some waste liquid can get into 1 bottom of cylinder body, and when opening glass door 7, the waste liquid will follow the combination department outflow of glass door 7 and cylinder body 1, and then pollutes the laboratory bench, and through setting up glass baffle 8, the waste liquid will be retained in 1 bottom of cylinder body, can not flow 1 outsides of cylinder body, and the effectual waste liquid that prevents flows prevents that the laboratory bench is polluted by the waste liquid.
The bottom of cylinder body 1 is equipped with locating plate 10, and locating plate 10 quantity is three, and locating plate 10 is used for the location to waste liquid groove 9, color comparison pipe support 14, sample introduction bottle frame 18, adjustable balance support 12, has laid nylon board 11 in the inside that locating plate 10 encloses, and check out test set is placed to the top of nylon board 11, and nylon board 11 is used for keeping apart check out test set and cylinder body 1.
The working principle is as follows: through setting up locating plate 10, waste liquid groove 9, the color comparison pipe support 14, advance kind bottle rack 18, when adjustable balance support 12 is placed in cylinder body 1, just can fix a position through locating plate 10, make waste liquid groove 9, the colour comparison tube 15 on the color comparison pipe support 14, advance kind bottle 19 on the kind bottle rack 18 under purifying column 5, guarantee that purifying column 5 can insert in colour comparison tube 15 or advance kind bottle 19, also guaranteed to get into waste liquid groove 9 from the washing liquid that purifying column 5 flows out, prevent that liquid from flowing to the outside, when adjustable balance support 12 adjusts color comparison pipe support 14 and advance kind bottle rack 18 height as required, locating plate 10 fixes a position adjustable balance support 12, and then also guaranteed waste liquid groove 9 above adjustable balance support 12, the location of color comparison 14 and advance kind bottle rack 18. Meanwhile, by arranging the positioning plate 10, the installation of the waste liquid tank 9, the colorimetric tube frame 14, the sample injection bottle frame 18 and the adjustable balance support 12 by operators can be facilitated, the adjusting time is shortened, and the working efficiency is improved.
It should be understood that the above examples are only for clarity of illustration and are not intended to limit the embodiments. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And obvious variations or modifications therefrom are within the scope of the invention.

Claims (6)

1. A filter bottle filling apparatus, comprising: the detection device comprises a cylinder body (1), wherein detection equipment is placed in the cylinder body (1), a plurality of through holes are formed in a top plate of the cylinder body (1), the through holes are used for inserting purification columns (5), a glass door (7) is rotatably connected in front of the cylinder body (1), a glass baffle (8) is arranged at the front end of the cylinder body (1), and the glass baffle (8) prevents organic waste liquid in the cylinder body (1) from flowing out;
the detection apparatus includes: a waste liquid tank (9), a colorimetric tube frame (14), a sample injection bottle frame (18), an adjustable balance bracket (12) and a purifying column adapter (16); the waste liquid tank (9) is used for collecting waste liquid flowing out of the purifying column (5); the colorimetric tube frame (14) is an upper three-layer plate, a middle three-layer plate and a lower three-layer plate, the upper three-layer plate, the middle three-layer plate and the lower three-layer plate are fixed by fixing columns, mounting holes are formed in the upper layer plate and the middle layer plate and used for placing colorimetric tubes (15), the positions of the mounting holes correspond to the positions of through holes in a top plate of the cylinder body (1) one by one, and the lower layer plate is a flat plate; the sample injection bottle rack (18) is a fixed plate with the thickness of 1cm, a plurality of sample injection bottle holes are formed in the sample injection bottle rack and used for placing sample injection bottles (19), and the positions of the sample injection bottle holes correspond to the positions of through holes in a top plate of the cylinder body (1) one by one; the adjustable balance support (12) is a normal lifting support and is used for adjusting the height of the waste liquid tank (9), the colorimetric tube support (14) and the sample injection bottle support (18); the purifying column adapter (16) is used for connecting two purifying columns (5) in series.
2. A filtering bottle filling device according to claim 1, wherein a sealing sleeve (4) is detachably mounted at the through hole on the top plate of the cylinder body (1), the purifying column (5) is divided into a first cylinder and a second cylinder, the diameter of the first cylinder is larger than that of the second cylinder, and the second cylinder of the purifying column (5) passes through the sealing sleeve (4) and extends to the inside of the cylinder body (1).
3. The filtering and bottling device according to claim 1, wherein a vacuum tube (2) is arranged on the bottom side of the cylinder body (1), a pressure gauge (3) is connected to the vacuum tube (2), one end of the vacuum tube (2) is connected to a vacuum pump, and four nylon anchor feet (17) are arranged on the bottom surface of the cylinder body (1).
4. A filtering bottle filling device according to claim 1, wherein a sealing ring (6) is arranged around the glass door (7), and the sealing ring (6) is attached to the outer wall of the cylinder body (1).
5. The filtering and bottling device according to claim 1, wherein the bottom of the cylinder body (1) is provided with three positioning plates (10), the positioning plates (10) are used for positioning the waste liquid tank (9), the colorimetric tube frame (14), the sample feeding bottle frame (18) and the adjustable balance support (12), a nylon plate (11) is laid in the inner part surrounded by the positioning plates (10), a detection device is arranged above the nylon plate (11), and the nylon plate (11) is used for isolating the detection device from the cylinder body (1).
6. A bottle filter filling device as claimed in claim 1, wherein a second positioning plate (13) is arranged on the lifting plate above the adjustable balance support (12), and the second positioning plate (13) is used for positioning the waste liquid tank (9), the colorimetric tube stand (14) and the sample bottle stand (18);
the top of the purifying column adapter (16) is in a plane circular shape, the middle of the purifying column adapter is provided with a hollow design with a round hole, the diameter of the purifying column adapter is reduced from top to bottom in sequence, and the reduced circular platform can be matched with purifying columns (5) of different models.
CN201921295374.5U 2019-08-12 2019-08-12 Filtering bottle filling device Active CN210495325U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201921295374.5U CN210495325U (en) 2019-08-12 2019-08-12 Filtering bottle filling device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921295374.5U CN210495325U (en) 2019-08-12 2019-08-12 Filtering bottle filling device

Publications (1)

Publication Number Publication Date
CN210495325U true CN210495325U (en) 2020-05-12

Family

ID=70588709

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201921295374.5U Active CN210495325U (en) 2019-08-12 2019-08-12 Filtering bottle filling device

Country Status (1)

Country Link
CN (1) CN210495325U (en)

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