CN210332665U

CN210332665U - Synthesizer of paclobutrazol product

Info

Publication number: CN210332665U
Application number: CN201920961854.4U
Authority: CN
Inventors: 崔利飞; 田勤俭; 尹占杰
Original assignee: Anyang Ruipu Agrochemical Co ltd
Current assignee: Anyang Ruipu Agrochemical Co ltd
Priority date: 2019-06-25
Filing date: 2019-06-25
Publication date: 2020-04-17
Anticipated expiration: 2029-06-25

Abstract

The utility model discloses a synthesis device of paclobutrazol products, which comprises a barrel body, wherein the barrel body is connected with a support ring, the support ring is connected with support legs, the support legs are provided with pad feet, the left side and the right side of the barrel body are respectively provided with a feed inlet, the top of the barrel body is connected with a motor, the motor is connected with a support column, the support column is connected with the barrel body, a heater is arranged inside the barrel body, the heater is provided with a heating pipe, the heater is connected with a synthesis chamber, a filter plate is arranged inside the synthesis chamber, the filter plate is provided with a plurality of filter holes, the top of the barrel body is connected with a mounting block, the power output end of the motor is connected with a rotating main shaft, the rotating main shaft is provided with a main gear, the main gear is arranged on the, the two ends of the rotary auxiliary shaft are connected with mounting seats, and bearings are arranged in the mounting seats.

Description

Synthesizer of paclobutrazol product

Technical Field

The utility model belongs to the technical field of synthesizer, concretely relates to synthesizer of paclobutrazol product.

Background

The preparation method of the paclobutrazol is reported in S1 of 1987 by using α -chloroppinacolone as a starting raw material, firstly reacting with 1,2, 4-triazole to generate a compound-oxazolone represented by a formula (II), then reacting with p-chlorobenzyl to generate a compound-chlorzolone represented by a formula (III), and finally reducing with potassium borohydride to generate the paclobutrazol.

SUMMERY OF THE UTILITY MODEL

To the problem that the above-mentioned background art provided, the utility model aims at: aiming at providing a synthesis device of a paclobutrazol product. In order to realize the technical purpose, the utility model discloses a technical scheme as follows:

a synthesizer of paclobutrazol products comprises a cylinder body, wherein the cylinder body is connected with a support ring, the support ring is connected with support legs, the support legs are provided with pad feet, the left side and the right side of the cylinder body are respectively provided with a feed inlet, the top of the cylinder body is connected with a motor, the motor is connected with a support column, the support column is connected with the cylinder body, a heater is arranged inside the cylinder body, the heater is provided with a heating pipe, the heater is connected with a synthesis chamber, a filter plate is arranged inside the synthesis chamber, the filter plate is provided with a plurality of filter holes, the top of the cylinder body is connected with an installation block, the power output end of the motor is connected with a rotating main shaft, the rotating main shaft is provided with a main gear, the main gear is arranged on the installation block, two sides of the main gear are respectively provided, the improved rotary stirring device is characterized in that a bearing is arranged in the mounting seat, the rotary auxiliary shaft is connected with an upper rotary stirring block and a lower rotary stirring block, the upper rotary stirring block and the two short lower rotary stirring blocks are arranged alternately, the upper rotary stirring block comprises four upper rotary stirring blades, the lower rotary stirring block comprises four lower rotary stirring blades, and a discharge hole is formed in the bottom of the barrel body.

Further limiting, the filtering holes are inverted cone-shaped holes, and are mixed and synthesized in a layered mode, so that excessive material discharging is prevented, and uniform mixing cannot be achieved.

Further limiting, the specification and model of the main gear and the auxiliary gears are the same, the main gear is driven to rotate by the motor, and the main gear drives the two auxiliary gears to rotate, so that the two rotary auxiliary shafts rotate.

Further limit, the included angle between the upper rotating stirring blade (141) and the horizontal plane is 45 degrees, the included angle between the lower rotating stirring blade (151) and the horizontal plane is 55 degrees, and materials can be stirred more smoothly and uniformly during stirring.

The utility model has the advantages of it is following:

1. the heating pipe is arranged, so that the raw materials are heated in the stirring process, and the finally synthesized materials are better;

2. the utility model discloses a set up the filter, when the feed inlet of both sides, through stirring the back for the first time, semisynthetic material flows into the synthetic chamber in below from the filtration pore and is stirring the synthesis, makes the mixture that two kinds of different materials can be abundant.

Drawings

The present invention can be further illustrated by the non-limiting examples given in the accompanying drawings;

FIG. 1 is a schematic diagram of a device for synthesizing a paclobutrazol product according to an embodiment of the present invention;

FIG. 2 is a schematic sectional view of a device for synthesizing a paclobutrazol product according to an embodiment of the present invention;

FIG. 3 is a schematic structural view of a stirring device of a device for synthesizing a paclobutrazol product according to an embodiment of the present invention;

FIG. 4 is an enlarged schematic view of a synthesis apparatus for a paclobutrazol product according to an embodiment of the present invention at A;

the main element symbols are as follows:

the device comprises a cylinder 1, a support ring 2, support legs 3, pad legs 4, a feed inlet 5, a motor 6, support columns 7, a heater 8, a heating pipe 9, a synthesis chamber 10, a filter plate 11, filter holes 12, a mounting block 13, a rotating main shaft 14, a main gear 15, a pinion gear 16, a rotating auxiliary shaft 17, a mounting seat 18, an upper rotating stirring block 19, an upper rotating stirring blade 191, a lower rotating stirring block 20, a lower rotating stirring blade 201 and a discharge port 21.

Detailed Description

In order to make the present invention better understood by those skilled in the art, the technical solutions of the present invention are further described below with reference to the accompanying drawings and examples.

As shown in figures 1-4, the utility model discloses a synthesizer of paclobutrazol products, a cylinder 1 is connected with a support ring 2, the support ring 2 is connected with a support foot 3, the support foot 3 is provided with a pad foot 4, the left and right sides of the cylinder 1 are respectively provided with a feed inlet 5, the top of the cylinder 1 is connected with a motor 6, the motor 6 is connected with a support column 7, the support column 7 is connected with the cylinder 1, the cylinder 1 is internally provided with a heater 8, the heater 8 is provided with a heating pipe 9, the heater 8 is connected with a synthesis chamber 10, the synthesis chamber 10 is internally provided with a filter plate 11, the filter plate 11 is provided with a plurality of filter holes 12, the top of the cylinder 1 is connected with a mounting block 13, the power output end of the motor 6 is connected with a rotating main shaft 14, the rotating main shaft 14 is provided with a main gear 15, the main, the two ends of the rotary auxiliary shaft 17 are connected with mounting seats 18, bearings are arranged in the mounting seats 18, the rotary auxiliary shaft 17 is connected with an upper rotary stirring block 19 and a lower rotary stirring block 20, the upper rotary stirring block 19 and the two short lower rotary stirring blocks 20 are arranged alternately, the upper rotary stirring block 19 comprises four upper rotary stirring blades 191, the lower rotary stirring block 20 comprises four lower rotary stirring blades 201, and a discharge port 21 is formed in the bottom of the barrel 1.

When in use, two different raw materials to be synthesized are respectively poured into the synthesis chamber from the two feed inlets, the synthesis chamber is divided into an upper synthesis chamber and a lower synthesis chamber by the filter plate 11, the motor 6 is started, the main rotating shaft 14 rotates to drive the main gear 15 to rotate, the two sides of the gear 15 are provided with the pinion gears 16 with the same teeth, the pinion gears 16 are rotated by the main gear 15, the pinion gears 16 are connected with the auxiliary rotating shaft 17, the auxiliary rotating shaft 17 is provided with the stirring block 20, the lower stirring block 19 pushes the materials downwards during stirring, the upper stirring block 20 pushes the materials at the bottom upwards, so that the materials are stirred more fully in the barrel body 1, the heating pipe 9 starts heating while stirring, and after stirring in the upper synthesis chamber, the raw materials are mixed and flow from the filtration pores 12 into the lower synthesis chamber, and the raw materials are sufficiently stirred and mixed in the lower synthesis chamber, and after sufficient reaction synthesis, the synthesized materials are taken out from the discharge port 21.

Preferably, the filtering holes 12 are inverted cone-shaped holes, and are formed by layered stirring synthesis, so that excessive discharging is prevented, and uniform stirring cannot be realized. In fact, the structure of the filtering holes 12 can also be considered as the case may be.

Preferably, the main gear 15 and the auxiliary gear 16 have the same specification and model, and the main gear is driven by a motor to rotate and drives the two auxiliary gears to rotate, so that the two rotary auxiliary shafts rotate. In fact, the configuration and type of the primary gear 15 and the secondary gear 16 may also be considered as the case may be.

Preferably, the included angle between the upper rotating stirring blade 141 and the horizontal plane is 45 degrees, the included angle between the lower rotating stirring blade 151 and the horizontal plane is 55 degrees, and the materials can be stirred more smoothly and uniformly during stirring. In fact, the structure of the upper rotary stirring vane 141 and the lower rotary stirring vane 151 may be considered as the case may be.

The above embodiments are merely illustrative of the principles and effects of the present invention, and are not to be construed as limiting the invention. Modifications and variations can be made to the above-described embodiments by those skilled in the art without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which may be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.

Claims

1. A synthesizer of paclobutrazol products comprises a cylinder body (1), and is characterized in that: the device is characterized in that the barrel (1) is connected with a support ring (2), the support ring (2) is connected with support legs (3), the support legs (3) are provided with pad feet (4), the left side and the right side of the barrel (1) are respectively provided with a feed inlet (5), the top of the barrel (1) is connected with a motor (6), the motor (6) is connected with a support column (7), the support column (7) is connected with the barrel (1), a heater (8) is arranged in the barrel (1), the heater (8) is provided with a heating pipe (9), the heater (8) is connected with a synthesis chamber (10), a filter plate (11) is arranged in the synthesis chamber (10), the filter plate (11) is provided with a plurality of filter holes (12), the top of the barrel (1) is connected with a mounting block (13), and the power output end of, rotatory main shaft (14) are equipped with master gear (15), master gear (15) are established on installation piece (13), master gear (15) both sides respectively are equipped with pinion (16) of a looks meshing, rotatory countershaft (17) is connected in pinion (16), rotatory countershaft (17) both ends all are connected with mount pad (18), be equipped with the bearing in mount pad (18), rotatory countershaft (17) are connected with top spin stirring piece (19) and underspin stirring piece (20), top spin stirring piece (19) and two short underspin stirring piece (20) alternate settings, top spin stirring piece (19) are including four upper spin stirring leaf (191), underspin stirring piece (20) are including four underspin stirring leaf (201), barrel (1) bottom is equipped with discharge gate (21).

2. The apparatus for synthesizing a paclobutrazol product according to claim 1, wherein: the filtering holes (12) are inverted cone-shaped holes.

3. The apparatus for synthesizing a paclobutrazol product according to claim 2, wherein: the specification and model of the main gear (15) and the specification and model of the auxiliary gear (16) are the same.

4. A synthesis plant for paclobutrazol products according to claim 3, wherein: the included angle between the upper rotating stirring blades (191) and the horizontal plane is 45 degrees, and the included angle between the lower rotating stirring blades (201) and the horizontal plane is 55 degrees.