CN210409547U - Solvent removal system after biological reagent synthesis - Google Patents
Solvent removal system after biological reagent synthesis Download PDFInfo
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- CN210409547U CN210409547U CN201921167563.4U CN201921167563U CN210409547U CN 210409547 U CN210409547 U CN 210409547U CN 201921167563 U CN201921167563 U CN 201921167563U CN 210409547 U CN210409547 U CN 210409547U
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Abstract
The utility model discloses a synthetic back solvent of biological reagent gets rid of system, concretely relates to biological reagent processing field, including the water bath case, the top fixedly connected with apron of water bath case, and the inside fixed mounting of water bath case has the processing case, the inside rotation of processing case is connected with the (mixing) shaft, and the fixed inserting in top of handling the case is equipped with the feed liquor pipe, fixed mounting has first liquid solenoid valve on the feed liquor pipe, and the one end fixed connection of feed liquor pipe is in the play liquid end of first water pump, the feed liquor end of first water pump passes through the bottom of body fixed connection at the stoste case, the bottom fixedly connected with discharging pipe of processing case, the bottom fixed connection of water bath case is run through in the inside of collecting tank in the bottom of discharging pipe. The utility model discloses be convenient for to the water-bath heating of handling incasement portion stoste, and the surface of handling the case is heated evenly, and the solvent volatilizees effectually, and the water after the heating can carry out the circulation heating and use, has realized the self-cleaning function to handling the case simultaneously.
Description
Technical Field
The utility model relates to a biological reagent processing field, more specifically say, the utility model relates to a synthetic back solvent removal system of biological reagent.
Background
5-bromo-4-chloro-3-indoleacetic acid ester is a chemical substance, the molecular formula is C10H7BrClNO2, it is a white crystalline powder, mainly used in cell lipase indicator, used as substrate of esterase in histochemistry, in the manufacturing process of medicament, some ingredients in the prepared product are difficult to dissolve in water, can't be well dissolved in aqueous solution, so organic solvent is often used to dissolve these ingredients in the production process, but organic solvent belongs to harmful substance to human body, there is toxicity or carcinogenesis, therefore must be effectively and thoroughly removed in the subsequent process of medicament manufacturing to ensure that the product can be safely used, and the toxicity or carcinogenesis of the residual organic solvent in medicament has been increasingly paid attention to, therefore it is necessary to design a system for removing solvent after biological agent synthesis.
The existing method for heating the product to remove the residual organic solvent in the product generally adopts a mode of heating the product to volatilize the organic solvent in the product, but the surface of the treatment box cannot be heated uniformly better in the heating process, and the inside of the treatment box is not convenient to clean.
SUMMERY OF THE UTILITY MODEL
In order to overcome the above-mentioned defect of prior art, the embodiment of the utility model provides a system is got rid of to synthetic back solvent of biological reagent, is convenient for to the water-bath heating who handles incasement portion stoste, and the surface heating of handling the case is even, and the solvent volatilizees effectually, and the water after the heating can carry out the circulation heating and use, has realized the self-cleaning function to handling the case simultaneously.
In order to achieve the above object, the utility model provides a following technical scheme: a system for removing solvent after synthesis of biological reagent comprises a water bath tank, wherein a cover plate is fixedly connected to the top end of the water bath tank, a treatment tank is fixedly arranged inside the water bath tank, a stirring shaft is rotatably connected inside the treatment tank, a liquid inlet pipe is fixedly inserted into the top of the treatment tank, a first liquid electromagnetic valve is fixedly mounted on the liquid inlet pipe, one end of the liquid inlet pipe is fixedly connected to the liquid outlet end of a first water pump, the liquid inlet end of the first water pump is fixedly connected to the bottom of a stock solution tank through a pipe body, a discharging pipe is fixedly connected to the bottom of the treatment tank, the bottom of the discharging pipe penetrates through the bottom of the water bath tank and is fixedly connected to the inside of the liquid collecting tank, a second liquid electromagnetic valve is fixedly mounted at the position below the water bath tank on the discharging pipe, a drain pipe is fixedly connected to the outer wall of the bottom of the water bath tank, and a, one end part of the drain pipe is inserted in the water bath tank, the other end of the drain pipe is fixedly connected with the top of the water tank, the water tank is positioned on one side below the water bath tank, an electric heating pipe is fixedly arranged inside the water tank, the top of the water bath tank is fixedly connected with a water inlet pipe, one end part of the water inlet pipe is positioned inside the water bath tank and is fixedly provided with a ball float valve, and the other end of the water inlet pipe is fixedly connected with a three-way pipe, one port of the three-way pipe is fixedly connected with a water delivery pipe, one end of the water delivery pipe is fixedly connected with the water outlet end of the second water pump, the water inlet end of the second water pump is fixedly connected with a water pumping pipe, the bottom end of the water pumping pipe is fixedly inserted in the water tank, the other port of the three-way pipe is fixedly connected with a cleaning pipe, the bottom end of the cleaning pipe penetrates through the inner part of the cover plate and is inserted into the top of the treatment box, and a fourth liquid electromagnetic valve is fixedly installed between the three-way pipe and the cover plate on the cleaning pipe.
In a preferred embodiment, the top end of the stirring shaft is connected with a motor at a position above the treatment box, a gasket is welded on the outer wall of the motor, and the gasket is connected with the top end of the treatment box through a bolt.
In a preferred embodiment, the bottom inner wall of the water bath tank is provided with a sealing ring at a position outside the tapping pipe.
In a preferred embodiment, a sealing ring is arranged at the external connection position of the inner wall of the water tank and the water pumping pipe, and a water filling port is arranged at the top of the water tank.
In a preferred embodiment, the processing box is fixedly connected with a volatilization exhaust pipe at the top, a through hole is formed in the position, corresponding to the bottom of the volatilization exhaust pipe, at the top of the processing box, the inside of the volatilization exhaust pipe is communicated with the inside of the processing box through the through hole, one end of the volatilization exhaust pipe penetrates through the inside of the cover plate, and the volatilization exhaust pipe is of an L-shaped structure.
In a preferred embodiment, the inner wall of the water bath box is provided with a heat insulation layer which is an asbestos member, and the front surface of the water bath box is provided with a control switch.
In a preferred embodiment, the cover plate is provided with a limiting hole at a position corresponding to the outside of the liquid inlet pipe, the volatilization exhaust pipe and the cleaning pipe.
In a preferred embodiment, a sealing ring is arranged at the joint of the drain pipe and the inner wall of the water bath box.
The utility model discloses a technological effect and advantage:
1. the utility model discloses during the use, through starting the second water pump, be convenient for take the inside hot water of water tank out, and get into the inside of water bath through the inlet tube and carry out heat treatment to handling the case, and control water level height through the floating ball valve, realized the water bath heating to handling the incasement portion stoste, and the temperature of water bath heating is gentler, and the surface of handling the case is heated evenly, the solvent volatilizees effectually, the water after the heating is in order to avoid cooling, through the bottom outer wall fixedly connected with drain pipe at the water bath, fixedly mounted with the third liquid solenoid valve on the drain pipe, and a tip of drain pipe inserts and establishes in the inside of water bath, the other end fixed connection of drain pipe is at the top of water tank, during the use, the water in the water bath flows into the inside of water tank again through the drain pipe and heats, the cyclic;
2. the utility model discloses an another port fixedly connected with scavenge pipe at the three-way pipe, the inside of establishing at the processing case is inserted to the bottom of scavenge pipe, and lie in fixed mounting between three-way pipe and the apron on the scavenge pipe and have fourth liquid solenoid valve, when needs wash the inside of processing case, through closing third liquid solenoid valve, the water level of water bath incasement portion is reaching the take in water through the ball-cock assembly automatic stop after the take to a take the altitude, then, open fourth liquid solenoid valve, second water pump and drive (mixing) shaft pivoted motor, be convenient for take the inside water of water tank out arrange to the inside of processing case, and rotate through the (mixing) shaft and realize the cleaning to the processing incasement portion, it can to open second liquid solenoid valve after the washing is accomplished waste water discharge, the self-cleaning function to the processing case has been realized.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a front view of the present invention.
Fig. 3 is an enlarged view of a portion a in fig. 1 according to the present invention.
Fig. 4 is an enlarged view of a portion B of fig. 1 according to the present invention.
Fig. 5 is a schematic structural diagram of the middle three-way pipe of the present invention.
The reference signs are: 1 water bath case, 2 apron, 3 treatment casees, 4 (mixing) shafts, 5 feed liquor pipes, 6 first liquid solenoid valves, 7 first water pump, 8 former liquid case, 9 discharging pipes, 10 second liquid solenoid valves, 11 header tanks, 12 drain pipes, 13 third liquid solenoid valves, 14 water tanks, 15 electric heating pipes, 16 inlet tubes, 17 ball-cock valves, 18 tee pipes, 19 raceway, 20 second water pump, 21 drinking-water pipes, 22 volatile blast pipe, 23 scavenge pipes, 24 fourth liquid solenoid valves, 25 control switch.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The utility model provides a system for removing solvent after synthesis of biological reagent, which comprises a water bath tank 1, wherein the top end of the water bath tank 1 is fixedly connected with a cover plate 2, the inside of the water bath tank 1 is fixedly provided with a treatment tank 3, the inside of the treatment tank 3 is rotatably connected with a stirring shaft 4, the top end of the stirring shaft 4 is positioned above the treatment tank 3 and is connected with a motor, the outer wall of the motor is welded with a gasket, the gasket is connected with the top end of the treatment tank 3 through a bolt, the top of the treatment tank 3 is fixedly inserted with a liquid inlet pipe 5, the liquid inlet pipe 5 is fixedly provided with a first liquid electromagnetic valve 6, one end of the liquid inlet pipe 5 is fixedly connected with the liquid outlet end of a first water pump 7, the liquid inlet end of the first water pump 7 is fixedly connected with the bottom of a raw liquid tank 8 through a pipe body, the bottom of the treatment tank 3 is fixedly connected with a discharging pipe 9, the bottom end of the discharging pipe 9 penetrates, a second liquid solenoid valve 10 is fixedly mounted on the discharging pipe 9 and located below the water bath tank 1, a sealing ring is arranged on the inner wall of the bottom of the water bath tank 1 and located at the outer position of the discharging pipe 9, a discharging pipe 12 is fixedly connected to the outer wall of the bottom of the water bath tank 1, a third liquid solenoid valve 13 is fixedly mounted on the discharging pipe 12, one end of the discharging pipe 12 is inserted into the water bath tank 1, the other end of the discharging pipe 12 is fixedly connected to the top of the water tank 14, the water tank 14 is located on one side below the water bath tank 1, an electric heating pipe 15 is fixedly mounted inside the water tank 14, a water inlet pipe 16 is fixedly connected to the top of the water bath tank 1, one end of the water inlet pipe 16 is located inside the water bath tank 1 and fixedly mounted with a ball float valve 17, a three-way pipe 18 is fixedly connected to the other end of the water inlet pipe 16, and a, the one end fixed connection of raceway 19 is in the play water end of second water pump 20, the end fixedly connected with drinking-water pipe 21 of intaking of second water pump 20, the bottom mounting of drinking-water pipe 21 inserts and establishes the inside of water tank 14, the inner wall of water tank 14 is provided with the sealing washer with the external junction of drinking-water pipe 21, and the top of water tank 14 is provided with the water filling port, the top fixedly connected with who handles case 3 volatilizees blast pipe 22, and the top that handles case 3 is provided with the through-hole corresponding to the bottom position department that volatilizees blast pipe 22, volatilize through-hole intercommunication between the inside of blast pipe 22 and the inside of handling case 3, the inside of apron 2 is passed to the one end of volatilizing blast pipe 22, and volatilizees blast pipe 22 and be the L shape structure, the inner wall of water bath case 1 is provided with the insulating layer, and the insulating layer is the component of an asbestos material, the front, and a sealing ring is arranged at the joint of the drain pipe 12 and the inner wall of the water bath tank 1.
As shown in fig. 1 to 5, the specific embodiment is as follows: when in use, the first water pump 7 is started to pump out the stock solution in the stock solution tank 8 and arrange the stock solution in the treatment tank 3, the interior of the treatment tank 3 is rotatably connected with the stirring shaft 4, the top end of the stirring shaft 4 is positioned above the treatment tank 3 and is connected with the motor, the outer wall of the motor is welded with the gasket, the gasket is connected with the top end of the treatment tank 3 through the bolt, the motor is convenient to install and fix, further, when in use, the stirring shaft 4 is driven by the starting motor to rotate to stir the stock solution, the volatilization speed is accelerated, the treatment tank 3 is fixedly arranged in the water bath tank 1, the bottom of the treatment tank 3 is fixedly connected with the discharge pipe 9, the bottom end of the discharge pipe 9 penetrates through the bottom of the water bath tank 1 and is fixedly connected in the collection tank 11, and the second liquid electromagnetic valve 10 is fixedly arranged on the discharge pipe 9 at the position below the, a sealing ring is arranged at the position, located outside the discharge pipe 9, of the inner wall of the bottom of the water bath tank 1, so that processed residual materials can be conveniently collected, a water inlet pipe 16 is fixedly connected to the top of the water bath tank 1, a ball float valve 17 is fixedly arranged at one end of the water inlet pipe 16, so that water injection into the water bath tank 1 can be automatically stopped when the water level in the water bath tank 1 is too high, a three-way pipe 18 is fixedly connected to the other end of the water inlet pipe 16, a water delivery pipe 19 is fixedly connected to one end of the three-way pipe 18, one end of the water delivery pipe 19 is fixedly connected to the water outlet end of a second water pump 20, a water suction pipe 21 is fixedly connected to the water inlet end of the second water pump 20, the bottom end of the water suction pipe 21 is fixedly inserted into the water tank 14, a sealing ring is arranged at the position, located outside the inner wall of the water tank 14 and the water suction pipe, when in use, the second water pump 20 is started, so that hot water in the water tank 14 is conveniently pumped out and enters the water bath tank 1 through the water inlet pipe 16 to heat the treatment tank 3, the water level height is controlled by the float valve 17, the water bath heating of the stock solution in the treatment tank 3 is realized, the temperature of water bath heating is milder, the surface of the treatment box 3 is heated uniformly, the solvent volatilization effect is good, the heated water is prevented from being cooled, the outer wall of the bottom of the water bath tank 1 is fixedly connected with a drain pipe 12, a third liquid electromagnetic valve 13 is fixedly arranged on the drain pipe 12, one end part of the water discharge pipe 12 is inserted in the water bath tank 1, the other end of the water discharge pipe 12 is fixedly connected with the top part of the water tank 14, when in use, the water in the water bath tank 1 flows into the water tank 14 again through the water discharge pipe 12 to be heated, and the water is recycled.
The other end of the three-way pipe 18 is fixedly connected with a cleaning pipe 23, the bottom end of the cleaning pipe 23 penetrates through the inside of the cover plate 2 and is inserted into the top of the treatment box 3, a fourth liquid electromagnetic valve 24 is fixedly mounted between the three-way pipe 18 and the cover plate 2 on the cleaning pipe 23, and limiting holes are formed in the positions, corresponding to the outside of the liquid inlet pipe 5, the volatilization exhaust pipe 22 and the cleaning pipe 23, in the cover plate 2.
As shown in fig. 1-2 and fig. 4-5, the specific embodiment is as follows: a cleaning pipe 23 is fixedly connected with the other port of the three-way pipe 18, the bottom end of the cleaning pipe 23 penetrates through the inside of the cover plate 2 and is inserted into the top of the treatment box 3, a fourth liquid electromagnetic valve 24 is fixedly installed between the three-way pipe 18 and the cover plate 2 on the cleaning pipe 23, a limiting hole is arranged in the cover plate 2 corresponding to the position outside the cleaning pipe 23, when the inside of the treatment box 3 needs to be cleaned, water is automatically stopped to enter through a ball float valve after the water level in the water bath box 1 reaches a certain height by closing the third liquid electromagnetic valve 13, then the fourth liquid electromagnetic valve 24, the second water pump 20 and a motor driving the stirring shaft 4 to rotate are started, so that water in the water tank 14 is conveniently pumped out and discharged into the inside of the treatment box 3, the cleaning treatment of the inside of the treatment box 3 is realized through the rotation of the stirring shaft 4, and the second liquid electromagnetic valve 10 is opened to discharge waste water, the cleaning treatment can be carried out for a plurality of times according to the requirement until the cleaning is completely carried out.
The utility model discloses the theory of operation:
referring to the attached drawings 1-5 of the specification, when in use, the second water pump 20 is started to conveniently pump out hot water in the water tank 14, the hot water enters the inside of the water bath tank 1 through the water inlet pipe 16 to heat the treatment tank 3, the water level height is controlled through the ball float valve 17, the water bath heating of the stock solution in the treatment tank 3 is realized, the water bath heating temperature is milder, the surface of the treatment tank 3 is uniformly heated, the solvent volatilization effect is good, the heated water is prevented from being cooled, a drain pipe 12 is fixedly connected to the outer wall of the bottom of the water bath tank 1, a third liquid electromagnetic valve 13 is fixedly installed on the drain pipe 12, one end part of the drain pipe 12 is inserted in the water bath tank 1, the other end of the drain pipe 12 is fixedly connected to the top of the water tank 14, when in use, the water in the water bath tank 1 flows into the inside of the water tank 14 again through, the water is recycled;
further, referring to the attached drawings 1-2 and 4-5 of the specification, a cleaning pipe 23 is fixedly connected to the other port of the three-way pipe 18, the bottom end of the cleaning pipe 23 is inserted into the inside of the treatment tank 3, and a fourth liquid solenoid valve 24 is fixedly installed on the cleaning pipe 23 between the three-way pipe 18 and the cover plate 2, when the inside of the treatment tank 3 needs to be cleaned, the water inlet is automatically stopped by closing the third liquid solenoid valve 13 after the water level inside the water bath tank 1 reaches a certain height through a ball float valve, then the fourth liquid solenoid valve 24, the second water pump 20 and a motor driving the stirring shaft 4 to rotate are opened, so that the water inside the water tank 14 is conveniently pumped out and discharged into the inside of the treatment tank 3, the cleaning treatment inside the treatment tank 3 is realized through the rotation of the stirring shaft 4, the second liquid solenoid valve 10 is opened after the cleaning is completed to discharge the wastewater, and the cleaning treatment can be performed for multiple times as required, until the cleaning is complete.
And finally: the above description is only for the preferred embodiment of the present invention and should not be taken as limiting the invention, and any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (8)
1. A post-biological reagent synthesis solvent removal system comprises a water bath (1), and is characterized in that: the top fixedly connected with apron (2) of water bath (1), and the inside fixed mounting of water bath (1) has and handles case (3), the inside of handling case (3) is rotated and is connected with (mixing) shaft (4), and the top of handling case (3) is fixed to be inserted and is equipped with feed liquor pipe (5), fixed mounting has first liquid solenoid valve (6) on feed liquor pipe (5), and the play liquid end of one end fixed connection in first water pump (7) of feed liquor pipe (5), the feed liquor end of first water pump (7) is through body fixed connection in the bottom of stoste case (8), the bottom fixedly connected with discharging pipe (9) of handling case (3), the bottom fixed connection of water bath (1) is run through in the inside of collection liquid case (11) in the bottom of discharging pipe (9), and lies in the below position department fixed mounting of water bath (1) on discharging pipe (9) and has second liquid solenoid valve (10), the water bath device is characterized in that a drain pipe (12) is fixedly connected to the outer wall of the bottom of the water bath box (1), a third liquid electromagnetic valve (13) is fixedly mounted on the drain pipe (12), one end of the drain pipe (12) is inserted into the water bath box (1), the other end of the drain pipe (12) is fixedly connected to the top of a water tank (14), the water tank (14) is located on one side below the water bath box (1), an electric heating pipe (15) is fixedly mounted inside the water tank (14), a water inlet pipe (16) is fixedly connected to the top of the water bath box (1), one end of the water inlet pipe (16) is located inside the water bath box (1) and is fixedly mounted with a ball float valve (17), a three-way pipe (18) is fixedly connected to the other end of the water inlet pipe (16), a water pipe (19) is fixedly connected to one port of the three-way pipe (18), and one end of the water pipe (19), the water inlet end of the second water pump (20) is fixedly connected with a water pumping pipe (21), the bottom end of the water pumping pipe (21) is fixedly inserted into the water tank (14), the other port of the three-way pipe (18) is fixedly connected with a cleaning pipe (23), the bottom end of the cleaning pipe (23) penetrates through the inner part of the cover plate (2) and is inserted into the top of the treatment tank (3), and a fourth liquid electromagnetic valve (24) is fixedly mounted between the three-way pipe (18) and the cover plate (2) on the cleaning pipe (23).
2. The post-synthesis solvent removal system of claim 1, wherein: the top of (mixing) shaft (4) is located the top position department of handling case (3) and is connected with the motor, and the outer wall welding of motor has the gasket, passes through bolted connection between gasket and the top of handling case (3).
3. The post-synthesis solvent removal system of claim 1, wherein: and a sealing ring is arranged on the outer position of the inner wall of the bottom of the water bath tank (1) on the discharge pipe (9).
4. The post-synthesis solvent removal system of claim 1, wherein: the sealing ring is arranged at the external connection position of the inner wall of the water tank (14) and the water pumping pipe (21), and a water filling port is arranged at the top of the water tank (14).
5. The post-synthesis solvent removal system of claim 1, wherein: handle the top fixedly connected with of case (3) and volatilize blast pipe (22), and the bottom position department that the top of handling case (3) corresponds volatilization blast pipe (22) is provided with the through-hole, through the through-hole intercommunication between the inside of volatilizing blast pipe (22) and the inside of handling case (3), the inside of apron (2) is passed to the one end of volatilizing blast pipe (22), and volatilizees blast pipe (22) and be L shape structure.
6. The post-synthesis solvent removal system of claim 1, wherein: the inner wall of the water bath box (1) is provided with a heat insulation layer which is a component made of asbestos, and the front surface of the water bath box (1) is provided with a control switch (25).
7. The post-synthesis solvent removal system of claim 1, wherein: the inside of apron (2) corresponds the outside position department of feed liquor pipe (5), exhaust pipe (22) and scavenge pipe (23) that volatilizees and all is provided with spacing hole.
8. The post-synthesis solvent removal system of claim 1, wherein: and a sealing ring is arranged at the joint of the drain pipe (12) and the inner wall of the water bath tank (1).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201921167563.4U CN210409547U (en) | 2019-07-24 | 2019-07-24 | Solvent removal system after biological reagent synthesis |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201921167563.4U CN210409547U (en) | 2019-07-24 | 2019-07-24 | Solvent removal system after biological reagent synthesis |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112590053A (en) * | 2020-12-29 | 2021-04-02 | 宁波艾克姆新材料有限公司 | Pre-dispersion master batch production coloring machine based on thermal cycle utilization |
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2019
- 2019-07-24 CN CN201921167563.4U patent/CN210409547U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112590053A (en) * | 2020-12-29 | 2021-04-02 | 宁波艾克姆新材料有限公司 | Pre-dispersion master batch production coloring machine based on thermal cycle utilization |
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